scholarly journals ADSORPSI AIR DARI CAMPURAN UAP ETANOL-AIR DENGAN ZEOLIT SINTETIS 4A DALAM PACKED BED DALAM RANGKA PRODUKSI FUEL GRADE ETHANOL

2018 ◽  
Vol 11 (2) ◽  
pp. 68
Author(s):  
Handrian Handrian ◽  
Wahyudi Budi Sediawan ◽  
Aswati Mindaryani

Ethanol can be used as fuel if it has a purity of 99.5%, while ethanol distillation will stop at its azeotrop point, ie at 95.6%. Adsorption of molecular sieve is one of the methods to obtain ethanol with level above the azeotropic point. Adsorbent that serves as molecular sieve is synthetic zeolite 4A. The adsorbent has a pore diameter of 3.9 Ǻ, then water and ethanol each has a molecular diameter of 2.75 Ǻ and 4.4 Ǻ. Hence the adsorbent is selective against the ethanol-water mixture. The purpose of this research is to obtain ethanol above its azeotropic point and to study the relationship between the influence of flow rate (Vz) and temperature (T) to changes in the number of mass transfer coefficient (kc), radial diffusivity (Der) and henry constants (H') which can be used as parameters in the design of adsorption tools on a commercial scale.This experiment was conducting by weighing zeolite 4A as much as 100 grams, then compiled and measured the height on packed bed column adsorbent. The heating regulator is switched on and set to a constant temperature of 80, 85, 90, 95 and 1000C. Ethanol 95.61% with 250 ml volume is put into three-neck flask, then heat to evaporate. Turn on the cooling back and adjust the amount of formed vapor rate by adjusting the faucet opening and the degree of voltage in the heating mantle. The magnitude of the vapor flow rate is set at 2, 4 and 6 liters / minute. The products is accomodated and samples were taken every minute to analyze the ethanol content.This adsorption process gives the highest yield of ethanol with 99.40% content. The steam flow rate of 2 lpm and the temperature of 800C is the optimum combination in this research because much of the water vapor adsorbed on the 4A zeolite grain is 7.93 grams. The numerical calculation provides the result that the value of Der in this experiment is 1.59.10-3 cm2 / men, and the relation of kc are the function of reynolds and H'  the function of temperature are as follows: kc = 7,95.10^-3.(Re)^0,1639 and H' = 4,47.10^-3.exp(2565,26/T)

2020 ◽  
Vol 17 (4) ◽  
pp. 47-52
Author(s):  
Vibha Goswami ◽  
Renu Upadhyaya ◽  
Sumanta Kumar Meher

In this study, synthesised Azadirachta indica adsorbent was used for the removal of methylene blue dye using a packed bed column. The effect of feed flow rate, feed methylene blue dye concentration, and bed height of column on percentage removal of dye was studied. It was observed that the column bed exhausted rapidly at a higher flow rate and therefore, a breakthrough occurred faster. However, it was observed that bed exhaustion time increases on increasing the bed height from 2 to 10 inch at 10 mg/L feed dye concentration and feed flow rate of 40 ml/min. It was also found that the breakthrough curve is more dispersed and the percentage removal of dye increases on decreasing the feed methylene dye concentration from 150 to 10 mg/L. The percentage removal was found to be 96.89% at 20 ml/min of feed flow rate under 10 inch of bed height and 10 mg/L of feed dye concentration. The atomic absorption spectrophotometer and scanning electron microscope were used for estimating the effluent dye concentration from the column and morphological study, respectively.


2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Satoshi Miyamoto ◽  
Zu Soh ◽  
Shigeyuki Okahara ◽  
Akira Furui ◽  
Taiichi Takasaki ◽  
...  

AbstractThe need for the estimation of the number of microbubbles (MBs) in cardiopulmonary bypass surgery has been recognized among surgeons to avoid postoperative neurological complications. MBs that exceed the diameter of human capillaries may cause endothelial disruption as well as microvascular obstructions that block posterior capillary blood flow. In this paper, we analyzed the relationship between the number of microbubbles generated and four circulation factors, i.e., intraoperative suction flow rate, venous reservoir level, continuous blood viscosity and perfusion flow rate in cardiopulmonary bypass, and proposed a neural-networked model to estimate the number of microbubbles with the factors. Model parameters were determined in a machine-learning manner using experimental data with bovine blood as the perfusate. The estimation accuracy of the model, assessed by tenfold cross-validation, demonstrated that the number of MBs can be estimated with a determinant coefficient R2 = 0.9328 (p < 0.001). A significant increase in the residual error was found when each of four factors was excluded from the contributory variables. The study demonstrated the importance of four circulation factors in the prediction of the number of MBs and its capacity to eliminate potential postsurgical complication risks.


2013 ◽  
Vol 781-784 ◽  
pp. 1637-1645 ◽  
Author(s):  
Ting Jun Ma ◽  
Yi Qing Xu

The degradation effectiveness and reaction kinetics of representative organophosphorus (OP) pesticide in a packed-bed plasma reactor have been studied. Important parameters, including peak voltage, pulse frequency, gas-flow rate, initial concentration, diameter of catalyst particles, and thickness of catalyst bed which influences the removal efficiency, were investigated. Experimental results indicated that rogor removal efficiency as high as 80% can be achieved at 35 kV with the gas flow rate of 800 mL/min and initial concentration of 11.2 mg/m3.The removal efficiency increased with the increase of pulsed high voltage, and pulse frequency, the decrease of the diameter of catalyst particles and the thickness of catalyst bed. Finally, a model was established to predict the degradation of the rogor, which generally can simulate the experimental measurements to some degree.


1965 ◽  
Vol 87 (1) ◽  
pp. 134-141 ◽  
Author(s):  
F. J. Moody

A theoretical model is developed for predicting the maximum flow rate of a single component, two-phase mixture. It is based upon annular flow, uniform linear velocities of each phase, and equilibrium between liquid and vapor. Flow rate is maximized with respect to local slip ratio and static pressure for known stagnation conditions. Graphs are presented giving maximum steam/water flow rates for: local static pressures between 25 and 3,000 psia, with local qualities from 0.01 to 1.00; local stagnation pressures and enthalpies which cover the range of saturation states.


1996 ◽  
Vol 118 (1) ◽  
pp. 29-35 ◽  
Author(s):  
K. Minemura ◽  
K. Egashira ◽  
K. Ihara ◽  
H. Furuta ◽  
K. Yamamoto

A turbine flowmeter is employed in this study in connection with offshore oil field development, in order to measure simultaneously both the volumetric flow rates of air-water two-phase mixture. Though a conventional turbine flowmeter is generally used to measure the single-phase volumetric flow rate by obtaining the rotational rotor speed, the method proposed additionally reads the pressure drop across the meter. After the pressure drop and rotor speed measured are correlated as functions of the volumetric flow ratio of the air to the whole fluid and the total volumetric flow rate, both the flow rates are iteratively evaluated with the functions on the premise that the liquid density is known. The evaluated flow rates are confirmed to have adequate accuracy, and thus the applicability of the method to oil fields.


2015 ◽  
Author(s):  
Silviu Sprinceana ◽  
Ioan Mihai ◽  
Marius Beniuga ◽  
Cornel Suciu

2011 ◽  
Vol 2011 ◽  
pp. 1-6 ◽  
Author(s):  
Hsiao-Ching Chen ◽  
Hen-Yi Ju ◽  
Tsung-Ta Wu ◽  
Yung-Chuan Liu ◽  
Chih-Chen Lee ◽  
...  

An optimal continuous production of biodiesel by methanolysis of soybean oil in a packed-bed reactor was developed using immobilized lipase (Novozym 435) as a catalyst in atert-butanol solvent system. Response surface methodology (RSM) and Box-Behnken design were employed to evaluate the effects of reaction temperature, flow rate, and substrate molar ratio on the molar conversion of biodiesel. The results showed that flow rate and temperature have significant effects on the percentage of molar conversion. On the basis of ridge max analysis, the optimum conditions were as follows: flow rate 0.1 mL/min, temperature52.1∘C, and substrate molar ratio 1 : 4. The predicted and experimental values of molar conversion were83.31±2.07% and82.81±.98%, respectively. Furthermore, the continuous process over 30 days showed no appreciable decrease in the molar conversion. The paper demonstrates the applicability of using immobilized lipase and a packed-bed reactor for continuous biodiesel synthesis.


Author(s):  
V Sureshkannan ◽  
TV Arjunan ◽  
D Seenivasan ◽  
SP Anbuudayasankar ◽  
M Arulraj

Compressed air free from traces of water vapour is vital in many applications in an industrial sector. This study focuses on parametric optimization of a pressure-based packed bed adsorption system for air dehumidification through the Taguchi method and Genetic Algorithm. The effect of operational parameters, namely absolute feed air pressure, feed air linear velocity, and purge air flow rate percent on adsorption uptake rate of molecular sieve 13X-water pair, are studied based on L25 orthogonal array. From the analysis of variance, it has been found that absolute feed air pressure and purge air flow rate percent were the parameters making significant improvement in the adsorption uptake rate. A correlation representing the process was developed using regression analysis. The optimum adsorption conditions were obtained through the Taguchi method and genetic algorithm and verified through the confirmation experiments. This system can be recommended for the industrial and domestic applications that require product air with the dew point temperature below 0°C.


2012 ◽  
Vol 2012 ◽  
pp. 1-6 ◽  
Author(s):  
R. Chandra ◽  
V. K. Vijay ◽  
P. M. V. Subbarao

This paper presents the results of an automated water scrubbing system used for enrichment of methane content in the biogas, to produce vehicular grade biomethane fuel. Incorporation of automatic control systems for precisely regulating the water level and maintaining constant operating pressure in the packed bed absorption column of water scrubbing system resulted in steady-state operation of the scrubbing system and a consistent supply of methane-enriched biogas from the gas outlet. The improved automated water scrubbing system was found to enrich 97% methane at an operating column pressure of 1.0 MPa with 2.5 m3/h biogas in-flow rate and 2.0 m3/h water in-flow rate into the scrubbing column unit.


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