scholarly journals Preparation of Silicone Emulsion Defoamer with Easy Separation of Magnetic Hydrophobic Nanoparticles

2021 ◽  
Vol 58 (2) ◽  
pp. 114-120
Author(s):  
Shengdi Zhang ◽  
Hongling Chen
Keyword(s):  
Magnetic Nanoparticles ◽  
Tetraethyl Orthosilicate ◽  
Solid Particles ◽  
Nano Particles ◽  
Step Process ◽  
X Ray ◽  
Silicone Emulsion ◽  
One Step ◽  
Core Shell Structure ◽  
Scanning Electron

Abstract To prepare lyophobic magnetic nanoparticles (LMNs) with core/shell structure to be applied in silicone emulsion defoamer, magnetic nanoparticles covered with silica (MNS) were prepared in a one-step process from FeCl3 · 6H2O, FeCl2 · 4H2O and tetraethyl orthosilicate and then modified with poly (methylhydrosiloxane). X-ray powder diffraction (XRD), scanning electron microscope (SEM), Fourier transform infrared spectroscope (FTIR), thermogravimetric analysis (TGA), and contact angle tests were performed to characterize the nano-particles, and the droplets of the defoamer emulsion were observed with a microscope. The foam breaking and foam inhibition properties of the defoamer and the magnetic separation of the particles were observed and recorded by a camera. It was found that the silicone emulsion defoamer exhibited good foam breaking and foam inhibition properties for foaming systems with anionic, cationic and non-ionic surfactants, respectively. The solid particles in the defoamer could be easily separated from the defoamed systems by a magnet.

One-Step Synthesis of BaCO3 Nano-Particles via Mechano-Chemical Method

2012 ◽  
Vol 622-623 ◽  
pp. 985-989
Author(s):  
H. Akbari Moayyer ◽  
A. Ataie ◽  
Amin Nozari ◽  
Saeed Jafari
Keyword(s):  
Chemical Method ◽  
Milling Time ◽  
Barium Carbonate ◽  
Phase Evolution ◽  
Nano Particles ◽  
X Ray Diffraction ◽  
Chemical Route ◽  
X Ray ◽  
One Step ◽  
Scanning Electron

Barium carbonate (BaCO3) nano-particles were synthesized from the mixture of Ba(OH)2.8H2O and Na2CO3 by mechano-chemical route without any subsequent heat treatment of the as-milled powders. Effects of milling time and addition of process control agents (PCA) on the phase composition and morphology of products have been investigated. The samples were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). XRD results show that BaCO3 nano-particles were synthesized only after 10 minutes of mechanical milling and phase evolution was not taken place by further milling. SEM results indicated that pencil-like and globular-like were two major morphologies of the particles. Addition of stearic acid as a PCA resulted in homogenized globular-like nano-particles with a mean particle size of 54 nm.

Preparation of nanocellulose by hydrolysis with ionic liquids and two-step hydrolysis with ionic liquids and enzymes

2021 ◽  
Vol 116 ◽  
pp. 5-14
Author(s):  
Marta Babicka ◽  
Magdalena Woźniak ◽  
Kinga Szentner ◽  
Sławomir Borysiak ◽  
Krzysztof Dwiecki ◽  
...  
Keyword(s):  
Ionic Liquids ◽  
Degree Of Crystallinity ◽  
Cellulolytic Enzyme ◽  
X Ray Diffraction ◽  
Production Methods ◽  
Step Process ◽  
X Ray ◽  
One Step ◽  
Xrd Patterns ◽  
The One

The aim of this study was to compare parameters of nanocellulose obtained by two different procedures: hydrolysis with ionic liquids (1-allyl-3-methylimidazolium chloride and 1-ethyl-3-methylimidazolium acetate) and hydrolysis with ionic liquids in combination with hydrolysis using a cellulolytic enzyme from Trichoderma reesei. Avicel cellulose was treated with two ionic liquids: 1-allyl-3-methylimidazolium chloride (AmimCl) and 1-ethyl 3-methylimidazolium acetate (EmimOAc). In the two-step hydrolysis cellulose after treatment with ionic liquids was additionally hydrolyzed with a solution of enzymes. In order to characterize the obtained material, the following analyses were used: infrared spectroscopy, X-ray diffraction and dynamic light scattering. The results indicated that cellulose obtained by two-step nanocellulose production methods (first hydrolysis with ionic liquids and then with enzymes) showed similar parameters (particle size, XRD patterns and degree of crystallinity) as the material after the one-step process, i.e. hydrolysis with ionic liquids.

scholarly journals The Effect of Nano-Particles and Water Glass on the Water Stability of Magnesium Phosphate Cement Based Mortar

Materials ◽  
2019 ◽  
Vol 12 (22) ◽  
pp. 3755 ◽  
Author(s):  
Hu Feng ◽  
Xiangyu Zhao ◽  
Gang Chen ◽  
Changwei Miao ◽  
Xiaocong Zhao ◽  
...  
Keyword(s):  
Electron Microscope ◽  
Water Glass ◽  
Water Immersion ◽  
Nano Particles ◽  
Magnesium Phosphate ◽  
Composition Analysis ◽  
Water Stability ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scanning Electron

This paper experimentally presented the water stability of magnesium phosphate cement (MPC) modified by nano-Al2O3 (NA), nano-Fe2O3 (NF) and water glass (WG). The optimal addition of 6% NA, 2% NF and 1% WG significantly improved the water stability of MPC mortar by 86%, 101% and 96% after 28 days of water immersion, respectively. X-Ray Diffraction (XRD) and Scanning Electron Microscope (SEM) were used to analyze the water stability of MPC modified by NA, NF and WG. The results of the micrograph and composition analysis revealed that the proper amount of NA, NF or WG could fill the micro pores and improve the hydration of interior structures of MPC mortar. Thus, the microstructural compactness was satisfied to keep a good water stability of MPC mortar.

The Effect of Alcoholic Reducing Agent on Morphology and Structure of VO2 (B) Nano-Particles

2011 ◽  
Vol 306-307 ◽  
pp. 1225-1228 ◽  
Author(s):  
Ji Qi ◽  
Chen Niu
Keyword(s):  
Cetyltrimethylammonium Bromide ◽  
Raw Materials ◽  
Thermal Reduction ◽  
Nano Particles ◽  
X Ray Diffraction ◽  
X Ray ◽  
Structure And Morphology ◽  
Morphology And Structure ◽  
Properties Of Materials ◽  
Scanning Electron

Vanadium dioxides (VO2) is synthesized by hydrothermal method. In this process,V2O5 powder is used as raw materials,cetyltrimethylammonium bromide (CTAB) is used as template and different alcohols such as methanol, ethanol, propanol and butanol are used as reductants. X-ray diffraction (XRD) and scanning electron microscopy (SEM) are used to test the properties of VO2 nanoparticles. The results show that VO2(B) nano-particles were succsessfully synthesized under the conditions of thermal reduction temperature 180°C, reaction time 24h and drying temperature 60°C. The variety of alcoholic reducing agents plays an important role in the structure and morphology of the product VO2(B), which relates closly to the electric properties of materials.

Ethylenediamine Processed Cu2SnS3 Nano Particles via Mild Solution Route

2016 ◽  
Vol 19 (1) ◽  
pp. 001-005 ◽  
Author(s):  
Paul Nesamony Prathiba Jeya Helan ◽  
Kannusamy Mohanraj ◽  
Sethuramachandran Thanikaikarasan ◽  
Thaiyan Mahalingam ◽  
Ganesan Sivakumar ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Fourier Transform ◽  
Fourier Transform Infrared ◽  
Nano Particles ◽  
X Ray Diffraction ◽  
X Ray ◽  
Electron Microscopy Analysis ◽  
Microscopy Techniques ◽  
Scanning Electron

Copper tin sulphide nanoparticles have been prepared by solution growth technique at various ethylenediamine concentrations. Prepared samples have been characterized using x-ray diffraction, fourier transform infrared, Raman and scanning electron microscopy techniques. x-ray diffraction results revealed that the prepared samples are nanocrystalline in nature with tetragonal structure. Fourier transform infrared spectroscopy analysis results showed the presence of Cu-O, Sn-O and Sn-S vibrations in the wavenumber range between 450 and 620 cm-1. Vibrational symmetry of prepared samples have been analyzed using Raman spectroscopy. Scanning electron microscopy analysis indicated the formation of flower like nanocrystals for samples prepared at various Ethylenediamine concentrations.

Study the Effect of HAp Content in PLA/HAp Microsphere on the Efficiency of Drug (Clindamycin) Loading Process

2013 ◽  
Vol 834-836 ◽  
pp. 559-562 ◽  
Author(s):  
Juntima Pradid ◽  
Wirunya Keawwattana ◽  
Siree Tangbunsuk
Keyword(s):  
Electron Microscopy ◽  
Thermal Process ◽  
High Performance ◽  
Core Shell ◽  
X Ray Diffraction ◽  
X Ray ◽  
Ultrasound Field ◽  
Sample Characterization ◽  
Core Shell Structure ◽  
Scanning Electron

An ultrasound field was applied to obtain Polylactic acid (PLA)/Hydroxyapatite (HAp) biocomposite microspheres with the specific core-shell structure to be applied as a carrier of a drug. The hydroxyapatite was obtained from crocodile bone by thermal process. Sample characterization was achieved by powder X-ray diffraction (XRD), Energy-dispersive X-ray spectroscopy (EDX) Scanning electron microscopy (SEM) and High Performance Liquid Chromatography (HPLC). As the result, the PLA/HAp loading clindamycin with different polymer-to-ceramic part wt.% ratio (100:0, 90:10, 80:20, and 70:30) showed the agglomeration of sphere-like particles. In addition, the loading efficiency of clindamycin increased with increasing HAp content up to 20%.

scholarly journals One Step Process for Infiltration of Magnetic Nanoparticles into CNT Arrays for Enhanced Field Emission

2018 ◽  
Vol 5 (15) ◽  
pp. 1701631 ◽  
Author(s):  
Srividya Sridhar ◽  
Chandra Sekhar Tiwary ◽  
Benjamin Sirota ◽  
Sehmus Ozden ◽  
Kaushik Kalaga ◽  
...  
Keyword(s):  
Magnetic Nanoparticles ◽  
Field Emission ◽  
Step Process ◽  
One Step ◽  
Cnt Arrays

Solvothermal Synthesis and Electrochemical Properties of Hairball-Like Bismuth Trisulphide Microcrystallines

2011 ◽  
Vol 233-235 ◽  
pp. 2289-2293
Author(s):  
Pin Jiang Li ◽  
Wen Jun Fa ◽  
Yan Ge Zhang ◽  
Bao Jun Huang ◽  
Yi Dong Zhang
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Solvothermal Synthesis ◽  
Growth Process ◽  
Solvothermal Process ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
One Step ◽  
Scanning Electron

Hairball-like bismuth trisulphide microcrystallines has been successfully prepared via one step solvothermal process and characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and high-resolution transmission electron microscopy (HRTEM) techniques. The morphologies of the Bi2S3 microcrystallines were influenced by reaction time, temperature, the mole ratio of the reactants and concentration of starting materials, and the growth process has been proposed. The electrochemical behavior of Bi2S3 was investigated using the cyclic voltammetry.

Effects of Reductive Conditions on the Electrochemical Properties of LiFePO4/C Derived by Fe3+ Sources

2014 ◽  
Vol 1081 ◽  
pp. 313-317
Author(s):  
Yan Wen Lu ◽  
Yu Ge ◽  
Yue Feng Tang
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Raw Materials ◽  
Thermal Method ◽  
X Ray Diffraction ◽  
Sintering Atmosphere ◽  
X Ray ◽  
Electrochemical Capacity ◽  
One Step ◽  
Scanning Electron

A one-step carbon thermal method was used to prepare LiFePO4/C particles by using normal Fe2O3, LiH2PO4and sucrose as raw materials. The effect of H2content in the sintering atmosphere of N2on the morphology and the electrochemical performance were investigated. LiFePO4/C materials were characterized by X-ray diffraction, scanning electron microscopy and the elemental analyzer. The results show that the precursor sintering under the atmosphere of 8%H2+N2exhibits the highest electrochemical capacity (162.3 mAh/g at 0.1C) .

scholarly journals Synthesis and thermal conductivity of functionalized biocarbon-Fe3O4 nanocomposite-based green nanofluid for heat transfer applications

2021 ◽  
Vol 321 ◽  
pp. 01003
Author(s):  
Divya Barai ◽  
Sohan Parbat ◽  
Bharat Bhanvase
Keyword(s):  
Heat Transfer ◽  
Electron Microscopy ◽  
Thermal Conductivity ◽  
Nanocomposite Particles ◽  
X Ray ◽  
Conductivity Enhancement ◽  
Water Based ◽  
One Step ◽  
Ultrasound Assisted ◽  
Scanning Electron

Bio-based graphitic carbon was synthesized in this work by one-step carbonization of bamboo waste at low temperature. This bio-based carbon was then functionalized in order to decorated it with Fe3O4 nanoparticles. The functionalized biocarbon-Fe3O4 (f-biocarbon-Fe3O4) nanocomposite was synthesized using ultrasound-assisted coprecipitation method which was then confirmed by scanning electron microscopy, Fourier transform infrared spectroscopy, and X-ray diffractometry. Water-based nanofluid was prepared using the synthesized f-biocarbon-Fe3O4 nanocomposite particles. Thermal conductivity of this nanofluid was analyzed at different concentrations and temperatures. A thermal conductivity enhancement of almost 80% was recorded at 35°C for nanofluid containing 0.1 vol.% of f-biocarbon-Fe3O4 nanocomposite particles compared to water. Also, empirical model is developed for prediction of thermal conductivity as a function of concentration and temperature of bamboo waste-derived f-biocarbon-Fe3O4 nanocomposite-based green nanofluid.

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