Scaling Up of Osmotic Distillation from Laboratory to Pilot Plant for Concentration of Fruit Juices

2005 ◽  
Vol 1 (2) ◽  
Author(s):  
A. V. Bui ◽  
H. M. Nguyen
Keyword(s):  
Pilot Plant ◽  
Grape Juice ◽  
Scaling Up ◽  
Pilot Scale ◽  
High Viscosity ◽  
Hollow Fibre ◽  
Fruit Juices ◽  
Operating Conditions ◽  
High Concentration ◽  
Osmotic Distillation

A step-by-step procedure for scaling up of an osmotic distillation system from laboratory to pilot plant is discussed. The newly built pilot scale OD system featured a flexibility of using 1 or 2 hollow fibre modules at a time to suit the concentration demands. Three types of hollow fibres were tested on the new system. Pilot trials for OD concentration of apple, grape juices and freeze concentrated (FC) grape juice were successfully carried out to achieve a final concentration up to 65°Brix with fluxes ranging from 2.4 to 0.69kg.m-2.h-1 depending on the fibre types and the operating conditions. Cascade effect was also employed to deal with high viscosity to achieve high concentration. The obtained pilot OD fluxes were comparable to the ones obtained in the lab under similar conditions, and they fitted well with the developed models. Sensory evaluation indicated that OD well preserved the quality attributes of the fruit juices.

scholarly journals Characteristics of Flame Stability and Gaseous Emission of Bio-Crude Oil from Coffee Ground in a Pilot-Scale Spray Burner

Energies ◽  
2020 ◽  
Vol 13 (11) ◽  
pp. 2882
Author(s):  
Sang Kyu Choi ◽  
Yeon Seok Choi ◽  
Yeon Woo Jeong ◽  
So Young Han ◽  
Quynh Van Nguyen
Keyword(s):  
Crude Oil ◽  
Pilot Scale ◽  
High Viscosity ◽  
Flame Stabilization ◽  
Operating Conditions ◽  
Injection System ◽  
Optimum Operating ◽  
Flame Stability ◽  
Gaseous Emission ◽  
Coffee Ground

Coffee ground has been recently considered as a new biomass resource in relation to the increasing coffee consumption worldwide. The bio-crude oil can be produced by fast pyrolysis of coffee ground, and it has advantages of larger heating values in comparison with those from other biomass. But the bio-crude oil from coffee ground has a significantly high viscosity which can hinder the application to conventional burners. In this study, a pilot-scale burner system with a 35 kW capacity with an air-blast atomizing nozzle was developed for the combustion of bio-crude oil from coffee ground with a high viscosity. A downward fuel injection system was adopted to enhance the ignition of fuel spray and the flame stabilization, and a movable block swirl generator was installed for the combustion air. The bio-crude oil was blended with ethanol at the volumetric ratio of 9:1 to enhance the combustion characteristics. The effect of various atomizing air pressures, swirl intensities, and overall equivalence ratios on the flame stability and gaseous emission were investigated to find out the optimum operating conditions for a bio-crude oil burner.

Treatment of Refinery Wastewater with Isolated Biological Aerated Filters: A Pilot-Scale Study

2012 ◽  
Vol 610-613 ◽  
pp. 2332-2341
Author(s):  
Jian Guang Huang ◽  
Li Zhong ◽  
Wen Yu Xie
Keyword(s):  
Waste Water ◽  
Waste Water Treatment ◽  
Oxygen Demand ◽  
Volume Ratio ◽  
Pilot Scale ◽  
Mean Value ◽  
Operating Conditions ◽  
Water Volume ◽  
High Concentration ◽  
Set Up

A pilot scale biochemical treatment system containing three isolated biological aerated filters, one oil-separation pool and one secondary sedimentation tank was set up and used for high concentration organic waste water treatment. Effect of different operating conditions on Chemical Oxygen Demand (CODCr), sulphides, hydroxybenzene and oil degradation was investigated. And the ways of sulphides removal were also explored. While CODCr, the concentrations of sulphides, hydroxybenzene and oil in the waste water are no more than 1500 mg/L, 800 mg/L, 15 mg/L and 150mg/L, respectively, the system can run stably and the total removal of these pollutants is 88.8%, 98.8%, 96.8% and 91.0% accordingly though hydraulic retention time (HRT) varies from 7.95 hr to 15.90 hr and the air/water volume ratio (AWVR) varies from 12 to 8. Most of the sulphides are removed by Biodegradation with Isolated Biological Aerated Filters. Most of the pollutants are removed in the 1st BAF and about 96.5% by mean value of sulphides transforme into elemental sulfur and only about 2.7% by mean value of sulphides transforme into sulphates.

scholarly journals ESCALONAMENTO DE TECNOLOGIAS: DESENVOLVIMENTO DE PRODUTO E PROCESSO DO LABORATÓRIO À ESCALA PILOTO CONECTADO AO MERCADO (PARTE 1)

Química Nova ◽  
2020 ◽  
Author(s):  
Elimar Vasconcellos ◽  
Priscila Souza ◽  
Marcella Franco ◽  
Vinícius Castro ◽  
Lorena Souza ◽  
...  
Keyword(s):  
Pilot Plant ◽  
Process Development ◽  
Scale Up ◽  
Feasibility Studies ◽  
Basic Research ◽  
Scaling Up ◽  
Pilot Scale ◽  
Economic Feasibility ◽  
One Step ◽  
Expensive Process

TECHNOLOGY SCALE UP: PROCESS DEVELOPMENT FROM THE LABORATORY TO PILOT SCALE CONNECTED TO MARKET (PART 1). In this article, it is described the main aspects to be considered during the process of scaling up hard sciences technologies developed in the Science and Technology Institutes aiming at industrial application. Based on the experience of our group in scaling up, pre-acceleration, and acceleration of different technologies, a methodology was developed and divided into four main stages: Step 1, which involves basic research, Step 2 with a focus on product development, and Step 3 with a focus on process development, all on the laboratory scale and the last one, Step 4 focused on pilot plant development. The most important aspect of this article is to show that many critical questions can be answered even in the laboratory phase. In this way, the risks of Step 4 are minimized. Step 4 is a complicated, lengthy, and expensive process of construction and operation of a pilot plant. Aspects such as proof of concept, technical and economic feasibility studies, minimum viable product, capital expenditures, and operating expenses of pilot plants are approached in a simplified way to serve as a basis for researchers who wants to know the long path to be followed by technology before reaching the industry, consequently the market.

scholarly journals Osmotic distillation and quality evaluation of sucrose, apple and orange juices in hollow fiber membrane contactor

2017 ◽  
Vol 23 (2) ◽  
pp. 217-227 ◽  
Author(s):  
Waheed Rehman ◽  
Waheed Zeb ◽  
Amir Muhammad ◽  
Wajid Ali ◽  
Mohammad Younas
Keyword(s):  
Hollow Fiber Membrane ◽  
Sucrose Solution ◽  
Water Flux ◽  
Quality Parameters ◽  
Hollow Fibre ◽  
Fruit Juices ◽  
Membrane Contactor ◽  
Flow Configuration ◽  
Osmotic Distillation ◽  
Start Up

Sucrose solution, apple and orange juices were concentrated through osmotic distillation (OD) process using a mini-module Liqui-CelTM hollow fibre membrane contactor. Mass transport characteristics of water molecules from feed to stripping solution were studied. Process parameters such as feed temperature, feed flow rate and concentration of stripping solution (CaCl2) were varied. Sucrose solution was concentrated from 135 to 510 g TSS kg-1 in 340 min using feed-in- -lumen flow configuration at a start-up water flux of 0.250 L m-2 h-1 and a temperature of 30?C. Similarly, it was concentrated up to 510 g TSS kg-1 in 200 min using feed-in-shell flow configuration at a start-up water flux of 0.505 L m-2 hr1 and a temperature of 30?C. In a total recycle time of 340 min, clarified apple and orange juices were concentrated up to 500 g TSS kg-1 using feed-in-lumen flow configuration at a start-up water flux of 0.204 and 0.294 L m-2 hr1, respectively. It was found that quality parameters of fruit juices were well improved after the osmotic distillation process. The process therefore has good potential for application in the fruit processing industry for concentration of fruit juices.

Demonstration of a Pilot-Scale Plant for Biomass Torrefaction and Briquetting

2018 ◽  
Vol 34 (1) ◽  
pp. 85-98 ◽  
Author(s):  
Mark A. Severy ◽  
Charles E. Chamberlin ◽  
Anthony J. Eggink ◽  
Arne E. Jacobson
Keyword(s):  
Energy Density ◽  
Moisture Content ◽  
Pilot Plant ◽  
Biomass Conversion ◽  
Dry Mass ◽  
Pilot Scale ◽  
Operating Conditions ◽  
Scale Production ◽  
Long Distance ◽  
Throughput Rate

Abstract. A semi-mobile torrefaction and densification pilot plant was constructed in order to determine ideal operating conditions and evaluate briquette quality and throughput rate using forest residuals as the input feedstock. Experiments were conducted at various conditions with feedstock moisture content ranging from 4% to 25% (wet basis), reactor residence times of 10 and 20 min, and final product temperatures between 214°C and 324°C. Optimal operating conditions, evaluated based on throughput rate, specific electricity demand, torrefied briquette grindability, briquette volumetric energy density, and briquette durability, were identified to occur with a short residence time (10 min), low feedstock moisture content (<11% wet basis), and high final product temperature between 267°C and 275°C. These conditions were able to process 510 to 680 kg h-1 (wet basis) feedstock with a dry mass yield of 79% to 84% to produce torrefied biomass with a higher heating value of 21.2 to 23.0 MJ kg-1 (dry basis) compared to 19.6 MJ kg-1 for the original biomass. Torrefied briquettes produced at these conditions had a neatly stacked packing density of 990 kg m-3 and a volumetric energy density of 21,800 MJ m-3. Their specific grinding energy was an average 37% of the energy required to grind a raw biomass briquette. These torrefied briquettes were more durable (94% DU) than raw briquettes (85% DU) directly following production, but were less durable after undergoing temperature and humidity fluctuations associated with long distance transportation (74% DU for torrefied and 84% DU for raw biomass briquettes). Results from this pilot plant are promising for commercial scale production of high quality torrefied briquettes and should lead to additional research and development of a torrefaction system optimized for a higher throughput rate at these conditions. Keywords: Biomass, Biomass conversion technology, Bioenergy, Briquetting, Densification, Forest residuals, Pyrolysis, Torrefaction.

scholarly journals Prediction of Permeate Flux in Ultrafiltration Processes: A Review of Modeling Approaches

Membranes ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 368
Author(s):  
Carolina Quezada ◽  
Humberto Estay ◽  
Alfredo Cassano ◽  
Elizabeth Troncoso ◽  
René Ruby-Figueroa
Keyword(s):  
Phenomenological Models ◽  
Membrane Filtration ◽  
Membrane Surface ◽  
Scaling Up ◽  
Fruit Juices ◽  
Operating Conditions ◽  
Percentage Error ◽  
Permeate Flux ◽  
Predictive Capacity ◽  
Theoretical Derivation

In any membrane filtration, the prediction of permeate flux is critical to calculate the membrane surface required, which is an essential parameter for scaling-up, equipment sizing, and cost determination. For this reason, several models based on phenomenological or theoretical derivation (such as gel-polarization, osmotic pressure, resistance-in-series, and fouling models) and non-phenomenological models have been developed and widely used to describe the limiting phenomena as well as to predict the permeate flux. In general, the development of models or their modifications is done for a particular synthetic model solution and membrane system that shows a good capacity of prediction. However, in more complex matrices, such as fruit juices, those models might not have the same performance. In this context, the present work shows a review of different phenomenological and non-phenomenological models for permeate flux prediction in UF, and a comparison, between selected models, of the permeate flux predictive capacity. Selected models were tested with data from our previous work reported for three fruit juices (bergamot, kiwi, and pomegranate) processed in a cross-flow system for 10 h. The validation of each selected model's capacity of prediction was performed through a robust statistical examination, including a residual analysis. The results obtained, within the statistically validated models, showed that phenomenological models present a high variability of prediction (values of R-square in the range of 75.91–99.78%), Mean Absolute Percentage Error (MAPE) in the range of 3.14–51.69, and Root Mean Square Error (RMSE) in the range of 0.22–2.01 among the investigated juices. The non-phenomenological models showed a great capacity to predict permeate flux with R-squares higher than 97% and lower MAPE (0.25–2.03) and RMSE (3.74–28.91). Even though the estimated parameters have no physical meaning and do not shed light into the fundamental mechanistic principles that govern these processes, these results suggest that non-phenomenological models are a useful tool from a practical point of view to predict the permeate flux, under defined operating conditions, in membrane separation processes. However, the phenomenological models are still a proper tool for scaling-up and for an understanding the UF process.

The Role of Operating Conditions in Osmotic Distillation and Direct Contact Membrane Distillation - A Comparative Study

2006 ◽  
Vol 2 (5) ◽  
Author(s):  
V. A. Bui ◽  
M. H. Nguyen
Keyword(s):  
Comparative Study ◽  
Direct Contact ◽  
Membrane Distillation ◽  
Operating Conditions ◽  
Flux Rate ◽  
High Concentration ◽  
Osmotic Distillation ◽  
Direct Contact Membrane Distillation ◽  
Feed Temperature

This paper presents a comparative study on the role of operating conditions in osmotic distillation (OD) and direct contact membrane distillation (DCMD). Comparisons were made for lab scale OD and DCMD experiments on two types of PVDF hollow fibres under similar operating conditions for the concentration of glucose solutions from 30 to 60% (w/w) at temperatures as low as 25 to 45°C. Analysis of the results indicated that temperature was the most influencing factor for process improvement for both OD and DCMD. The flux in DCMD was improved by 3 to 4 times when feed temperature increased by 15 degrees, while this figure was nearly 3 times for OD when feed temperature increased by 20 degrees. The flow rates of the two streams played a more important role in maintaining the driving force, and consequently the flux rate, in DCMD rather than in OD. It was found that feed velocity had significant effect on DCMD performance, but insignificant in OD. Feed concentration, as the determining factor on water activity and viscosity, caused a more serious reduction of the flux rate in the high concentration range of 45-60% rather than in the dilute region of 30-40%. The effect was more significant in DCMD than in OD. The ratio of DCMD flux over that of OD ranged from 0.41 to 0.66 for PV375 when concentrating glucose solutions 30-40% w/w and from 0.35 to 0.69 for PV650 when concentrating high solid content ones. However, DCMD can overcome the disadvantages of OD being poor consumers’ perception, (due to the use of brine solution being a chemical), the potential problem of corrosion by the brine and the cost of its reconcentration.

Application of a Pilot-Scale Pulsed Electrocoagulation system to OCC-Based Paper Mill Effluent

TAPPI Journal ◽  
2009 ◽  
Vol 8 (3) ◽  
pp. 14-20 ◽  
Author(s):  
YUAN-SHING PERNG ◽  
EUGENE I-CHEN WANG ◽  
SHIH-TSUNG YU ◽  
AN-YI CHANG
Keyword(s):  
Water Quality ◽  
Quality Indicators ◽  
Paper Mill ◽  
Pilot Scale ◽  
Operating Conditions ◽  
Optimal Dosage ◽  
Water Quality Indicators ◽  
Paper Mill Effluent ◽  
Treated Effluent ◽  
True Color

Trends toward closure of white water recirculation loops in papermaking often lead to a need for system modifications. We conducted a pilot-scale study using pulsed electrocoagulation technology to treat the effluent of an old corrugated containerboard (OCC)-based paper mill in order to evaluate its treatment performance. The operating variables were a current density of 0–240 A/m2, a hydraulic retention time (HRT) of 8–16 min, and a coagulant (anionic polyacrylamide) dosage of 0–22 mg/L. Water quality indicators investigated were electrical con-ductivity, suspended solids (SS), chemical oxygen demand (COD), and true color. The results were encouraging. Under the operating conditions without coagulant addition, the highest removals for conductivity, SS, COD, and true color were 39.8%, 85.7%, 70.5%, and 97.1%, respectively (with an HRT of 16 min). The use of a coagulant enhanced the removal of both conductivity and COD. With an optimal dosage of 20 mg/L and a shortened HRT of 10 min, the highest removal achieved for the four water quality indicators were 37.7%, 88.7%, 74.2%, and 91.7%, respectively. The water qualities thus attained should be adequate to allow reuse of a substantial portion of the treated effluent as process water makeup in papermaking.

A pilot web former designed to study retention-formation relationships

2010 ◽  
Vol 25 (2) ◽  
pp. 185-194
Author(s):  
Anna Svedberg ◽  
Tom Lindström
Keyword(s):  
Pilot Scale ◽  
Operating Conditions ◽  
Montmorillonite Clay ◽  
Speed Ratio ◽  
Good Reproducibility ◽  
Total Solids ◽  
Retention Aids ◽  
Solids Content ◽  
Relationship Of ◽  
The Relationship

Abstract A pilot-scale fourdrinier former has been developed for the purpose of investigating the relationship between retention and paper formation (features, retention aids, dosage points, etc.). The main objective of this publication was to present the R-F (Retention and formation)-machine and demonstrate some of its fields of applications. For a fine paper stock (90% hardwood and 10% softwood) with addition of 25% filler (based on total solids content), the relationship between retention and formation was investigated for a microparticulate retention aid (cationic polyacrylamide together with anionic montmorillonite clay). The retention-formation relationship of the retention aid system was investigated after choosing standardized machine operating conditions (e.g. the jet-to-wire speed ratio). As expected, the formation was impaired when the retention was increased. Since good reproducibility was attained, the R-F (Retention and formation)-machine was found to be a useful tool for studying the relationship between retention and paper formation.

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