scholarly journals Effects of Heat Treatment on Morphology, Texture and Mechanical Properties of a MnSiAl Multiphase Steel with TRIP Behavior

2018 ◽  
Author(s):  
Alvaro Salinas ◽  
Alfredo Artigas ◽  
Juan Pérez-Ipiña ◽  
Felipe M. Castro-Cerda ◽  
Nelson F. Garza-Montes-de-Oca ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Retained Austenite ◽  
Room Temperature ◽  
Single Phase ◽  
Intercritical Annealing ◽  
Tensile Tests ◽  
Temperature Homogenization ◽  
Cold Rolled ◽  
Multiphase Steel

: The effect that the microstructure exerts on the TRIP phenomenon and on the mechanical properties in a multiphase steel was studied. Samples of an initially cold-rolled ferrite-pearlite steel underwent different intercritical annealing treatments at 750 °C until an equal fractions of austenite/ferrite was reached; the intercritical treatment was followed by isothermal bainitic treatments before cooling the samples to room temperature. Samples in the first treatment were heated  directly to the intercritical temperature, whereas other samples were heated to either 900 or 1100 °C to obtain a fully homogenized, single phase austenitic microstructure prior to the conducting the intercritical treatment. The high temperature homogenization of austenite resulted in the decrease in its stability, so a considerable austenite fraction transformed into martensite by cooling to room temperature after the bainitic heat treatment. Most of the retained austenite transformed during the tensile tests, and as a consequence, the previously homogenized steels showed the highest UTS. In turn, the steel with a ferritic-pearlitic initial microstructure, exhibited higher ductility than the other steels and texture components that favor forming processes.     

scholarly journals Effects of Heat Treatment on Morphology, Texture, and Mechanical Properties of a MnSiAl Multiphase Steel with TRIP Behavior

Metals ◽  
2018 ◽  
Vol 8 (12) ◽  
pp. 1021 ◽  
Author(s):  
Alvaro Salinas ◽  
Alfredo Artigas ◽  
Juan Perez-Ipiña ◽  
Felipe Castro-Cerda ◽  
Nelson Garza-Montes-de-Oca ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Room Temperature ◽  
Single Phase ◽  
Intercritical Annealing ◽  
Tensile Tests ◽  
Transformation Induced Plasticity ◽  
Temperature Homogenization ◽  
Cold Rolled ◽  
Multiphase Steel

The effect that the microstructure exerts on the Transformation-Induced Plasticity (TRIP) phenomenon and on the mechanical properties in a multiphase steel was studied. Samples of an initially cold-rolled ferrite–pearlite steel underwent different intercritical annealing treatments at 750 °C until equal fractions of austenite/ferrite were reached; the intercritical treatment was followed by isothermal bainitic treatments before cooling the samples to room temperature. Samples in the first treatment were heated directly to the intercritical temperature, whereas other samples were heated to either 900 °C or 1100 °C to obtain a fully homogenized, single-phase austenitic microstructure before performing the intercritical treatment. The high-temperature homogenization of austenite resulted in a decrease in its stability, so a considerable austenite fraction transformed into martensite by cooling to room temperature after the bainitic heat treatment. Most of the retained austenite transformed during the tensile tests, and, consequently, the previously homogenized steels showed the highest Ultimate Tensile Strength (UTS). In turn, the steel with a ferritic–pearlitic initial microstructure exhibited higher ductility than the other steels and texture components that favor forming processes.

Influence of Heat Treatment on Microstructure and Mechanical Properties of Selective Laser Melted TiAl6V4 Alloy

2018 ◽  
Vol 284 ◽  
pp. 615-620 ◽  
Author(s):  
R.M. Baitimerov ◽  
P.A. Lykov ◽  
L.V. Radionova
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Selective Laser Melting ◽  
Room Temperature ◽  
Base Alloy ◽  
Tensile Tests ◽  
Heat Treatments ◽  
Laser Melting ◽  
Microstructure And Mechanical Properties ◽  
Treatment Procedures

TiAl6V4 titanium base alloy is widely used in aerospace and medical industries. Specimens for tensile tests from TiAl6V4 with porosity less than 0.5% was fabricated by selective laser melting (SLM). Specimens were treated using two heat treatment procedures, third batch of specimens was tested in as-fabricated statement after machining. Tensile tests were carried out at room temperature. Microstructure and mechanical properties of SLM fabricated TiAl6V4 after different heat treatments were investigated.

Effect of Intercritical Annealing Time on Microstructure and Mechanical Behavior of Advanced Medium Mn Steels

2012 ◽  
Vol 706-709 ◽  
pp. 2693-2698 ◽  
Author(s):  
A. Arlazarov ◽  
M. Gouné ◽  
O. Bouaziz ◽  
A. Hazotte ◽  
F. Kegel
Keyword(s):  
Mechanical Behavior ◽  
Annealing Time ◽  
Room Temperature ◽  
Intercritical Annealing ◽  
Tensile Tests ◽  
The Other ◽  
Metastable Austenite ◽  
High Fraction ◽  
Cold Rolled ◽  
Strength And Ductility

The study about the influence of intercritical annealing time on a cold rolled 0.1%C – 4.6%Mn (wt.%) steel was performed. The tensile tests show an interesting balance between strength and ductility especially after 7 hours annealing at 670°C. A part of this good result can be explained by the presence of rather high fraction of metastable austenite at room temperature. On the other hand a very complex microstructure combining lath-like and polygonal features was observed making the interpretation complicated.

scholarly journals The Impact of Retained Austenite on the Mechanical Properties of Bainitic and Dual Phase Steels

2022 ◽  
Author(s):  
Bogusława Adamczyk-Cieślak ◽  
Milena Koralnik ◽  
Roman Kuziak ◽  
Kamil Majchrowicz ◽  
Tomasz Zygmunt ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Transformation Temperature ◽  
Retained Austenite ◽  
Tensile Tests ◽  
Total Elongation ◽  
Isothermal Transformation ◽  
Bainitic Transformation ◽  
Bainitic Steel ◽  
Continuous Cooling

AbstractThis paper presents the microstructural changes and mechanical properties of carbide-free bainitic steel subjected to various heat treatment processes and compares these results with similarly treated ferritic–pearlitic steel. A key feature of the investigated steel, which is common among others described in the literature, is that the Si content in the developed steel was >1 wt.% to avoid carbide precipitation in the retained austenite during the bainitic transformation. The phase identification before and after various heat treatment conditions was carried out based on microstructural observations and x-ray diffraction. Hardness measurements and tensile tests were conducted to determine the mechanical properties of the investigated materials. In addition, following the tensile tests, the fracture surfaces of both types of steels were analyzed. Changing the bainitic transformation temperature generated distinct volume fractions of retained austenite and different values of mechanical strength properties. The mechanical properties of the examined steels were strongly influenced by the volume fractions and morphological features of the microstructural constituents. It is worth noting that the bainitic steel was characterized by a high ultimate tensile strength (1250 MPa) combined with a total elongation of 18% after austenitizing and continuous cooling. The chemical composition of the bainitic steel was designed to obtain the optimal microstructure and mechanical properties after hot deformation followed by natural cooling in still air. Extensive tests using isothermal transformation to bainite were conducted to understand the relationships between transformation temperature and the resulting microstructures, mechanical properties, and fracture characteristics. The isothermal transformation tests indicated that the optimal relationship between the sample strength and total elongation was obtained after bainitic treatment at 400 °C. However, it should be noted that the mechanical properties and total elongation of the bainitic steel after continuous cooling differed little from the condition after isothermal transformation at 400 °C.

scholarly journals The Effect of Pre-Annealing on the Evolution of the Microstructure and Mechanical Behavior of Aluminum Processed by a Novel SPD Method

Materials ◽  
2020 ◽  
Vol 13 (10) ◽  
pp. 2361 ◽  
Author(s):  
Alexander P. Zhilyaev ◽  
Mario J. Torres ◽  
Homero D. Cadena ◽  
Sandra L. Rodriguez ◽  
Jessica Calvo ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Grain Size ◽  
High Temperature ◽  
Room Temperature ◽  
Pure Aluminum ◽  
Continuous Process ◽  
Tensile Tests ◽  
New Method ◽  
Slow Cooling

A novel continuous process of severe plastic deformation (SPD) named continuous close die forging (CCDF) is presented. The CCDF process combines all favorite advances of multidirectional forging and other SPD methods, and it can be easily scaled up for industrial use. Keeping constant both the cross section and the length of the sample, the new method promotes a refinement of the microstructure. The grain refinement and mechanical properties of commercially pure aluminum (AA1050) were studied as a function of the number of CCDF repetitive passes and the previous conditioning heat treatment. In particular, two different pre-annealing treatments were applied. The first one consisted of a reheating to 623 K (350 °C) for 1 h aimed at eliminating the effect of the deformation applied during the bar extrusion. The second pre-annealing consisted on a reheating to 903 K (630 °C) for 48 h plus cooling down to 573 K (300 °C) at 66 K/h. At this latter temperature, the material remained for 3 h prior to a final cooling to room temperature within the furnace, i.e., slow cooling rate. This treatment aimed at increasing the elongation and formability of the material. No visible cracking was detected in the workpiece of AA1050 processed up to 16 passes at room temperature after the first conditioning heat treatment, and 24 passes were able to be applied when the material was subjected to the second heat treatment. After processing through 16 passes for the low temperature pre-annealed samples, the microstructure was refined down to a mean grain size of 0.82 µm and the grain size was further reduced to 0.72 µm after 24 passes, applied after the high temperature heat treatment. Tensile tests showed the best mechanical properties after the high temperature pre-annealing and 24 passes of the novel CCDF method. A yield strength and ultimate tensile strength of 180 and 226 MPa, respectively, were obtained. Elongation to fracture was 18%. The microstructure and grain boundary nature are discussed in relation to the mechanical properties attained by the current ultrafine-grained (UFG) AA1050 processed by this new method.

Study on the Mechanical Stability of Retained Austenite in Cold-Rolled Medium-Mn Steel

2014 ◽  
Vol 936 ◽  
pp. 1283-1289
Author(s):  
Jun Hu ◽  
Wen Quan Cao ◽  
Jie Shi ◽  
Han Dong
Keyword(s):  
Mechanical Properties ◽  
Retained Austenite ◽  
Mechanical Stability ◽  
Volume Fraction ◽  
Residual Austenite ◽  
Tensile Tests ◽  
Medium Mn Steel ◽  
Cold Rolled ◽  
Mn Steel ◽  
High Mechanical Stability

The mechanical stability of the retained austenite in the cold-rolled medium-Mn steel was studied. Tensile tests were carried out to measure the mechanical properties of the annealed steel. Scanning electron microscopy was applied to characterize the microstructure evolution during the tensile process; X-ray diffraction analysis was used to determine the residual austenite content in the deformed steel. It was found that the volume fraction of retained austenite gradually decreases with strain .The value of the stability coefficient of retained austenite k was small in the test steel, which indicated high mechanical stability of retained austenite. Due to TRIP effect, the high mechanical stability of the retained austenite strongly delays the onset of necking, which resulted in good comprehensive mechanical properties with ultrahigh strength and plasticity.

scholarly journals On the Q&P Potential of a Commercial Spring Steel

Metals ◽  
2021 ◽  
Vol 11 (10) ◽  
pp. 1612
Author(s):  
Markus Härtel ◽  
Alisa Wilke ◽  
Sebastian Dieck ◽  
Pierre Landgraf ◽  
Thomas Grund ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Electron Backscatter Diffraction ◽  
Tensile Tests ◽  
Spring Steel ◽  
Process Window ◽  
Compression Tests ◽  
Process Step

Over the last years heat treatment concept of “quenching and partitioning” (Q&P) has reached popularity for its ability to precisely adjust material properties to desired values. Mostly, Q&P process are applied on tailor-made materials with high purities or prototype alloys. The research in hand presents the whole routine of how to investigate the potential of a commercial 0.54C-1.45Si-0.71Mn spring steel in terms of Q&P heat treatment from lab scale in dilatometer measurements to widely used inductive heat treatment on larger scale. In order to obtain the small process window for this material we were focusing on the interplay of the formed microstructure and the resulting mechanical properties in hardness measurements, compression tests as well as tensile tests. After full austenitizing, three different Q&P processing routes were applied. Microstructural analyses by optical microscopy, Scanning Electron Microscopy (SEM) and Electron Backscatter Diffraction (EBSD) exhibit a condition with 6.4 % and 15 % volume fraction of fine distributed retained austenite. Interestingly, the 15 % of retained austenite developed during the partitioning heat treatment. Contradictory to our expectations, tensile and compression testing were showing that the 6.4 % condition achieved improved mechanical properties compared to the 15 % retained austenite condition. The remarkable conclusion is that not only volume fraction and fine distribution of retained austenite determines the potential of improving mechanical properties by Q&P in commercial alloys: also the process step when the retained austenite is developing as well as occurring parallel formation of carbides may strongly influence this potential.

The Effects of Intercritical Annealing Temperature and Initial Microstructure on the Stability of Retained Austenite in a 0.1C-6Mn Steel

2016 ◽  
Vol 879 ◽  
pp. 1847-1852 ◽  
Author(s):  
Katharina Steineder ◽  
Daniel Krizan ◽  
Reinhold Schneider ◽  
Coline Beal ◽  
Christof Sommitsch
Keyword(s):  
Mechanical Properties ◽  
Retained Austenite ◽  
Annealing Temperature ◽  
Intercritical Annealing ◽  
Strong Dependence ◽  
Tensile Tests ◽  
Initial Microstructure ◽  
Intercritical Annealing Temperature ◽  
Batch Annealing ◽  
The Stability

The effects of the intercritical annealing temperature and initial microstructure on the stability of retained austenite were investigated for a 0.1C-6Mn (wt-%) steel. Medium-Mn transformation-induced plasticity (TRIP) steels exhibit a strong dependence of their mechanical properties on the variation of intercritical annealing temperature. This behavior is strongly linked to the amount and stability of the retained austenite. Thus, interrupted tensile tests were used to examine the effect of annealing temperature on the stabilization of the retained austenite. Detailed microstructural investigations were employed to elaborate the effects of its chemical and mechanical stabilization. Furthermore, the final microstructure was varied by applying the batch annealing step to an initial non-deformed and deformed microstructure respectively. Retained austenite stability along with resulting mechanical properties of the investigated medium-Mn TRIP steel was significantly influenced as the amount and morphology of the respective phases altered as a consequence of both initial microstructure and applied intercritical annealing temperature.

A research on the effect of retrogression and re-aging heat treatment on hot tensile properties of AA7075 aluminum alloys

2021 ◽  
pp. 1-23
Author(s):  
Talha Sunar ◽  
Dursun Ozyurek
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Ductile Fracture ◽  
Room Temperature ◽  
Elevated Temperatures ◽  
Xrd Analysis ◽  
Tensile Tests ◽  
Heat Treatments ◽  
Tensile Behaviour ◽  
Heat Treated

Abstract Aluminium alloys are preferred in most industries due to the functional properties they provide. It is known that alloys that can be processed with heat treatments shows better mechanical properties. 7xxx series alloys can be processed vi heat treatments and are often used in environmental conditions such as extreme temperatures and corrosive environments. Corrosive sensitivities such as stress corrosion cracking (SCC) can be observed with the effect of working conditions. It is known that retrogression and re-aging (RRA) heat treatment provide corrosion resistance and decrease the SCC velocity. The purpose of this study is to examine the tensile behaviour of annealed and retrogression-re-aging (RRA) heat treated AA7075 alloys at elevated temperatures. The mechanical properties of the alloys were investigated by conducting tensile tests at room temperature (RT), 100, 200, and 300°C. Hardness tests were performed at room temperature on the samples which were taken from tensile test specimens after tensile tests. The potential effects of test temperature on mechanical and microstructural properties were examined. The annealed and RRA heat treated alloys were characterized by scanning electron microscope (SEM), and X-ray diffraction (XRD) analysis. As a result, an increase in strength and hardness of the RRA treated AA7075 alloys was observed. Ductility of the RRA alloy was lower compared to the annealed AA7075 alloy. Fracture surface examinations showed that there was a semi-ductile fracture below 200°C and ductile fracture at temperatures of 200 and 300°C. Ductility was observed to increase with increasing temperature.

Research on Substitution of Molybdenum by Manganese in Low Alloyed Bainite Ductile Iron

2011 ◽  
Vol 299-300 ◽  
pp. 57-60
Author(s):  
De Qiang Wei ◽  
Ke Liu
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Electron Microscope ◽  
Impact Toughness ◽  
Ductile Iron ◽  
Retained Austenite ◽  
Room Temperature ◽  
The Matrix ◽  
The Impact ◽  
Scanning Electron

The low alloyed bainite ductile iron is obtained by alloying and austempering in room-temperature machine oil. The microstructure is investigated. The mechanical properties are discussed. In general, the number of white-bright zones and segregation is increasing with the increasing in the content of Mn, but the impact toughness is decreased. Therefore, the content of Mn is no more than 0.5 wt.%. The microstructure of bainite, martensite and a little retained austenite in the matrix of the ductile iron was investigated by scanning electron microscope (SEM). The hardness and impact toughness of the ductile iron subjected to heat-treatment are 54~56 HRC and 14.2 J/cm2, respectively. The substitution of 0.3~0.5wt.% Mo by 0.7~1.0 wt.% Mn can be realized in the bainite ductile iron.

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