Radiation-Enhanced Plastic Flow of Covalent Materials During Ion Irradiation

1991 ◽  
Vol 235 ◽  
Author(s):  
C. A. Volkert ◽  
A. Polman
Keyword(s):  
Plastic Deformation ◽  
Amorphous Materials ◽  
Ion Irradiation ◽  
Ion Beam ◽  
Polycrystalline Aluminum ◽  
Aluminum Films ◽  
Crystalline Materials ◽  
Curvature Measurement ◽  
Viscous Shear ◽  
Viscous Shear Flow

ABSTRACTPlastic deformation of several covalently-bound materials has been studied during ion irradiation. In all of these materials, namely crystalline and amorphous silicon, crystalline and amorphous Si0.9Ge0.1, and amorphous SiO2, the damage created by the ion beam causes density changes in the irradiated region which eventually saturate with ion dose. In the crystalline materials, the density changes were accompanied by a transformation to the amorphous phase. Superimposed on the density changes is plastic deformation which occurs during irradiation of both crystalline and amorphous materials to relieve stresses in the irradiated region. A wafer curvature measurement technique has been developed which allows the contributions from density changes and plastic deformation to be distinguished and the stress dependence of the plastic deformation to be determined.In all of the amorphous materials, the plastic deformation is Newtonian viscous shear flow, which is characteristic of solids where deformation is governed by the diffusive motion of point defects. The radiation-enhanced shear viscosity per ion was flux-independent, revealing that flow occurs rapidly, probably within the localized damaged regions created by each ion. This viscosity does not depend strongly on the material. In fact, similar viscosities were obtained during measurements of radiation-enhanced plastic deformation of crystalline covalent samples and polycrystalline aluminum films.

Ion-beam induced plastic deformation in amorphous materials investigated by marker implantation and RBS

1992 ◽  
Vol 64 (1-4) ◽  
pp. 684-686 ◽  
Author(s):  
A. Benyagoub ◽  
S. Klaumünzer ◽  
L. Thomé ◽  
J.C. Dran ◽  
F. Garrido ◽  
...  
Keyword(s):  
Plastic Deformation ◽  
Amorphous Materials ◽  
Ion Beam

Ion-Beam-Induced Plastic Deformation of Amorphous Materials

1987 ◽  
Vol 93 ◽  
Author(s):  
S. Klaumünzer ◽  
Hou Ming-Dong ◽  
G. Schumacher ◽  
Li Chang-Lin
Keyword(s):  
Plastic Deformation ◽  
Glass Transition ◽  
Transition Temperature ◽  
Glass Transition Temperature ◽  
Metallic Glasses ◽  
Heavy Ions ◽  
Amorphous Materials ◽  
Ion Beam ◽  
Amorphous Material ◽  
Essential Parameter

ABSTRACTAt temperatures far below the glass transition temperature metallic glasses undergo plastic deformation during irradiation with a beam of fast heavy ions at energies at which electronic stopping is the dominant deceleration mechanism. This plastic deformation causes irreversible anisotropic changes in sample dimensions. Various (Fe,Co,Ni)∼8O(B,Si)∼20 glasses and the crystalline alloys Ni80Cr20 and Fe70Cr25A15 are examin? 9 for their susceptibility to this effect by irradiation below 50 K with 129Xe ions at 2.8 MeV/u. The data suggest that the excess free volume of an amorphous material is an essential parameter for the magnitude of ion-beam-induced plastic deformation.

TEM studies of amorphization processes and amorphous structures

1988 ◽  
Vol 46 ◽  
pp. 448-449
Author(s):  
T. E. Mitchell ◽  
R. B. Schwarz
Keyword(s):  
Amorphous Materials ◽  
Fission Products ◽  
Rapid Quenching ◽  
Surface Films ◽  
List Type ◽  
Oxide Glasses ◽  
Crystalline Materials ◽  
Amorphous Structures ◽  
Amorphous Surface ◽  
Interfacial Films

Traditional oxide glasses occur naturally as obsidian and can be made easily by suitable cooling histories. In the past 30 years, a variety of techniques have been discovered which amorphize normally crystalline materials such as metals. These include [1-3]:Rapid quenching from the vapor phase.Rapid quenching from the liquid phase.Electrodeposition of certain alloys, e.g. Fe-P.Oxidation of crystals to produce amorphous surface oxide layers.Interdiffusion of two pure crystalline metals.Hydrogen-induced vitrification of an intermetal1ic.Mechanical alloying and ball-milling of intermetal lie compounds.Irradiation processes of all kinds using ions, electrons, neutrons, and fission products.We offer here some general comments on the use of TEM to study these materials and give some particular examples of such studies.Thin specimens can be prepared from bulk homogeneous materials in the usual way. Most often, however, amorphous materials are in the form of surface films or interfacial films with different chemistry from the substrates.

Electron and ion irradiation-induced dissolution of mechanical twins in the intermetalic U3Si: An in situ HVEM study

1989 ◽  
Vol 47 ◽  
pp. 652-653
Author(s):  
Charles W. Allen ◽  
Robert C. Birtcher
Keyword(s):  
Elevated Temperatures ◽  
Ion Irradiation ◽  
Ion Beam ◽  
National Laboratory ◽  
Argonne National Laboratory ◽  
Heavy Ion ◽  
High Energy ◽  
Mechanical Twinning ◽  
In Situ Experiments

The uranium silicides, including U3Si, are under study as candidate low enrichment nuclear fuels. Ion beam simulations of the in-reactor behavior of such materials are performed because a similar damage structure can be produced in hours by energetic heavy ions which requires years in actual reactor tests. This contribution treats one aspect of the microstructural behavior of U3Si under high energy electron irradiation and low dose energetic heavy ion irradiation and is based on in situ experiments, performed at the HVEM-Tandem User Facility at Argonne National Laboratory. This Facility interfaces a 2 MV Tandem ion accelerator and a 0.6 MV ion implanter to a 1.2 MeV AEI high voltage electron microscope, which allows a wide variety of in situ ion beam experiments to be performed with simultaneous irradiation and electron microscopy or diffraction.At elevated temperatures, U3Si exhibits the ordered AuCu3 structure. On cooling below 1058 K, the intermetallic transforms, evidently martensitically, to a body-centered tetragonal structure (alternatively, the structure may be described as face-centered tetragonal, which would be fcc except for a 1 pet tetragonal distortion). Mechanical twinning accompanies the transformation; however, diferences between electron diffraction patterns from twinned and non-twinned martensite plates could not be distinguished.

scholarly journals Comparison of short-range order in irradiated dysprosium titanates

2021 ◽  
Vol 5 (1) ◽  
Author(s):  
Roman Sherrod ◽  
Eric C. O’Quinn ◽  
Igor M. Gussev ◽  
Cale Overstreet ◽  
Joerg Neuefeind ◽  
...  
Keyword(s):  
Long Range ◽  
Short Range ◽  
Structural Model ◽  
Ion Irradiation ◽  
Function Analysis ◽  
Ion Beam ◽  
Structural Response ◽  
Heavy Ion ◽  
Range Order ◽  
Radiation Resistant

AbstractThe structural response of Dy2TiO5 oxide under swift heavy ion irradiation (2.2 GeV Au ions) was studied over a range of structural length scales utilizing neutron total scattering experiments. Refinement of diffraction data confirms that the long-range orthorhombic structure is susceptible to ion beam-induced amorphization with limited crystalline fraction remaining after irradiation to 8 × 1012 ions/cm2. In contrast, the local atomic arrangement, examined through pair distribution function analysis, shows only subtle changes after irradiation and is still described best by the original orthorhombic structural model. A comparison to Dy2Ti2O7 pyrochlore oxide under the same irradiation conditions reveals a different behavior: while the dysprosium titanate pyrochlore is more radiation resistant over the long-range with smaller degree of amorphization as compared to Dy2TiO5, the former involves more local atomic rearrangements, best described by a pyrochlore-to-weberite-type transformation. These results highlight the importance of short-range and medium-range order analysis for a comprehensive description of radiation behavior.

Submicron Patterned Anodic Oxidation of Aluminum Thin Films

2000 ◽  
Vol 636 ◽  
Author(s):  
Qiyu Huang ◽  
Whye-Kei Lye ◽  
David M. Longo ◽  
Michael L. Reed
Keyword(s):  
Thin Films ◽  
Anodic Oxidation ◽  
Ion Beam ◽  
Electrochemical Anodization ◽  
Optical Methods ◽  
Imprint Lithography ◽  
Aluminum Films ◽  
Aspect Ratios ◽  
Potential Applications ◽  
Nano Imprint

AbstractAlumina formed by the electrochemical anodization of bulk aluminum has a regular porous structure [1]. Sub-100 nm pores with aspect ratios as high as 1000:1 can easily be formed [2] without elaborate processing. Anodization of aluminum thus provides the basis for the inexpensive, high throughput microfabrication of structures with near vertical sidewalls [2]. In this work we explore the patterned anodic oxidation of deposited aluminum thin films, facilitating the integration of this technique with established microfabrication tools. An anodization barrier of polymethylmethacrylate (PMMA) is deposited onto 300 nm thick aluminum films. The barrier film is subsequently patterned and the exposed aluminum anodized in a 10% sulfuric acid solution. Barrier patterning techniques utilized in this study include optical exposure, ion-beam milling and nano-imprint lithography. Sharp edge definition on micron scale patterns has been achieved using optical methods. Extension of this technique to smaller dimensions by ion-beam milling and nano-imprint lithography is presented. We further report on the observation of contrast reversal of anodization with very thin PMMA barriers, which provides a novel means of pattern transfer. Potential applications and challenges will be discussed.

Deformation and Heat Treatment of Cold Drawn Gold

2007 ◽  
Vol 550 ◽  
pp. 289-294
Author(s):  
Suk Hoon Kang ◽  
Jae Hyung Cho ◽  
Joon Sub Hwang ◽  
Jong Soo Cho ◽  
Yong Jin Park ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Plastic Deformation ◽  
Mechanical Stability ◽  
Ion Beam ◽  
Quantitative Measure ◽  
Electron Backscattered Diffraction ◽  
Conducting Path ◽  
Deformation And Heat Treatment ◽  
Gold Wires

Cold drawn gold wires are widely applied in electronic packaging process to interconnect micro-electronic components. They basically provides a conducting path for electronic signal transfer, and experience thermo-mechanical loads in use. The mechanical stability of drawn gold wires is a matter of practical concern in the reliable functioning of electronic devices. It is known that mechanical properties of materials are deeply related to the microstructure. With appropriate control of deformation and heat processes, the mechanical properties of final products, such as tensile strength and elongation can be improved. Severe plastic deformation by torsion usually contributes to grain refinement and increment of strength. In this study, microstructure variations with torsion strain followed by drawing and heat treatment were investigated. Analyses by focused ion beam (FIB) and electron backscattered diffraction (EBSD) were carried out to characterize the effect of deformation and heat treatment on the drawn gold wires. Pattern quality of EBSD measurements was used as a quantitative measure for plastic deformation.

The viscous secondary flow ahead of an infinite cylinder in a uniform parallel shear flow

1960 ◽  
Vol 7 (1) ◽  
pp. 145-155 ◽  
Author(s):  
Alar Toomre
Keyword(s):  
Shear Flow ◽  
Lateral Displacement ◽  
Reynolds Numbers ◽  
Infinite Cylinder ◽  
List Type ◽  
Displacement Effect ◽  
Simple Method ◽  
Viscous Shear ◽  
Parallel Shear Flow ◽  
Viscous Shear Flow

A simple method is presented in this paper for calculating the secondary velocities, andthe lateral displacement of total pressure surfaces (i.e. the ‘displacement effect’) in the plane of symmetry ahead of an infinitely long cylinder situated normal to a steady, incompressible, slightly viscous shear flow; the cylinder is also perpendicular to the vorticity, which is assumed uniform but small. The method is based on lateral gradients of pressure, these being calculated from the primary flow alone. Profiles of the secondary velocities are obtained at several Reynolds numbers ahead of two specific cylindrical shapes: a circular cylinder, and a flat plate normal to the flow. The displacement effect is derived and, rathe surprisingly, is found to be virtually independent of the Reynolds number.

SPUTTERING WITH GAS CLUSTER-ION BEAMS

1996 ◽  
Vol 03 (01) ◽  
pp. 1017-1021 ◽  
Author(s):  
J. MATSUO ◽  
M. AKIZUKI ◽  
J. NORTHBY ◽  
G.H. TAKAOKA ◽  
I. YAMADA
Keyword(s):  
Ion Irradiation ◽  
Removal Rate ◽  
Ion Beam ◽  
Solid Surfaces ◽  
Silicon Surfaces ◽  
Cluster Ions ◽  
Mass Filter ◽  
Cluster Bombardment ◽  
Cluster Ion Beams ◽  
Cluster Ion

A high-current (~100 nA) cluster-ion-beam equipment with a new mass filter has been developed to study the energetic cluster-bombardment effects on solid surfaces. A dramatic reduction of Cu concentration on silicon surfaces has been achieved by 20-keV Ar cluster (N~3000) ion bombardment. The removal rate of Cu with cluster ions is two orders of magnitude higher than that with monomer ions. A significantly higher sputtering yield is expected for cluster-ion irradiation. An energetic cluster-ion beam is quite suitable for removal of metal.

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