scholarly journals Effect of Immediate Dentin Sealing and Surface Conditioning on the Microtensile Bond Strength of Resin-based Composite to Dentin

2019 ◽  
Vol 44 (6) ◽  
pp. E289-E298 ◽  
Author(s):  
CRG van den Breemer ◽  
M Özcan ◽  
MS Cune ◽  
AP Almeida Ayres ◽  
B Van Meerbeek ◽  
...  
Keyword(s):  
Bond Strength ◽  
Analysis Of Variance ◽  
Water Storage ◽  
Silica Coating ◽  
Microtensile Bond Strength ◽  
Surface Conditioning ◽  
Clinical Procedures ◽  
Significant Difference ◽  
The One ◽  
Storage Times

SUMMARY This study evaluated the microtensile bond strength (μTBS) of resin-based composite (RBC) to dentin after different immediate dentin sealing (IDS) strategies and surface-conditioning (SC) methods and on two water storage times. Human molars (n=48) were randomly divided into eight experimental groups involving four different IDS strategies—IDS-1L with one layer of adhesive, IDS-2L with two layers of adhesive, IDS-F with one layer of adhesive and one layer of flowable RBC, and DDS (delayed dentin sealing) with no layer of adhesive (control)—and two different SC methods—SC-P with pumice rubbing and SC-PC with pumice rubbing followed by tribochemical silica coating. The μTBS test was performed after one week and after six months of water storage, being recorded as the “immediate” and “aged” μTBS, respectively. Composite-adhesive-dentin microspecimens (0.9×0.9×8–9 mm) were stressed in tension until failure to determine the μTBS. Failure mode and location of failure were categorized. Two-way analysis of variance was applied to analyze the data for statistically significant differences between the experimental groups (p<0.05). Two-way analysis of variance revealed no significant differences between the one-week μTBS specimens for IDS strategy (p=0.087) and SC methods (p=0.806). However, the interaction of IDS strategy and SC methods appeared statistically significant (p=0.016). The six-month specimen evaluation showed no significant difference in μTBS for SC (p=0.297) and SC/IDS interaction (p=0.055), but the μTBS of the IDS strategies differed significantly among them (p=0.003). For tribochemical silica-coated IDS, no significant effect of aging on μTBS was recorded (p=0.465), but there was a highly significant difference in μTBS depending on the IDS strategy (p<0.001). In addition, the interaction of IDS and aging was borderline statistically significant (p=0.045). The specimens failed mainly at the adhesive-dentin interface for all experimental groups. Dentin exposure during clinical procedures for indirect restorations benefits from the application of IDS, which was shown to result in higher bond strength. No significant differences were found between cleaning with solely pumice or pumice followed by tribochemical silica coating.

scholarly journals Influence of Water Aging on Microtensile Bond Strength of a Flowable and a Packable Bulk-fill Resin Composites to Dentin

2020 ◽  
Vol 8 (D) ◽  
pp. 112-117
Author(s):  
Ayah Atif Selim ◽  
Ahmed Fawzy Abo Elezz ◽  
Rehab Khalil Safy
Keyword(s):  
Bond Strength ◽  
Storage Time ◽  
Resin Composite ◽  
Water Storage ◽  
Aging Effect ◽  
Mean Value ◽  
Control Group ◽  
Microtensile Bond Strength ◽  
Significant Difference ◽  
Influence Of Water

AIM: Investigation of the aging effect on the microtensile bond strength (μTBS) of bulk-fill resin composite (RC) versus a conventionally incrementally applied one. MATERIALS AND METHODS: A total number of 45 sound human impacted third molars extracted molars have been selected to prepare specimens for the μTBS test. Teeth were randomly divided into three groups (C) according to type of RC material which used for restoring the teeth. Where nanohybrid RC (Grandio®SO) was used as the control Group (C1), packable bulk-fill RC (X-tra fil®) was used for restoring teeth in C2 group and flowable bulk-fill RC (X-tra base®) was used for restoring teeth in C3 group. Each group was further subdivided into 3 subgroups (n = 5) according to the water storage time, where in subgroup 1; teeth were stored for 24 h, subgroup 2; teeth were stored for 3 months while for subgroup 3; and teeth were stored for 6 months. After water storage, teeth were sectioned for preparation of μTBS testing beams. Maximum tensile stresses were recorded in megapascal (MPa). RESULTS: After 24 h of water storage, the X-tra base® showed a higher statistically significant μTBS to dentin (33.82 ± 9.84 MPa) than did the other two types of RCs. After 3 months, the X-tra fil® showed the lowest mean value of μTBS (10.90 ± 5.66 MPa), meanwhile, after 6 months of water storage Grandio®SO showed the highest mean value of μTBS (15.85 ± 6.76 MPa). Regardless of the time the X-tra fil® showed the lowest mean of μTBS (15.07 ± 11.73 MPa), while there is no significant difference between the X-tra base® and Grandio®SO. Furthermore, the water aging adversely affects μTBS values which deceased gradually by time. CONCLUSION: The packable bulk-fill RC characterized by lower μTBS to dentin in comparison to the flowable bulk fill and the incrementally applied nanohybrid RCs. Furthermore, the μTBS of the three tested materials decreased gradually by aging.

scholarly journals Bonding Performance of a Hydrophilic Amide Monomer Containing Adhesive to Occlusal and Cervical Dentin

Materials ◽  
2020 ◽  
Vol 13 (21) ◽  
pp. 4727
Author(s):  
Eri Seitoku ◽  
Shuhei Hoshika ◽  
Takatsumi Ikeda ◽  
Shigeaki Abe ◽  
Toru Tanaka ◽  
...  
Keyword(s):  
Bond Strength ◽  
Water Storage ◽  
Adhesive System ◽  
Adhesive Failure ◽  
Adhesive Systems ◽  
Microtensile Bond Strength ◽  
Bonding Performance ◽  
One Step ◽  
The Mean ◽  
The One

This study aimed to evaluate the bonding performance of a new one-step self-etching adhesive system containing a novel hydrophilic amide monomer. Clearfil Universal Bond Quick (CUB) and Clearfil Megabond 2 (CMB) were used as the one-step and two-step adhesive systems, respectively. Flat dentin surfaces of human premolars were exposed using #600 SiC (silicon carbide) and bonded with the respective adhesives of each system. The teeth were sectioned to obtain beams (1 mm × 1 mm) after 24 h of water storage. The mean bond strength and standard deviations (MPa) on an occlusal surface were as follows: CUB: 45.9 ± 19.7 and CMB: 67.9 ± 25.3. The values for cervical ones were CUB: 56.0 ± 20.3 and CMB: 67.6 ± 16.0, respectively. In both conditions, the microtensile bond strength (μTBS) value was lower than that of CMB. As seen during the microscopic observation, no adhesive failure was observed after μTBS testing because CUB formed a firm and tight adhesive interface.

scholarly journals Evaluation of Microtensile Bond Strength of Universal Self-etch Adhesive System to Wet and Dry Dentin

2020 ◽  
Vol 8 (D) ◽  
pp. 77-81
Author(s):  
Mohamed Ahmed Wakwak ◽  
Eslam Hassan Gabr ◽  
Ahmed Mohamed Elmarakby
Keyword(s):  
Bond Strength ◽  
Adhesive System ◽  
Solvent Free ◽  
Microtensile Bond Strength ◽  
Universal Adhesive ◽  
Significance Level ◽  
Significant Difference ◽  
One Step ◽  
Storage Times ◽  
Self Etch

BACKGROUND: The durability of dentin-resin interfaces with the universal adhesive system is a crucial characteristic with chemical interactions between the exposed collagen and the adhesive monomers, but it is still compromised with wet and dry mode. AIM: The present study evaluated the effect of dentin wetness and solvents containing of one-step self-etch adhesives on the microtensile bond strength (μTBS) of dentin at different storage times. METHODS: Occlusal dentin of 54 extracted human molars was exposed. Each adhesive agent was applied according to manufacturer instructions to wet and dry dentin surfaces. Composite resin was incrementally built up. Bond strengths to dentin were determined using the μTBS test after water storage for 24 h, 1 month, and 6 months. One-way ANOVA was used to compare between more than two non-related samples. The significance level was set at p ≤ 0.05. RESULTS: Dryness of dentin increases the μTBS with solvent-containing adhesives while decrease the μTBS with solvent-free adhesive. There was an increase in microtensile bond strength values in the case of ethanol water-based self-etch adhesive over time. No statistically significant difference was found among different storage times regarding μTBS for solvent-free adhesive, while a statistically significant difference was found among different storage times in μTBS for solvent-containing adhesives. CONCLUSION: Universal adhesive systems improve the durability and stability of dentin bond strength.

scholarly journals Influence of desensitizers agents on the dentin bond strength after one-year water storage

2020 ◽  
Vol 19 ◽  
pp. e201602
Author(s):  
Gabriel Nima ◽  
Renata Bacelar Sá ◽  
Marcelo Giannini
Keyword(s):  
Bond Strength ◽  
Test Data ◽  
Composite Resin ◽  
Water Storage ◽  
Adhesive System ◽  
Microtensile Bond Strength ◽  
Mixed Anova ◽  
Dentin Surface ◽  
Significant Difference ◽  
One Year

Aim: Evaluate the effect of adhesives systems combined with desensitizer agents on the microtensile bond strength (μTBS) of a composite resin to dentin. Methods: Cervical dentin of thirty-two human molars were used to simulate hypersensitivity areas. The teeth were divided into four groups (n=8), according to the type of adhesive system and desensitizer agents. No desensitizer was used in the control (Clearfil SE Bond – CS). Two experimental groups were pretreated with either MS Coat Bond (MS) or Biofluorid 12 (BF) immediately prior to bonding with CS. The last group corresponded to Gluma Comfort Bond + Desensitizer (GC) application. After dentin treatments, a composite block was built-up on dentin surface and after 24 hours teeth were serially sectioned to obtain bonded bean specimens. Beams were stored in water for 24 hours or one year. Subsequently, the specimens were submitted to the μTBS test. Data were analyzed by two-way mixed ANOVA and Bonferroni’s test (α = 0.05). Results: At 24 hours, there was no significant difference in μTBS among groups. However, at one year, dentin treated with MS or BF demonstrated significantly lower μTBS of CS to dentin compared to control and GC, which kept their μTBS stable. Conclusion: The effect of MS and BF desensitizer agents on the μTBS of CS to dentin did not reduce the μTBS at 24 hours, but it decreases significantly after one year.

scholarly journals Impact of Immediate Dentin Sealing Using Universal Adhesive under Simulated Pulp Pressure on Microtensile Bond Strength of Indirect Resin Composite Restorations and Dentin Permeability

2021 ◽  
Author(s):  
Emad Abd Elfatah Abo-Alazm ◽  
Rehab Khalil Safy
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
Water Storage ◽  
Microtensile Bond Strength ◽  
Universal Adhesive ◽  
Dentin Permeability ◽  
Composite Restorations ◽  
Significant Difference ◽  
Cad Cam ◽  
Self Etch

Abstract Objective The aim of this study was to investigate the effect of immediate dentin sealing (IDS) technique using universal adhesive under simulated pulp pressure on microtensile bond strength (µTBS) of indirect resin composite restorations and dentin permeability. Materials and Methods Fifty extracted caries-free human third molars were used for specimens' preparation. Each molar's occlusal table was abraded flat and their roots were separated under continuous water cooling. Forty specimens were used for microtensile bond strength test (µTBST) evaluation. The µTBST specimens were randomly assigned to two groups according to the dentin sealing time; Immediate dentin sealing (IDS) and delayed dentin sealing (DDS). Each group was further subdivided into two subgroups according to the adhesive system used for dentin sealing: iBOND self-etch adhesive and GLUMA Bond Universal. All specimens were exposed to simulated pulp pressure for 1 week then restored using computer-aided design/computer-aided manufacturing (CAD/CAM) resin composite blocks. The µTBS was evaluated for all tested subgroups after 24 hours and 6 months of water storage. The remaining 10 teeth were used for the preparation of dentin discs for dentin permeability evaluation. They were divided into two groups according to type of self-etch adhesive used. Fluid filtration rate was evaluated after etching, with smear layer and after adhesive application. Results obtained were statistically analyzed using Shapiro–Wilk test and Weibull analysis. Results Statistically significant difference was recorded between μTBS mean values of both IDS and DDS techniques at 24 hours and after 6 months of water storage. GLUMA Bond Universal adhesive had significantly higher bond strength compared with iBond at both IDS and DDS techniques, but both adhesives showed a significant reduction in the Weibull characteristic strength after 6 months of water storage. Significant reduction in dentin permeability was recorded by both adhesives without any significant difference between them. Conclusions The IDS technique using universal adhesive in self-etch mode is an effective strategy for improving the final bond strength of CAD/CAM resin composite restorations and reducing dentin permeability.

scholarly journals Microtensile Bond Strength of Methacrylate and Silorane Resins to Enamel and Dentin

2014 ◽  
Vol 25 (4) ◽  
pp. 327-331 ◽  
Author(s):  
Gisele Rodrigues da Silva ◽  
Isabela Sousa Araújo ◽  
Rodrigo Dantas Pereira ◽  
Bruno de Castro Ferreira Barreto ◽  
Célio Jesus do Prado ◽  
...  
Keyword(s):  
Bond Strength ◽  
Aging Time ◽  
Storage Time ◽  
Composite Resin ◽  
Glass Plate ◽  
Composite Resins ◽  
Microtensile Bond Strength ◽  
Bonding Interaction ◽  
Significant Difference ◽  
And Storage

The aim of this study was to evaluate the microtensile bond strength (µTBS) of two substrates (enamel and dentin) considering two study factors: type of composite resin [methacrylate-based (Filtek Supreme) or silorane-based (Filtek LS)] and aging time (24 h or 3 months). Twenty human molars were selected and divided into 2 groups (n=10) considering two dental substrates, enamel or dentin. The enamel and dentin of each tooth was divided into two halves separated by a glass plate. Each tooth was restored using both tested composite resins following the manufacturer's instructions. The samples were sectioned, producing 4 sticks for each composite resin. Half of them were tested after 24 h and half after 3 months. µTBS testing was carried out at 0.05 mm/s. Data were analyzed by three-way ANOVA and Tukey's HSD tests at α=0.05. Significant differences between composite resins and substrates were found (p<0.05), but no statistically significant difference was found for aging time and interactions among study factors. The methacrylate-based resin showed higher µTBS than the silorane-based resin. The µTBS for enamel was significantly higher than for dentin, irrespective of the composite resin and storage time. Three months of storage was not sufficient time to cause degradation of the bonding interaction of either of the composite resins to enamel and dentin.

scholarly journals Graphene oxide nano-filler based experimental dentine adhesive. A SEM / EDX, Micro-Raman and microtensile bond strength analysis

2020 ◽  
Vol 18 ◽  
pp. 228080002096693 ◽  
Author(s):  
Abdullah Alshahrani ◽  
Mohammed S Bin-Shuwaish ◽  
Rana S Al-Hamdan ◽  
Thamer Almohareb ◽  
Ahmed M Maawadh ◽  
...  
Keyword(s):  
Graphene Oxide ◽  
Bond Strength ◽  
Sem Analysis ◽  
Strength Analysis ◽  
Hybrid Layer ◽  
Microtensile Bond Strength ◽  
Significant Difference ◽  
Strength And Durability ◽  
And Control ◽  
Microraman Spectroscopy

Aim: The study aimed to assess graphene oxide (GO) adhesive and its dentin interaction using scanning electron microscopy (SEM), MicroRaman spectroscopy and Microtensile bond strength (μTBS). Materials and Methods: Experimental GOA and control adhesives (CA) were fabricated. Presence of GO within the experimental adhesive resin was assessed using SEM and Micro-Raman spectroscopy. Ninety specimens were prepared, sixty teeth were utilized for μTBS, twenty for SEM analysis of interface for CA and GOA and ten were assessed using microRaman spectroscopy. Each specimen was sectioned and exposed dentine was conditioned (35% phosphoric acid) for 10 s. The surface was coated twice with adhesive (15 s) and photopolymerized (20 s). Composite build-up on specimen was photo-polymerized. Among the bonded specimens, thirty specimen were assessed using Micro-Raman spectrometer, SEM and energy dispersive X-ray spectroscopy (EDX), whereas remaining specimens were divided in to three sub-groups ( n = 10) based on the storage of 24 h, 8 weeks and 16 weeks. μTBS testing was performed at a crosshead speed of 0.5 mm/min using a microtensile tester. The means of μ-tbs were analyzed using ANOVA and post hoc Tukey multiple comparisons test. Results: No significant difference in μTBS of CA and GOA was observed. Storage time presented a significant interaction on the μTBS ( p < 0.01). The highest and lowest μTBS was evident in CA (30.47 (3.55)) at 24 h and CA (22.88 (3.61)) at 18 weeks. Micro-Raman analysis identified peaks of 1200 cm-1 to 1800 cm1, D and G bands of GO nanoparticles in the resin. Uniform distribution of graphene oxide nanoparticles was present at the adhesive and hybrid layer. Conclusion: GO showed interaction within adhesive and tooth dentin similar to CA, along with formation of hybrid layer. In ideal conditions (absence of nanoleakage), graphene oxide modified adhesive shows comparable bond strength and durability of resin dentine bond.

scholarly journals Effect of cleaning agent, primer application and their combination on the bond strength of a resin cement to two yttrium-tetragonal zirconia polycrystal zirconia ceramics

2017 ◽  
Vol 11 (01) ◽  
pp. 006-011 ◽  
Author(s):  
William Matthew Negreiros ◽  
Glaucia Maria Bovi Ambrosano ◽  
Marcelo Giannini
Keyword(s):  
Bond Strength ◽  
Water Storage ◽  
Tetragonal Zirconia ◽  
Resin Cement ◽  
Zirconia Ceramic ◽  
Coupling Agents ◽  
Zirconia Ceramics ◽  
Cleaning Agent ◽  
Failure Data ◽  
Significant Difference

ABSTRACT Objective: The objective of this study is to evaluate the effect of a cleaning agent and priming on the bond strength (BS) of a resin cement (RC) to zirconia ceramics after 24 h and 1 year of water-storage. Materials and Methods: Fifty-six Katana and 56 ZirCAD zirconia ceramic plates were prepared and each zirconia brand was divided into four groups (n = 14): (1) untreated; (2) treated with Ivoclean cleaning agent; (3) treated with Monobond Plus coupling agent; (4) treated with Ivoclean + Monobond Plus. Cleaning and coupling agents were applied to zirconia following the manufacturers' instructions. The RC was manipulated, inserted into tubes (0.75 mm diameter/1 mm height) that were positioned on the zirconia surfaces and light activated. Specimens were tested after 24 h and 1 year of water storage. A shear load was applied to the base of the RC cylinders (until failure. Data were analyzed by three-way ANOVA and Tukey tests (α = 5%). Results: No significant difference in BS was noted between zirconia ceramics, except when the combination of cleaning and coupling agents was used. This combination increased the BS for Katana zirconia. One year of water storage leads to a decrease in BS for all experimental groups. Conclusion: The combination of cleaning agent and priming can yield higher BS for Katana at 24 h. BS to zirconia ceramics reduced approximately 50% after 1 year.

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