scholarly journals The Effect of Solution Treatment on Mechanical Properties and Micro Structure of Zr-10Ti-Sn Alloy for Screw Dental Implant Application

2021 ◽  
Vol 2 (2) ◽  
pp. 91
Author(s):  
Deva Ayu Utami ◽  
R. Henny Mulyani ◽  
Djoko Hadi Prajitno
Keyword(s):  
Mechanical Properties ◽  
Corrosion Resistance ◽  
Dental Implant ◽  
Solution Treatment ◽  
Hardness Test ◽  
Alpha Phase ◽  
X Ray Diffraction ◽  
X Ray ◽  
Good Corrosion Resistance ◽  
Low Modulus

<p>The research was to investigate the effect of solution treatment on the mechanical properties and microstructure of Zr-10Ti-Sn alloy for dental implant biomaterials. The addition of titanium as a material has good corrosion resistance and stannum as a material has a low modulus young and can increase hardness of the alloy in accordance with the material criteria as a dental implant, which must have good corrosion resistance and good mechanical properties. Zr -10Ti-xSn alloy (x = 0, 2, and 4% wt) were subjected to solution treatment with temperature variations of 900<sup>o</sup>C, 1000<sup>o</sup>C and 1100<sup>o</sup>C with water quenching. The results  is increase in stannum content can also increase the hardness because stannum can inhibit the enlargement of grain boundaries and the microstructure is more homogeneous and tends to be smaller with an uniaxial shape. Stannum as alpha stabilizer will form a hard alpha phase. Micro Vickers hardness test with the highest hardness value of 601,438 HV alloy Zr-10Ti-2Sn with 900<sup>o</sup>C solution treatment, phases formed were α-Zr and β-Zr and intermetallic Zr<sub>4</sub>Sn and SnTi<sub>3</sub> Zr-10Ti-4Sn alloys which were identified using X-Ray Diffraction (XRD).</p>

Laser Cladding of Zr55Al10Ni5Cu30/SiC Amorphous Composite Coatings on AZ91D Magnesium Alloy for Improvement of Corrosion Resistance

2011 ◽  
Vol 179-180 ◽  
pp. 757-761 ◽  
Author(s):  
Kai Jin Huang ◽  
Hou Guang Liu ◽  
Chang Rong Zhou
Keyword(s):  
Corrosion Resistance ◽  
Magnesium Alloy ◽  
Laser Cladding ◽  
Composite Coatings ◽  
Corrosion Property ◽  
Nacl Solution ◽  
X Ray Diffraction ◽  
X Ray ◽  
Good Corrosion Resistance ◽  
Az91d Magnesium Alloy

To improve the corrosion property of magnesium alloys, Zr-based amorphous composite coatings have been fabricated on AZ91D magnesium alloy by laser cladding using mixed powders Zr55Al10Ni5Cu30/SiC. The microstructure of the coating was characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The corrosion resistance of the coatings was tested in 3.5wt.% NaCl solution. The results show that the coatings mainly consist of amorphous and different crystalline phases. The coatings compared with AZ91D magnesium alloy exhibit good corrosion resistance because of the presence of the amorphous phase in the coatings.

Measurement of Alloying Degree of Galvannealed Steels by X-Ray Diffraction

2006 ◽  
Vol 321-323 ◽  
pp. 1461-1464 ◽  
Author(s):  
Hyoung Kuk Park ◽  
Jea Hwa Hong ◽  
Chong Soo Lee
Keyword(s):  
Mechanical Properties ◽  
Corrosion Resistance ◽  
Quantitative Analysis ◽  
Xrd Analysis ◽  
Pls Regression ◽  
Processing Conditions ◽  
X Ray Diffraction ◽  
X Ray ◽  
Excellent Corrosion Resistance ◽  
Galvannealed Steel

Galvannealed steels are produced by reheating of Zinc-coated steels, in which the iron and the zinc are interdiffused to form Zn-Fe intermatallic compound. In recent years, application of galvannealed steel has increased due to its excellent corrosion resistance, good weldability and paintability. Galvannealed production requires strict control of processing conditions to obtain an optimal alloying degree in the coatings. The analysis of the alloying degree is very important since they are closely related to the corrosion and mechanical properties. This study is measurement of alloying degree of the galvannealed steel by using the XRD. Partial least squares (PLS) model is a powerful multivariate tool that has been successfully applied to the quantitative analysis of data in XRD. The alloying degree was determined by using PLS regression to a concentration accuracy of 0.2%. The XRD analysis and proposed PLS model can be successfully used to determine the alloying degree of industrially produced galvannealed steel.

scholarly journals Effects of TiO2/SiO2 Reinforced Nanoparticles on the Mechanical Properties of Green Hybrid Coating

2015 ◽  
Vol 47 ◽  
pp. 56-66 ◽  
Author(s):  
Mohammed Gobara
Keyword(s):  
Mechanical Properties ◽  
Sol Gel ◽  
Hardness Test ◽  
Silica Sol ◽  
X Ray Diffraction ◽  
Properties Of Coatings ◽  
X Ray ◽  
Hybrid Silica ◽  
Transmission Electron ◽  
Adhesion Performance

Titanium and silica oxides nanoparticles were introduced into hybrid silica sol–gel/epoxy coating to enhance the mechanical properties of coatings. Titanium dioxide (TiO2) and silica oxide (SiO2) were chemically synthesised before adding to the prepared silica sol gel coating. X-ray diffraction (XRD), Energy-dispersive x-ray analysis (EDX) and Transmission Electron microscope (TEM) were used to characterize the prepared nanoparticles. The coating was then applied to 3003 aluminium alloy (AA3003) surface. The adhesion performance of different sol gel coating compositions was investigated using shear test to define the influence of nanoparticles on adhesive strength of the coating. The Rockwell C hardness test was used to study the micro-hardness of different compositions of sol gel coating. Also, contact angel was used to investigate the hydrophobicity of the coatings. The results showed that there was a significant improvement of the adhesion performance of hybrid silica sol gel coating due to addition of TiO2 and the hydrophobicity of sol gel coating was increased due to addition of SiO2 nanoparticles.

The Effect of RE and Ca on Corrosion Resistance of AZ91

2005 ◽  
Vol 488-489 ◽  
pp. 869-872 ◽  
Author(s):  
Yu Fan ◽  
Guo Hua Wu ◽  
Hong Tao Gao ◽  
Chun Quan Zhai
Keyword(s):  
Mechanical Properties ◽  
Corrosion Resistance ◽  
Corrosion Rate ◽  
Testing Machine ◽  
X Ray Diffraction ◽  
X Ray ◽  
Effective Barrier ◽  
Mechanical Properties And Corrosion ◽  
Universal Material Testing Machine ◽  
Material Testing Machine

The effects of RE and Ca on the mechanical properties and corrosion behavior of AZ91 have been studied by Zwick electronic universal material testing machine, X-ray diffraction, corrosion test and polarization experiment. The results showed that the addition of RE and Ca could improve the mechanical properties and corrosion resistance of AZ91 alloys. The ultimate tensile strength of AZ91 with addition of 1%RE and 1%Ca increased by 15.9%. The addition of 1%RE in AZ91 made the corrosion rate decrease from 0.453mg·cm-2·d-1 to 0.178mg·cm-2·d-1. Furthermore, with adding 1%Ca in AZ91+1%RE, the corrosion rate of AZ91 decreased to 0.086mg·cm-2·d-1 due to the formation of reticular Al2Ca phases, which acts as an effective barrier against corrosion.

Laser Cladding of Mg65Cu25Y10/SiC Amorphous Composite Coatings on AZ91D Magnesium Alloy for Improvement of Corrosion Resistance

2010 ◽  
Vol 143-144 ◽  
pp. 758-762
Author(s):  
Kai Jin Huang ◽  
Hou Guang Liu ◽  
Chang Rong Zhou
Keyword(s):  
Corrosion Resistance ◽  
Magnesium Alloy ◽  
Laser Cladding ◽  
Composite Coatings ◽  
Corrosion Property ◽  
Nacl Solution ◽  
X Ray Diffraction ◽  
X Ray ◽  
Good Corrosion Resistance ◽  
Az91d Magnesium Alloy

To improve the corrosion property of magnesium alloys, Mg-based amorphous composite coatings have been fabricated on AZ91D magnesium alloy by laser cladding using mixed powders Mg65Cu25Y10/SiC. The microstructure of the coating was characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The corrosion resistance of the coatings was tested in 3.5wt.% NaCl solution. The results show that the coatings mainly consist of amorphous and different crystalline phases. The coatings compared to AZ91D magnesium alloy exhibit good corrosion resistance because of the presence of the amorphous phase in the coatings.

Microstructural and Mechanical Properties of Ti3Al-Based Intermetallics Produced by Powder Metallurgy

2005 ◽  
Vol 494 ◽  
pp. 211-216 ◽  
Author(s):  
B. Dimčić ◽  
M. Vilotijević ◽  
D. Božić ◽  
D. Rajnović ◽  
M.T. Jovanović
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Powder Metallurgy ◽  
Room Temperature ◽  
Solution Treatment ◽  
Microstructural Characterization ◽  
Compression Tests ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scanning Electron

The structural and compression mechanical properties of Ti3Al-based intermetallics produced by powder metallurgy techniques have been studied. The as-milled powders were compacted by hot pressing to non-porous homogenous compacts. Prior to compression tests, all compacts were homogenized by a solution treatment at 1050°C (a+β region) for 1h, followed by water quenching. The compression tests were performed from room temperature to 500°C in vacuum at a strain rate of 1 3 10 4 . 2 − − × s . Detailed microstructural characterization was evaluated by scanning electron microscopy (SEM), followed by energy dispersive spectroscopy (EDS) and X-ray diffraction analysis.

scholarly journals Manufacture of ceramics with high mechanical properties from red mud and granite waste

2019 ◽  
Vol 69 (333) ◽  
pp. 180 ◽  
Author(s):  
I. Gonzalez-Triviño ◽  
J. Pascual-Cosp ◽  
B. Moreno ◽  
M. Benítez-Guerrero
Keyword(s):  
Mechanical Properties ◽  
Red Mud ◽  
Bauxite Residue ◽  
Hardness Test ◽  
X Ray Diffraction ◽  
Alumina Production ◽  
X Ray ◽  
Test Electron ◽  
Electron Scanning Microscopy ◽  
Global Inventory

Red mud (bauxite residue) is an alkaline suspension that is the by-product of alumina production via the Bayer process. Its elevated annual production and the global inventory of red mud determine its valorisation. Granite can be used as a source of fluxing oxides for the ceramic industry, as can the flake-shaped waste generated during the flaming of granite. In this work, a set of ceramic pieces made of red mud and granite waste are prepared and characterised via X-ray diffraction, a hardness test, electron scanning microscopy, a leaching test, and determining open porosity, water absorption, bulk density and flexural strength of the samples. The main crystalline phases in the high-temperature fired products are hematite, pseudobrookite and anorthite; the presence of magnetite reveals their ferrimagnetic character. All samples present high mechanical properties. Leaching results are below critical levels established by regulations.

scholarly journals Mechanical properties and microstructure evolution of high-manganese (0.9 C – 13.95 Mn) steel during aging

2021 ◽  
Vol 297 ◽  
pp. 01044
Author(s):  
Omar Ben lenda ◽  
Sara Benmaziane ◽  
Ahmed Tara ◽  
Elmadani Saad
Keyword(s):  
Mechanical Properties ◽  
Hardness Test ◽  
Manganese Steel ◽  
X Ray Diffraction ◽  
High Manganese ◽  
High Manganese Steel ◽  
Influence Of Temperature ◽  
X Ray ◽  
Influence Of Temperature On ◽  
Mn Steel

The influence of temperature on the structural and mechanical properties of the (0.9 C - 13.95 Mn) steel was investigated in this work. The high-manganese steel has underwent aging treatments at temperatures 700, 750, 800 and 850 °C for different times. The experimental techniques used are hardness test, scanning electron microscopy, optical microscopy and X-ray diffraction. The mechanical behavior and microstructural evolution of the high-manganese steel during aging are almost the same. The aging of the high-manganese steel was characterized by a rapid hardening while the overaging by a slow softening. In aging, the dispersion of fine M7C3 carbides in the austenite led to an increase in hardness. In overaging, the softening was caused by the coarsening of the M7C3 carbides.

Effect of Solution Treatment on Microstructure and Mechanical Properties in an Al-9.3Zn-2.0Mg-1.8Cu Alloy

2016 ◽  
Vol 877 ◽  
pp. 606-610
Author(s):  
Kai Wen ◽  
Bai Qing Xiong ◽  
Yong An Zhang ◽  
Xi Wu Li ◽  
Zhi Hui Li ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Solution Treatment ◽  
Second Phase ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Residual Phase ◽  
Solution Treated ◽  
Treatment Parameter ◽  
The Matrix

The microstructure solution treated by various temperatures of 2h in as-extruded Al-9.3Zn-2.0Mg-1.8Cu alloy was investigated by means of optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X-ray diffraction (XRD), and differential scanning calorimetry (DSC) analysis. The mechanical properties treated at 465oC for various times were tested by room temperature tensile mechanical properties test. The results indicated that second phase of the as-extruded alloy mainly consists of Mg (Zn,Cu,Al)2 and Fe-rich phases. Mg (Zn,Cu,Al)2 phase completely dissolved into the matrix solution treated at 465oC or higher for 2h while residual phase was mainly Fe-rich phase. The mechanical properties treated at 465oC for various time were tested and optimized solution treatment parameter was chosen as 465°C/1.5h.

Mechanical properties of FeAlSi powders prepared by mechanical alloying from different initial feedstock materials

2019 ◽  
Vol 107 (2) ◽  
pp. 207 ◽  
Author(s):  
Jaroslav Čech ◽  
Petr Haušild ◽  
Miroslav Karlík ◽  
Veronika Kadlecová ◽  
Jiří Čapek ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Mechanical Alloying ◽  
Young’S Modulus ◽  
Milling Time ◽  
Young's Modulus ◽  
Element Model ◽  
X Ray Diffraction ◽  
X Ray ◽  
Powder Particles ◽  
Complete Homogenization

FeAl20Si20 (wt.%) powders prepared by mechanical alloying from different initial feedstock materials (Fe, Al, Si, FeAl27) were investigated in this study. Scanning electron microscopy, X-ray diffraction and nanoindentation techniques were used to analyze microstructure, phase composition and mechanical properties (hardness and Young’s modulus). Finite element model was developed to account for the decrease in measured values of mechanical properties of powder particles with increasing penetration depth caused by surrounding soft resin used for embedding powder particles. Progressive homogenization of the powders’ microstructure and an increase of hardness and Young’s modulus with milling time were observed and the time for complete homogenization was estimated.

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