scholarly journals Physicochemical Properties and Bioactive Potential of a New Epoxy Resin-based Root Canal Sealer

2019 ◽  
Vol 30 (6) ◽  
pp. 563-568 ◽  
Author(s):  
Mario Tanomaru-Filho ◽  
Maiby Cristine Prado ◽  
Fernanda Ferrari Esteves Torres ◽  
Raqueli Viapiana ◽  
Mariana Mena Barreto Pivoto-João ◽  
...  
Keyword(s):  
Physicochemical Properties ◽  
Water Solubility ◽  
Setting Time ◽  
Volumetric Change ◽  
Time Flow ◽  
Before And After ◽  
Ah Plus ◽  
The Difference ◽  
Bioactive Potential ◽  
Low Solubility

Abstract The aim of this study was to evaluate physicochemical properties and bioactive potential of Sealer Plus, in comparison with MTA Fillapex, Sealapex and AH Plus. Setting time, flow, and radiopacity were evaluated based on ISO 6876 Standard. Flow was also assessed in area (mm²). The solubility and volumetric change of the sealers were evaluated after 7 and 30 days of immersion in distilled water. Solubility was evaluated by the difference in mass of materials before and after immersion. Volumetric change was evaluated by using microcomputed tomography (micro-CT). The bioactive potential was observed by Scanning Electron Microscopy (SEM) after immersion in PBS. Data were compared using ANOVA and Tukey tests (α=0.05). Sealer Plus presented the shortest setting time (196 min.) and Sealapex the longest (912 min.) (p<0.05). AH Plus showed the highest radiopacity (9.5 mm Al) and MTA Fillapex the lowest (2.7 mm Al) (p<0.05). All the sealers presented flow in accordance with ISO 6876/2012 (>17 mm). Sealer Plus showed low solubility and volumetric change (<1%), and MTA Fillapex showed the highest solubility (>25%), and volumetric change (>4%) after all time intervals (p<0.05). MTA Fillapex was the only sealer that showed bioactive potential. In conclusion, Sealer Plus presented proper physicochemical properties. However, this sealer did not present a bioactive potential.

scholarly journals Evaluation of Physicochemical Properties of New Calcium Silicate-Based Sealer

2018 ◽  
Vol 29 (6) ◽  
pp. 536-540 ◽  
Author(s):  
Aline Teixeira Mendes ◽  
Paula Barcellos da Silva ◽  
Bruna Barcelos Só ◽  
Lina Naomi Hashizume ◽  
Rodrigo Ricci Vivan ◽  
...  
Keyword(s):  
Physicochemical Properties ◽  
Calcium Ion ◽  
Calcium Silicate ◽  
Calcium Release ◽  
Setting Time ◽  
Porto Alegre ◽  
Ion Release ◽  
Ph Values ◽  
Time Flow ◽  
Ah Plus

Abstract This study aimed to evaluate the physicochemical properties of a calcium silicate-based sealer (Sealer Plus BC; MK Life, Porto Alegre, Brazil) compared with an epoxy-resin sealer (AH Plus; Dentsply DeTrey GmbH, Konstanz, Germany). Initial and final setting time was assessed based on ISO 6876:2012 and ASTM C266:03. Calcium ion release and pH were evaluated by filling polyethylene tubes with sealers and then immersing them in 10 mL of deionized water. Following experimental periods of 1, 24, 72 and 168 hours, the samples were measured regarding pH and calcium ion release with a pH meter and a colorimetric spectrophotometer, respectively. The flow was examined based on ISO 6876:2012. Rings of 10 mm in diameter with 1 mm thickness were prepared to analyze the radiopacity (ISO 6876:2012 and ADA n.57) and solubility (ISO 6876:2012). The data were analyzed by variance analysis, Student-T and Tukey tests (p<0.05). The calcium ion release and pH values were significantly higher for the Sealer Plus BC compared with the AH Plus (p<0.05). Lower setting time, flow and radiopacity were observed for the bioceramic sealer than for AH Plus (p<0.05). Sealer Plus BC exhibited higher solubility compared with AH Plus (p<0.05). Sealer Plus BC showed physicochemical properties as setting time, pH, calcium release, flow, and radiopacity following the required standards, but higher solubility than the minimum values required by ISO 6876:2012.

scholarly journals Physicochemical Properties, Cytocompatibility and Antibiofilm Activity of a New Calcium Silicate Sealer

2021 ◽  
Vol 32 (4) ◽  
pp. 8-18
Author(s):  
Cristiane Lopes Zordan-Bronzel ◽  
Mario Tanomaru-Filho ◽  
Fernanda Ferrari Esteves Torres ◽  
Gisselle Moraima Chávez-Andrade ◽  
Elisandra Marcia Rodrigues ◽  
...  
Keyword(s):  
Physicochemical Properties ◽  
Calcium Silicate ◽  
Setting Time ◽  
Neutral Red ◽  
Antibiofilm Activity ◽  
Micro Ct ◽  
Volumetric Change ◽  
Crystal Violet Assay ◽  
Ah Plus ◽  
Proper Setting

Abstract The aim of this study was to evaluate the physicochemical properties, cytocompatibility and antibiofilm activity of a new calcium silicate-based endodontic sealer, Sealer Plus BC (MK Life, Brazil), in comparison with TotalFill BC Sealer (FKG Dentaire SA, Switzerland) and AH Plus (Dentsply, Germany). Setting time and flow were evaluated based on ISO 6876 standard. The pH was evaluated after different periods, and radiopacity by radiographic analysis (mmAl). Solubility (% mass loss) and volumetric change (by micro-CT) were assessed after 30 days of immersion in distilled water. Cytocompatibility was assessed by methyltetrazolium (MTT) and neutral red (NR) assays, after exposure of Saos-2 cells to the sealer extract for 24 h. An additional analysis was performed by using MTT assay after 1, 3 and 7 days of exposure of Saos-2 to the sealers 1:8 dilution extracts. Antibiofilm activity against Enterococcus faecalis and/or Candida albicans was evaluated by crystal violet assay and modified direct contact test. The physicochemical properties were analyzed using ANOVA/Tukey tests; MTT and NR data were analyzed by ANOVA and Bonferroni tests; the antimicrobial tests were analyzed by Kruskal-Wallis and Dunn tests (α=0.05). Sealer Plus BC had proper setting time, radiopacity, flow and alkalization capacity. Sealer Plus BC was significantly more soluble than AH Plus (p<0.05) and presented volumetric change similar to AH Plus and TotalFill BC (p>0.05). Sealer Plus BC presented antibiofilm activity and no cytotoxic effect. In conclusion, although Sealer Plus BC had higher solubility, this sealer showed proper physicochemical properties, cytocompatibility, and antibiofilm activity.

scholarly journals Influence of Powder-to-Gel Ratio on Physicochemical Properties of a Calcium Silicate Sealer

2020 ◽  
pp. 337-345
Author(s):  
Fernanda F. E. Torres ◽  
Patricia Perinoto ◽  
Roberta Bosso-Martelo ◽  
Gisselle M. Chávez-Andrade ◽  
Juliane M. Guerreiro-Tanomaru ◽  
...  
Keyword(s):  
Physicochemical Properties ◽  
Calcium Silicate ◽  
Setting Time ◽  
Repair Material ◽  
Alkaline Ph ◽  
Root Canal Sealer ◽  
Work Time ◽  
Lower Solubility ◽  
Low Solubility ◽  
One Way Anova

Differences in liquid-to-powder ratio can affect the properties of calcium silicate-based materials. This study assessed the influence of powder-to-gel ratio on physicochemical properties of NeoMTA Plus. Setting time (minutes), flow (mm and mm²), pH (at different periods), radiopacity (mm Al) and solubility (% mass loss) were evaluated using the consistencies for root repair material (NMTAP-RP; 3 scoops of powder to 2 drops of gel) and root canal sealer (NMTAP-SE; 3 scoops of powder to 3 drops of gel), in comparison to Biodentine cement (BIO) and TotalFill BC sealer (TFBC). Statistical analysis was performed using one-way ANOVA and Tukey tests (α=0.05). BIO had the shortest setting time, followed by NMTAP-RP and NMTAP-SE. TFBC showed the highest setting time and radiopacity. BIO, NMTAP-RP, and NMTAP-SE had similar radiopacity. All materials promoted an alkaline pH. NMTAP-RP/SE presented lower solubility than BIO and TFBC. Regarding the flow, TFBC had the highest values, followed by NMTAP-SE, and NMTAP-RP. BIO had the lowest flow. In conclusion, NMTAP in both powder-to-gel ratios showed high pH and low solubility. The increase in the powder ratio decreased the setting time and flow. These findings are important regarding the proper consistency and work time to clinical application.

scholarly journals Physical and Biological Properties of a High-Plasticity Tricalcium Silicate Cement

2018 ◽  
Vol 2018 ◽  
pp. 1-6 ◽  
Author(s):  
Arthur Dias Galarça ◽  
Wellington Luiz de Oliveira Da Rosa ◽  
Tiago Machado Da Silva ◽  
Giana da Silveira Lima ◽  
Neftalí Lenin Villarreal Carreño ◽  
...  
Keyword(s):  
Compressive Strength ◽  
Film Thickness ◽  
Cell Viability ◽  
Water Solubility ◽  
Setting Time ◽  
Mineral Trioxide Aggregate ◽  
Biological Properties ◽  
High Plasticity ◽  
Silicate Matrix ◽  
Time Flow

Introduction. Mineral Trioxide Aggregate (MTA) is a tricalcium-based silicate, dicalcium silicate matrix. Despite its good biologic properties, some clinicians still claim to have difficulties in handling MTA after its preparation due to its sandy consistency. The aim of the present study was to evaluate the physicochemical properties and cytotoxicity of MTA Repair HP (Angelus, Londrina, PR, Brazil) compared with MTA Angelus (Angelus, Londrina, PR, Brazil). Materials and Method. The properties assessed were particle size, setting time, flow, film thickness, radiopacity, water solubility, compressive strength, and cytotoxicity. Statistical analysis was performed considering p < 0.05 as statistically significant. Results. For radiopacity, water absorption and solubility MTA Repair HP were statistically similar to MTA Angelus. The MTA Angelus had statistically different film thickness values, higher than MTA Repair HP (p < 0.05). Besides, MTA Angelus showed a lower and statistically different compressive strength after 28 days than MTA Repair HP (p<0.05). Additionally, MTA Repair HP set more slowly (p < 0.05). Relative to cell viability, MTA Repair HP was statistically similar to MTA Angelus after 24 and 48 h in cell viability. Conclusions. The MTA Repair HP presented similar cell viability, lower film thickness, higher flow, setting time, and compressive strength values after 28 days than MTA Angelus. In general, the MTA Repair HP presented physicochemical and biological properties similar to the MTA Angelus.

scholarly journals Solubility of Calcium Silicate Based Cements – a Comparative Study

2020 ◽  
Vol 47 (2) ◽  
pp. 27-29
Author(s):  
Y. Kouzmanova ◽  
I. Dimitrova
Keyword(s):  
Treatment Failure ◽  
Physicochemical Properties ◽  
Calcium Silicate ◽  
Mineral Trioxide Aggregate ◽  
Distilled Water ◽  
Tissue Fluid ◽  
Before And After ◽  
Calcium Silicate Cements ◽  
Low Solubility ◽  
As Solubility

AbstractCalcium silicate based cement is a group of biomaterials, based on Portland cement. Its physicochemical properties such as solubility are of the utmost importance. It should have low solubility in tissue fluid since the dissolution of materials may lead to treatment failure.The aim of this study is to evaluate the solubility of five calcium silicate cements after being placed in distilled water for a period of 28 days.Material and methods: The purpose of this study was to compare solubility of a four new calcium silicate-based cements, such as: gray MTA Angelus; white MTA Angelus; BioAggregate and Biodentine with conventional mineral trioxide aggregate White ProRoot. Solubility is evaluated using standardized samples of materials, which are weighed before and after 28-day immersion in distilled water.Results: The lowest solubility is found at White ProRoot and the significantly highest solubility – at Biodentine.

scholarly journals Effect of Different Dimensions of Test Samples on the Volumetric Change Assessment Of Endodontic Materials

2021 ◽  
Vol 32 (1) ◽  
pp. 42-47
Author(s):  
Fernanda Ferrari Esteves Torres ◽  
Juliane Maria Guerreiro-Tanomaru ◽  
Jader Camilo Pinto ◽  
Mario Tanomaru-Filho
Keyword(s):  
Morphological Changes ◽  
Micro Ct ◽  
Volume Loss ◽  
Micro Computed Tomography ◽  
Volumetric Change ◽  
Before And After ◽  
Different Dimensions ◽  
The Difference ◽  
The Stability ◽  
Different Diameters

Abstract New methodologies using micro-CT to evaluate solubility besides dimensional and morphological changes of endodontic materials are proposed. However, there is no standardization in the methods. The aim of this study was to assess the effect of different dimensions of test samples on volumetric change evaluation of different endodontic materials. AH Plus, FillCanal and Sealapex root canal sealers, Biodentine, IRM and MTA root-end filling cements were used in the tests. Samples of each material with a thickness of 1.5 mm and different diameters were manufactured: 6.3, 7.75, and 9.0 mm. The samples were scanned in micro-computed tomography (micro-CT) after setting and after 7 days of immersion in distilled water. The volumetric change was evaluated by means of the difference in the total volume of the specimens before and after immersion. Data were submitted to ANOVA and Tukey tests (p<0.05). The size of the samples did not affect the percentage of volumetric change of the materials (p>0.05). All sample sizes had greater volume loss for Sealapex among the sealers and Biodentine for the cements (p<0.05). In conclusion, Biodentine and Sealapex had the highest volume loss after immersion. Samples with 1.5 mm thickness, and diameters ranging between 6.3 and 9.0 mm can be used to assess the stability of endodontic materials using micro-CT without affecting the percentage of volumetric change.

scholarly journals Impact of Water Solubility on Chemical Composition and Surface Structure of Two Generations of Bioceramic Root Canal Sealers

2022 ◽  
Vol 12 (2) ◽  
pp. 873
Author(s):  
Sawsan T. Abu Abu Zeid ◽  
Ruaa A. Alamoudi ◽  
Abeer A. Mokeem Mokeem Saleh
Keyword(s):  
Surface Structure ◽  
Root Canal ◽  
Water Solubility ◽  
Setting Time ◽  
Chemical Properties ◽  
Solubility Test ◽  
Setting Times ◽  
Before And After ◽  
Two Generations ◽  
Root Canal Sealers

Aimed to evaluate the effect of water solubility on chemical properties and surface structure of bioceramic-based (BC-HiFlow and BC-EndoSeqence) compared with resin-based (Adseal) root canal sealers. Fresh mix was inserted into polyethylene mold (n = 10) and subjected to Vicat needle to evaluate the setting time. The set discs were analyzed by Fourier transform infrared (FTIR) spectroscopy then immersed in deionized water for 1, 7, 14 and 28 days. The solubility%, pH changes, released calcium (Ca2+), phosphate (PO43−) and silicon (Si4+) ions were evaluated after each immersion period. The discs were analyzed by scanning electron microscopy/Energy dispersed X-ray (SEM/EDX) before and after solubility test. Although FTIR detected similar composition of both bioceramic-sealers, BC-EndoSequence determined the prolonged setting times. At the end of solubility test, both bioceramic-sealers exhibited significant greater solubility (>3%), alkaline pH (>11) at p < 0.001. Adseal displayed the significant greatest Ca2+ and PO43− released, while BC-HiFlow displayed the significant greatest Si4+ release (p < 0.001). SEM revealed voids and pores on the surface of all tested sealers with the greatest value on Adseal surface. In conclusion, although both bioceramic-sealers had high solubility, BC-Hiflow complied the ISO standard regarding setting time and least surface micropores better than that of BC-EndoSequence.

scholarly journals Physicochemical Properties of Epoxy Resin-Based and Bioceramic-Based Root Canal Sealers

2017 ◽  
Vol 2017 ◽  
pp. 1-8 ◽  
Author(s):  
Ju Kyung Lee ◽  
Sang Won Kwak ◽  
Jung-Hong Ha ◽  
WooCheol Lee ◽  
Hyeon-Cheol Kim
Keyword(s):  
Physicochemical Properties ◽  
Epoxy Resin ◽  
Setting Time ◽  
Alkaline Ph ◽  
Ph Change ◽  
Ah Plus ◽  
The One ◽  
Post Hoc ◽  
Root Canal Sealers ◽  
One Way Anova

Three bioceramic sealers (EndoSequence BC sealer, EndoSeal MTA, and MTA Fillapex) and three epoxy resin-based sealers (AH-Plus, AD Seal, and Radic-Sealer) were tested to evaluate the physicochemical properties: flow, final setting time, radiopacity, dimensional stability, and pH change. The one-way ANOVA and Tukey’s post hoc test were used to analyze the data (P=0.05). The MTA Fillapex sealer had a highest flow and the BC Sealer presented a flow significantly lower than the others (P<0.05). The BC Sealer and MTA Fillapex samples were not set in humid incubator condition even after one month. EndoSeal MTA had the longest setting time among the measurable materials and Radic-Sealer and AD Seal showed shorter setting time than the AH-Plus (P<0.05). AH-Plus and EndoSeal MTA showed statistically higher values and MTA Fillapex showed statistically lower radiopacity (P<0.05). BC Sealer showed the highest alkaline pH in all evaluation periods. Set samples of 3 epoxy resin-based sealers and EndoSeal MTA presented a significant increase of pH over experimental time for 4 weeks. In conclusion, the bioceramic sealer and epoxy resin-based sealers showed clinical acceptable physicochemical properties, but BC Sealer and MTA Fillapex were not set completely.

scholarly journals Supercritical Fluid Extraction of Fat and Caffeine with Theobromine Retention in the Cocoa Shell

Processes ◽  
2019 ◽  
Vol 7 (6) ◽  
pp. 385 ◽  
Author(s):  
Fanny Adabel González-Alejo ◽  
Juan Barajas-Fernández ◽  
María de los Ángeles Olán-Acosta ◽  
Laura Mercedes Lagunes-Gálvez ◽  
Pedro García-Alamilla
Keyword(s):  
Removal Rate ◽  
Added Value ◽  
23 Factorial Design ◽  
Extraction Behavior ◽  
Before And After ◽  
Dynamic Extraction ◽  
Ft Ir ◽  
Cocoa Shell ◽  
The Difference ◽  
Low Solubility

The cocoa shell is a residue of low commercial value, which represents an alternative for obtaining substances of added value for the food and pharmaceutical industry. Substances of interest in the shell include fat and methylxanthines (theobromine and caffeine). In order to obtain the extraction behavior with supercritical CO2, a 23 factorial design was proposed with six central points, taking dynamic extraction into consideration. The following factors were involved: pressure (2,000–6,000 psi), temperature (313–333 K), and time (30–90 min). The obtained yield was between 3.66% and 15.30%. Fat was the substance that was extracted most effectively (94.73%). Caffeine demonstrated variability in the residue, with at least six treatments that exceeded a removal rate of more than 90%, while it was practically impossible to extract theobromine. The difference with regard to the extraction of theobromine may be attributed to its low solubility. Characterization using FT–IR showed the modifications before and after the process, providing clear evidence of the changes corresponding to the fat at 2,924, 2,854 and 1,745 cm−1. The results presented establish the basis for the extraction of substances such as fats and methylxanthines from a cocoa shell with the use of CO2.

scholarly journals Solubility, Porosity, Dimensional and Volumetric Change of Endodontic Sealers

2019 ◽  
Vol 30 (4) ◽  
pp. 368-373 ◽  
Author(s):  
Fernanda Ferrari Esteves Torres ◽  
Juliane Maria Guerreiro-Tanomaru ◽  
Roberta Bosso-Martelo ◽  
Camila Galletti Espir ◽  
Josette Camilleri ◽  
...  
Keyword(s):  
Physical Properties ◽  
Dimensional Stability ◽  
Water Solubility ◽  
Total Porosity ◽  
Distilled Water ◽  
Micro Ct ◽  
Volumetric Change ◽  
Significance Level ◽  
Ah Plus ◽  
Endodontic Sealers

Abstract The aim of this study was to evaluate physical properties of endodontic sealers (AH Plus, MTA Fillapex and Endofill), by conventional and micro-CT tests. Dimensional stability was evaluated after immersion of materials in distilled water for 30 days. Solubility and volumetric change were evaluated after 7 and 30 days of immersion in distilled water. Solubility was evaluated by means of mass loss and volumetric change was assessed by micro-CT. Porosity was evaluated under a microscope after 7 days of immersion in distilled water, and by using micro-CT after setting and immersion in distilled water for 7 and 30 days. Statistical analysis was performed by ANOVA and Tukey’s test with 5% significance level. MTA Fillapex presented the highest solubility (p<0.05), showing values above the ISO/ADA recommendations. MTA Fillapex presented higher volumetric and dimensional changes, followed by Endofill and AH Plus (p<0.05). Dimensional stability of the MTA Fillapex and AH Plus did not follow ISO/ADA standards. The highest total porosity was observed for MTA Fillapex (p<0.05). Endofill had higher total porosity than AH Plus according to microscope evaluation (p<0,05), and both sealers were similar in micro-CT assessment (p>0,05). In conclusion, MTA Fillapex presented higher solubility, dimensional and volumetric change besides porosity compared to the other evaluated sealers. The assessed physical properties of sealers are related, and the different tests provided complementary data. Micro-CT is a valuable method for assessment of physical properties of endodontic materials.

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