scholarly journals OPTIMIZATION OF THE AQUEOUS EXTRACT PROCESS FROM MANGOSTEEN PEEL FOR DYEING SILK

2018 ◽  
Vol 54 (4B) ◽  
pp. 94
Author(s):  
Hong Phuong Pham Thi
Keyword(s):  
Aqueous Extract ◽  
Extraction Efficiency ◽  
Extraction Process ◽  
Extraction Temperature ◽  
Color Fastness ◽  
Silk Fabric ◽  
Color Strength ◽  
Water Solvent ◽  
Mangosteen Peel ◽  
Juice Extraction

This research studied the juice extraction process from mangosteen peel with water solvent and the paramesters influencing on extraction process such as extraction temperature, extraction time and extraction ratio, and evaluating the juice of extract by determining extraction efficiency, color saturation of fabric and color fastness of silk fabric. The research results showed that the juice extracted from mangosteen peel can be used to dye silk fabric with high color strength and fastness. And the results of research will bring the efficiency of environmental, economy and society; and will meet urgent demands today.

Optimization of Murrayafoline A ethanol extraction process from the roots of Glycosmis stenocarpa, and evaluation of its Tumorigenesis inhibition activity on Hep-G2 cells

2021 ◽  
Vol 19 (1) ◽  
pp. 830-842
Author(s):  
Quoc Toan Tran ◽  
The Dan Pham ◽  
Thanh Duong Nguyen ◽  
Van Huyen Luu ◽  
Huu Nghi Do ◽  
...  
Keyword(s):  
Large Scale ◽  
Extraction Efficiency ◽  
Raw Materials ◽  
Biological Activities ◽  
Extraction Process ◽  
Extraction Time ◽  
Extraction Temperature ◽  
Hep G2 ◽  
Independent Parameters

Abstract Glycosmis stenocarpa is a species of shrub found in the Northern provinces of Vietnam. Its roots contain different carbazolic derivatives, mainly Murrayafoline A (Mu-A), which exhibits valuable biological activities. In this study, we performed an extraction of Mu-A from the roots of G. stenocarpa and optimized this process using response surface methodology (RSM) according to a central composite design, with three independent parameters including extraction time (min), extraction temperature (°C), and solvent/material ratio (mL/g). Two dependent variables were the Mu-A content (mg/g raw materials) and extraction efficiency (%). The optimal conditions to extract Mu-A were found to be as follows: extraction temperature, 67°C; extraction time, 165 min; and solvent/material ratio, 5:1. Under these conditions, the Mu-A content and extraction efficiency were 38.94 ± 1.31 mg/g raw materials and 34.98 ± 1.18%, respectively. Mu-A exhibited antiproliferation and antitumor-promoting activity against the HepG-2 cell line. The present optimization work of Mu-A extraction from G. stenocarpa roots contributed to the attempt of designing a large-scale extraction process for the compound and further exploitation of its potential in vivo applications.

scholarly journals Citrus Bioactive Limonoid Extraction using Environment-friendly Hydrotropy

HortScience ◽  
2006 ◽  
Vol 41 (4) ◽  
pp. 1008C-1008
Author(s):  
Deepak Dandekar ◽  
G. K. Jayaprakasha ◽  
Bhimanagouda Patil
Keyword(s):  
Extraction Efficiency ◽  
Design Method ◽  
Maximum Yield ◽  
Extraction Process ◽  
Extraction Methods ◽  
Raw Material ◽  
Extraction Temperature ◽  
Optimum Conditions ◽  
Environment Friendly ◽  
Health Promoting

Citrus consumption has been shown to promote human health due to presence of several bioactive compounds. In the process of understanding the health benefits of citrus, we need to isolate and characterize these compounds. Limonoids are one of such prominent, but lesser-known phytonutrients that have been shown to prevent cancers of the mouth, skin, lung, breast, and colon. With the growing interest in the health-promoting properties of citrus limonoids, the demand for these bioactives has significantly increased. It has been critical to explore environment-friendly extraction methods rather than using hazardous organic solvents. A water-based hydrotropic extraction of limonoid aglycones from sour orange (Citrus aurantium L.) seeds was developed. Two hydrotropes, sodium salicylate (Na-Sal) and sodium cumene sulfonate (Na-CuS), were studied for extraction efficiency using the Box Behnken experiment design method. The extraction efficiency of prominent aglycone limonin was observed depending on hydrotrope concentration, extraction temperature, and percentage of raw material loading. Response Surface Analysis (RSA) of data predicted the optimum conditions for maximum yield. Recovery of aglycones from filtered extract is also easily achieved by mere dilution using water at pH 3 or 7 or by partitioning the extract with dichloromethane. At optimum conditions, limonin yield of 0.46 mg/g seeds in the case of Na-Sal extraction and 0.65 mg/g seeds in the case of Na-CuS extraction was achieved. The results demonstrated that the hydrotropic extraction process of limonoid aglycones has practical commercial importance. This project is based upon work supported by the USDA–CSREES IFAFS #2001 52102 02294 and USDA–CSREES #2005-34402-14401 “Designing Foods for Health” through the Vegetable and Fruit Improvement Center.

Analysis and Study of Effect of Natural Dye From Bombax malabarica on Silk Fabric

2019 ◽  
Vol 38 (1) ◽  
pp. 49-58
Author(s):  
V. Narayana Swamy
Keyword(s):  
Reduction Rate ◽  
Operating Conditions ◽  
Natural Dye ◽  
Color Fastness ◽  
Silk Fabric ◽  
Fastness Properties ◽  
Dye Uptake ◽  
Color Strength ◽  
Cielab System ◽  
Silk Fabrics

The current study deals with the extraction of natural dye from Bombax malabarica flowers, readily available by-product. Dye was extracted under different operating conditions such as time (60–90 min), temperature (90–95 °C), and pH 9. The dyed samples were subjected to CIELAB system using Gretag Macbeth Color Eye 7000A Spectrophotometer for the evaluation of color strength and L*a*b* C and H values. To improve the dye uptake and color fastness, pre and postmordanting was carried out using alum, tannic, and tartaric acid mordants. Dyed silk fabrics were tested for its color fastness when subjected to light, washing, and rubbing. Fastness properties of dyed silk fabric samples were found considerably good. Mordanted silk fabric samples showed increase in dye uptake resulting in high color strength and better fastness properties. The dyed silk samples displayed good antimicrobial activity (reduction rate: 48%) against the bacteria Escherichia coli and (reduction rate: 55%) against Staphylococcus aureus.

scholarly journals ENHANCEMENT OF CAFFEINE RECOVERY FROM ROASTED COFFEE POWDER BY ENZYME CELLULASE PRETREATMENT, HOT-WATER EXTRACTION AND CO2-ADDING

2020 ◽  
Vol 1 (40) ◽  
pp. 103-111
Author(s):  
Quoc Kien Giang ◽  
Thuy Mong Lam ◽  
Duy The Phan
Keyword(s):  
Extraction Efficiency ◽  
Extraction Process ◽  
Hot Water ◽  
Roasted Coffee ◽  
Enzyme Pretreatment ◽  
Water Solvent ◽  
Pretreatment Time ◽  
Coffee Powder ◽  
Positive Results

The efficiency of caffeine recovery during extraction with highpressure hot-water solvent was investigated to find out the conditions for maximum caffeine recovery in roasted coffee powder. In addition, to support the extraction process with high-pressure hot-water solvent, cellulase enzyme pretreatment of roasted coffee powder is also applied and has demonstrated the supporting role of the enzyme in improving caffeine extraction efficiency. CO2 can participate in the extraction process with the role of changing the pH of the solvent at the high temperature and obtained positive results. In the presence of the enzyme cellulase at avalue of 8 UI/g, the pretreatment time was 90 minutes; the extraction process performed at 110oC for temperature and 10 min for the extraction time, the efficiency of caffeine recovery can reach 96,36 ±2,56%.

Pigment Extraction of Safflower, Dyeing Properties and Antimicrobial Study of Dyed Silk

2016 ◽  
Vol 675-676 ◽  
pp. 19-22 ◽  
Author(s):  
Ploysai Ohama ◽  
Sirilak Namwong ◽  
Saowanee Kumpun
Keyword(s):  
Yellow Pigment ◽  
Color Fastness ◽  
Silk Fabric ◽  
Red Pigment ◽  
Light Fastness ◽  
Color Strength ◽  
Dyeing Process ◽  
Pigment Extraction ◽  
Red Color ◽  
Silk Dyeing

The extractions of yellow and red pigments from safflower petals were studied. The pigment extracted was further utilized as a natural dye for silk dyeing. The safflower petals were water-extracted in order to remove the yellow pigment and the extraction of red pigment from the petals was done with alkali solution. The extracted red pigment was applied to a silk fabric by dyeing process. The effects of dye concentration and pH of dye bath were studied. The colourimetric analysis of each dyed material was done in terms of the CIELab (L*, a* and b*) and K/S values. Maximum color strength for red color was obtained at pH 4. Color fastness to washing and light was evaluated. Washing fastness was 4-5 but light fastness for red dyed silk was 1. The dyed silk did not display antimicrobial activity against the bacteria Staphylococcus aureus ATCC25923T and Escherichia coli ATCC25922T.

Mathematical Simulation of Solid-Liquid Diffusion in Continuous Countercurrrent Extraction Process, Part II - Modeling Verification and Its Application

2010 ◽  
Vol 8 (1) ◽  
Author(s):  
Waigoon Rittirut ◽  
Chakrit Thongurai ◽  
Chairat Siripatana
Keyword(s):  
Operation Time ◽  
Extraction Process ◽  
Extraction Temperature ◽  
Liquid Ratio ◽  
Countercurrent Extraction ◽  
External Resistance ◽  
Solid Retention Time ◽  
Juice Extraction ◽  
Solid Liquid ◽  
Continuous Countercurrent Extraction

In this work, a backmixing-diffusion model was developed for continuous countercurrent extraction process. Various parameters/factors influenced the extraction were investigated for juice extraction. Important parameters/factors studied were solid to liquid ratio, solid retention time, extraction temperature, external resistance to mass transfer, size and shape of solid materials and degree of backmixing for solid and liquid phase. For juice extraction from pineapple, apple and pear, it was found that the backmixing-diffusion concept can be used through the whole range of operation time. The model could predict the concentration profile well for both unsteady state period and steady state one. The simulation was successful for juice extraction process.

Microwave Assisted Multi-Stage Countercurrent Extraction of Dihydromyricetin from Ampelopsis grossedentataa

2011 ◽  
Vol 7 (4) ◽  
Author(s):  
Wei Li ◽  
Cheng Zheng ◽  
Jian Zhao ◽  
Zhengxiang Ning
Keyword(s):  
Extraction Efficiency ◽  
Extraction Process ◽  
Extraction Time ◽  
Countercurrent Extraction ◽  
Bioactive Substances ◽  
Extraction Solvent ◽  
Microwave Assisted ◽  
Multi Stage ◽  
The Matrix ◽  
Substantial Concentration

A novel microwave assisted multi-stage countercurrent extraction (MAMCE) technique was developed for the extraction of dihydromyricetin from Chinese rattan tea, Ampelopsis grossedentata. The technique combined the advantages of microwave heating and dynamic multi-stage countercurrent extraction and achieved marked improvement in extraction efficiency over microwave assisted batch extraction. Analysis of dihydromyricetin concentrations in the solvent and matrix throughout the extraction process showed that by dividing the extraction into multiple stages and exchanging of solvents between stages, steady and substantial concentration gradients were established between the matrix and solvent, thus enabling the achievement of high extraction efficiency. The yield of dihydromyricetin was significantly affected by temperature, pH, solvent/material ratio and extraction time, and optimal extraction conditions were found to be 80-100°C, at acidic pH with a solvent/material ratio of 25-30 to 1 and extraction time of 5-10 min. With the high extraction efficiency and low usage of extraction solvent, MAMCE could prove to be a promising extraction technique which can be applied to the extraction of dihydromyricentin and other bioactive substances from natural materials.

scholarly journals Reusing wasteroot of Rubia wallichiana dyeing from Monpa of Tibet in China

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Rong Yang ◽  
Yu Zhang ◽  
Sailesh Ranjitkar ◽  
Mingxiang Li ◽  
Yongjie Guo ◽  
...  
Keyword(s):  
Cultural Values ◽  
Aqueous Extract ◽  
Ethyl Alcohol ◽  
Economic Benefits ◽  
Natural Dyes ◽  
Body Parts ◽  
Color Strength ◽  
Alcohol Extract ◽  
Dyeing Properties ◽  
Ecological Economic

AbstractHumans have dyed textiles and leather, colored food, and paint body parts using natural dyes throughout history. Natural dyes have suffered drastically due to recent socioeconomic changes and replacement with synthetic dye in the textile industry. Hence, it is urgent to study indigenous dye plants and dyeing craft in local communities to protect these resources' potential ecological, economic, and cultural values. In 11 Monpa villages of Mêdog County, South-east Tibet, China, we conducted field research to record the indigenous method of cloth dyeing using madder dye. An aqueous extract of the root of Rubia wallichiana is a traditional madder dye. In this study, we used traditional dye and ethyl alcohol extract of the residue of aqueous extract. Two fabrics were dyed with the extractions in the presence of one of the metallic mordants or biomordants. Pigment compounds from aqueous extraction of madder and ethyl alcohol extraction of recycled madder were evaluated using Phytochemical, UV–visible spectroscopy, and FTIR test. We carried out One-way ANOVA and Duncan's new multiple range method to analyze different dying approaches and conditions. The dyed fabrics were evaluated by indicators of color strength and fastness, including washing, rubbing, and perspiration. The findings revealed the potentiality of biomordants to improve the dyeing properties of madder. The dyeing properties of recycled madder were marginally better than traditional madder. The results revealed the feasibility of enhancing the dyeing property and reuse of the residue from madder dyeing. The improved dyeing and reuse of residue can improve local ecological, economic benefits, and cultural heritage while applying research findings for the subsequent commercialization of plant dyes.

Mathematical Modeling of Betanin Extraction from Red Beet (Beta vulgaris L.) by Solid–Liquid Method

2015 ◽  
Vol 11 (1) ◽  
pp. 17-22 ◽  
Author(s):  
Honggao Xu ◽  
Qiang Peng ◽  
Fang Yuan ◽  
Yanxiang Gao
Keyword(s):  
Mathematical Modeling ◽  
Effective Diffusion ◽  
Spherical Model ◽  
Extraction Process ◽  
Extraction Temperature ◽  
Optimal Parameters ◽  
Practical Application ◽  
Sulfurous Acid ◽  
Red Beet ◽  
Solid Liquid

Abstract Effective diffusion coefficient (D-value) is an important parameter for the extraction process. In this study, a cylindrical model to estimate the D-value of betanin extraction from red beet roots was developed. The influence of extraction temperature, pH, cylindrical thickness and type of acids on the D-value was also investigated. The optimal parameters of betanin extraction were 30°C, pH 4.0 adjusted with sulfurous acid or acetic acid. D-values under the above conditions were 18.95×10−11 m2/s and 17.87×10−11 m2/s, respectively. The result showed that D-value elevated with the increase of cylindrical thickness, which was consistent with earlier conclusion from spherical model. The modeling may be useful for the investigation into extraction process and practical application.

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