Structural and Magnetic Properties of Untwinned Yba2Cu3O6+x Single Crystals

1989 ◽  
Vol 169 ◽  
Author(s):  
Debra L. Kaiser ◽  
Frank W. Gayle ◽  
Lydon J. Swartzendruber ◽  
Winnie Wong-Ng ◽  
Steven F. Watkins ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Single Crystals ◽  
Flux Pinning ◽  
Magnetic Measurements ◽  
Mirror Plane ◽  
X Ray Diffraction ◽  
X Ray ◽  
Structural And Magnetic Properties ◽  
Low Levels ◽  
Superconducting Onset Temperature

AbstractWe have conducted structural and magnetic investigations on thermomechanically-detwinned YBa2Cu3O6+x single crystals. Single crystal x-ray diffraction studies on a fully untwinned crystal with a superconducting onset temperature of 54 K have revealed that oxygen atoms in the basal plane are offset from the crystallographic mirror plane in the a direction, leading to “zig-zag” Cu-O chains. Magnetic measurements on untwinned and twinned crystals at 77 K indicate low levels of flux pinning in both crystals, with a slightly larger amount of pinning in the twinned crystal.

Structural and magnetic properties of DyCo4−xFexGa compounds

2010 ◽  
Vol 25 (S1) ◽  
pp. S31-S35
Author(s):  
W. H. Zhang ◽  
J. Q. Li ◽  
Y. J. Yu ◽  
F. S. Liu ◽  
W. Q. Ao ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Magnetic Measurements ◽  
Uniaxial Anisotropy ◽  
Solubility Limit ◽  
Spin Reorientation ◽  
X Ray Diffraction ◽  
X Ray ◽  
Cell Parameters ◽  
Spin Reorientation Transition ◽  
Structural And Magnetic Properties

The structural and magnetic properties of the DyCo4−xFexGa compounds with x=0, 0.5, 1, and 1.5 have been investigated by X-ray diffraction and magnetic measurements. Powder X-ray diffraction analysis reveals that each of the DyCo4−xFexGa compounds has a hexagonal CaCu5-type structure (space group P6/mmm). The Fe solubility limit in DyCo4−xFexGa is x<1.5. The higher the value of x, the larger the unit-cell parameters a, c, V, and the 3d-sublattice moment but the smaller the 3d uniaxial anisotropy. Magnetic measurements show that the Curie temperature of DyCo4−xFexGa increases from 498 K for x=0 to 530 K for x=1.5, the compensation temperature Tcomp decreases from 286 K for x=0 to 238 K for x=1.5, and the spin-reorientation transition temperature increases from 403 K for x=0 to 530 K for x=0.5. No spin-reorientation transition was found in the samples with x=1.0 and 1.5. The saturation magnetization of DyCo4−xFexGa measured at 173 K increases but the magnetization measured at 300 K decreases with increasing Fe content x.

Structural and magnetic properties of pure and cobalt doped Gallium Nitride nanocrystals

2010 ◽  
Vol 1257 ◽  
Author(s):  
Vottikondala Ganesh ◽  
Suresh Sundaram ◽  
Krishnan Baskar
Keyword(s):  
Magnetic Properties ◽  
Gallium Nitride ◽  
Magnetic Measurements ◽  
Raw Materials ◽  
Ferromagnetic Behavior ◽  
Secondary Phases ◽  
X Ray Diffraction ◽  
X Ray ◽  
Structural And Magnetic Properties ◽  
Co Doped

AbstractIn the present study pure and doped gallium nitride (GaN) nanocrystals were synthesized using gallium trichloride (GaCl3), ethylene diamine tetra acetic acid (EDTA) and cobalt chloride as raw materials at a temperature of 900 °C in ammonia (NH3) atmosphere. The XRD spectrum for pure and cobalt doped GaN nanocrystals shows the formation of single phase wurtzite structure. No impurity phases were observed in the X-ray diffraction pattern for 5% Co doped sample whereas secondary phases were observed when the doping concentration exceeds 5 %. Shift in X-ray diffraction peaks were observed in Co doped samples towards lower angle side compared to pure GaN, it confirms that the Co atoms introduces in to the GaN lattice. Transmission electron microscopy images were taken for pure and Co doped GaN. Hexagonal morphology was observed in pure GaN samples. The average size of the particle was found to be ˜20 nm for pure and Co doped GaN. The magnetic measurements were carried out for the Co (5% & 10%) doped samples both at 10K and 300K. Clear hysteresis loop in the magnetization curve suggest the presence of ferromagnetic behavior in cobalt doped GaN. Temperature dependent magnetization (M-T) measurements were also carried out for doped samples using Super Conducting Quantum Interface Device (SQUID) from 10K to 300K The results have been discussed and correlated to structural and magnetic properties of the materials.

Influence of Alloying Additions on Enhancement of Soft Magnetic Properties Effect and Crystallization in FeXSiB (X=Cu, V, Co, Zr, Nb) Amorphous Alloys

2007 ◽  
Vol 130 ◽  
pp. 171-174 ◽  
Author(s):  
Z. Stokłosa ◽  
G. Badura ◽  
P. Kwapuliński ◽  
Józef Rasek ◽  
G. Haneczok ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Amorphous Alloys ◽  
Crystallization Process ◽  
Annealing Temperature ◽  
Magnetic Measurements ◽  
X Ray Diffraction ◽  
Soft Magnetic ◽  
X Ray ◽  
Second Stage ◽  
Transmission Electron

The crystallization and optimization of magnetic properties effects in FeXSiB (X=Cu, V, Co, Zr, Nb) amorphous alloys were studied by applying X-ray diffraction methods, high resolution transmission electron microscopy (HRTEM), resistometric and magnetic measurements. The temperatures of the first and the second stage of crystallization, the 1h optimization annealing temperature and the Curie temperature were determined for different amorphous alloys. Activation energies of crystallization process were obtained by applying the Kissinger method. The influence of alloy additions on optimization effect and crystallization processes was carefully examined.

Single crystal growth and magnetic properties of Co-doped ZnNb2O6

2019 ◽  
Vol 33 (23) ◽  
pp. 1950274
Author(s):  
Ying Liu ◽  
Dapeng Xu ◽  
Huamin Yu ◽  
Tian Cui ◽  
Liang Li
Keyword(s):  
Magnetic Properties ◽  
Single Crystals ◽  
Photoelectron Spectroscopy ◽  
Physical Property Measurement System ◽  
Physical Property ◽  
X Ray Diffraction ◽  
Zone Method ◽  
X Ray ◽  
Structure Formula ◽  
Property Measurement

The columbite structure [Formula: see text] single crystals have been successfully grown by using the optical floating zone method. The as-grown crystals are characterized by X-ray diffraction (XRD), Raman spectroscopy (RS) and X-ray photoelectron spectroscopy (XPS). All these analyses show that the doping Co ions do not disturb the structure of columbite [Formula: see text] and some [Formula: see text] ions are substituted by transition metal [Formula: see text] ions without any other impurities. The magnetic properties of as-grown [Formula: see text] crystals have been investigated using Physical Property Measurement System (PPMS). The effective magnetic moment of [Formula: see text] crystals is [Formula: see text], indicating that [Formula: see text] ions present in [Formula: see text] single crystals are in mixed HS and LS states. The ferromagnetic, antiferromagnetic and paramagnetic characters of as-grown crystals are also discussed.

scholarly journals Structural and Magnetic Properties of Ni0.8Fe0.2/Ti Nanoscale Multilayers

Nanomaterials ◽  
2018 ◽  
Vol 8 (10) ◽  
pp. 780 ◽  
Author(s):  
Ricardo López Antón ◽  
Juan A. González ◽  
Juan P. Andrés ◽  
Andrei V. Svalov ◽  
Galina V. Kurlyandskaya
Keyword(s):  
Magnetic Properties ◽  
Temperature Dependence ◽  
Layered Structure ◽  
Magnetic Measurements ◽  
Hysteresis Loops ◽  
Multilayered Structures ◽  
X Ray ◽  
Structural And Magnetic Properties

The influence of the thickness of the Ni0.8Fe0.2 (Permalloy, Py) layers on the structural and magnetic properties of magnetron sputtered Py/Ti multilayers was studied. The thickness of the Py layers was varied in the interval of 8 to 30 Å. X-ray reflectivity scans evidence the existence of a well-defined layered structure in all the samples considered, but also the presence of a complex intermixed interface. The shape of both the temperature dependence of magnetization and the hysteresis loops of the multilayered structures depends strongly on Py thickness. Magnetic and reflectivity measurements were comparatively analyzed in order to better understand the structure of the samples, and specifically, their interfaces. In particular, the presence of small superparamagnetic Py at the interfaces of the samples, especially evident in the samples with the thinnest Py layers, seems confirmed by the magnetic measurements, agreeing well with the reflectivity results.

scholarly journals Structure and magnetic properties of Co-Zn substituted hexagonal ferrites

2018 ◽  
Vol 197 ◽  
pp. 02007
Author(s):  
Erfan Handoko ◽  
Anggoro B S ◽  
Iwan Sugihartono ◽  
Mangasi AM ◽  
Dini Siti Nurwulan ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Single Phase ◽  
Hexagonal Ferrites ◽  
X Ray Diffraction ◽  
Small Particles ◽  
Scanning Electron Microscopy Micrographs ◽  
Ceramic Method ◽  
X Ray ◽  
Structural And Magnetic Properties ◽  
Substitutional Effect

In In this study to understand the substitutional effect of Co-Zn on structural and magnetic properties of the BaFe12-2xCoxZnxO19 M-type hexagonal ferrites with concentration (x= 0.0, 0.2, 0.4, 0.6, 0.8, 1.0) were synthesized by the ceramic method. The results of x-ray diffraction show polycrystalline with single phase. Scanning electron microscopy micrographs shows the hexagonal ferrites that are composed of small particles with large porosity, roughly of spherical shapes. The substitution of Fe3+ ion by Co2+ and Zn2+ has changed magnetic properties of hexagonal ferrites.

scholarly journals Structural and Magnetic Properties of FePd Thin Film Synthesized by Electrodeposition Method

Materials ◽  
2020 ◽  
Vol 13 (6) ◽  
pp. 1454
Author(s):  
Gabriele Barrera ◽  
Federico Scaglione ◽  
Matteo Cialone ◽  
Federica Celegato ◽  
Marco Coïsson ◽  
...  
Keyword(s):  
Thin Film ◽  
Thin Films ◽  
Magnetic Properties ◽  
Deposition Time ◽  
Magnetic Measurements ◽  
X Ray Diffraction ◽  
X Ray ◽  
Fundamental Properties ◽  
Magnetic Features ◽  
Application Fields

Bimetallic nanomaterials in the form of thin film constituted by magnetic and noble elements show promising properties in different application fields such as catalysts and magnetic driven applications. In order to tailor the chemical and physical properties of these alloys to meet the applications requirements, it is of great importance scientific interest to study the interplay between properties and morphology, surface properties, microstructure, spatial confinement and magnetic features. In this manuscript, FePd thin films are prepared by electrodeposition which is a versatile and widely used technique. Compositional, morphological, surface and magnetic properties are described as a function of deposition time (i.e., film thickness). Chemical etching in hydrochloric acid was used to enhance the surface roughness and help decoupling crystalline grains with direct consequences on to the magnetic properties. X-ray diffraction, SEM/AFM images, contact angle and magnetic measurements have been carried out with the aim of providing a comprehensive characterisation of the fundamental properties of these bimetallic thin films.

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