scholarly journals Pengaruh penambahan hidroksiapatit terhadap porositas dan compressive strength basis resin akrilik heat-curedEffect of hydroxyapatite addition towards porosity level and compressive strength of heat-cured acrylic resin base

2020 ◽  
Vol 32 (2) ◽  
pp. 91
Author(s):  
Chaterina Diyah Nanik Kusumawardani ◽  
Ronaldo Triputro Chondro ◽  
Ivan Andrian ◽  
Rima Parwati Sari

Pendahuluan: Resin akrilik heat cured (HC) merupakan pilihan utama bahan sebagai basis gigi tiruan. Hidroksiapatit (HAP) adalah molekul kristalin yang sudah banyak digunakan di kedokteran gigi. Penelitian terdahulu membuktikan bahwa HAP mampu mengurangi monomer sisa pada resin akrilik HC, yang akan mengurangi juga porositas resin akrilik tersebut. Berkurangnya porositas resin akrilik, diharapkan akan meningkatkan kekuatan mekanik resin akrilik tersebut. Tujuan penelitian menganalisis pengaruh penambahan hidroksiapatit terhadap porositas dan compressive strength resin akrilik HC. Metode: Jenis penelitian eksperimental laboratoris. Sampel penelitian 20 resin akrilik HC berbentuk silindris (6x3mm), dibagi menjadi 4 kelompok. Kelompok kontrol (tanpa penambahan HAP), kelompok HAP 2%, kelompok HAP 5%, dan kelompok HAP 10%. Permukaan sampel diteliti menggunakan SEM untuk porositasnya. Penghitungan compressive strength sampel menggunakan Universal Testing Machine (load cell 300kg/mm2). Hasil: Uji one-way ANOVA dan Tukey-HSD menunjukkan perbedaan signifikan (p<0,05) antara kelompok kontrol (90±13,5MPa) dengan 5%HAP (105±4,3MPa) dan 10%HAP (113±10,2MPa), begitu pula antara 2%HAP (96±8,4MPa) dengan 10%HAP. Uji SEM menunjukkan tidak adanya reaksi kimia antara HAP dan resin akrilik HC. Tampak pula bercak putih tersebar tidak merata pada permukaan sampel akrilik di kelompok-kelompok perlakuan. Bercak putih ditemukan meningkat sebanding dengan peningkatan konsentrasi HAP, dengan diameter yang semakin besar. Simpulan: Penambahan HAP pada basis resin akrilik HC mampu menurunkan tingkat porositas dan meningkatkan nilai compressive strength. Penurunan tingkat porositas meningkat seiring dengan penambahan HAP. Compressive strength yang paling tinggi didapatkan pada basis resin akrilik heat cured dengan penambahan 10% hidroksiapatit.Kata kunci: Compressive strength, uji SEM, resin akrilik heat cured, hidroksiapatit. ABSTRACT Introduction: Heat-cured acrylic resin has been commonly used as a denture base, whereas hydroxyapatite (HAP) is a crystalline molecule widely used in the field of dentistry. Previous research has been proofed that HAP could reduce the residual monomer of heat-cured acrylic resin, which will reduce the porosity level in advance, so it was expected for better mechanical properties. This research was aimed to analyse the effect of HAP addition towards the porosity level and compressive strength of heat-cured acrylic resin. Methods: An experimental laboratory research was conducted towards 20 cylindrical samples (6 x 3 mm) of heat-cured acrylic resins, which were divided into four groups: Control group (without HAP addition), 2% HAP addition group, 5% HAP addition group, and 10% HAP addition group. Compressive strength was tested using Universal Testing Machine (load cell of 300kg / mm2). Each sample surface porosity was observed using the scanning electron microscope (SEM). Results: One-way ANOVA and Tukey-HSD tests results showed significant differences (p < 0.05) between compressive strength in the control group (90 ± 13.5 MPa) compared to 5% (105 ± 4.3 MPa) and 10% HAP addition group (113 ± 10.2 MPa), significant differences were also shown between the 2% (96±8.4MPa) and 10% HAP addition group. SEM imaging showed that there was no chemical reaction between HAP and heat-cured acrylic resin. It showed uneven white spots in acrylic sample’s surface in all treatment groups. Those white spots were likely to be found more in the higher concentration of HAP, so did the diameter of white spots was also found more in the higher concentration. Conclusion: The addition of hydroxyapatite to the base of heat-cured acrylic resin can reduce the level of porosity and increase the compressive strength value. The decrease in the porosity level increases with the addition of hydroxyapatite. The highest compressive strength is obtained with the addition of 10% hydroxyapatite.Keywords: Compressive strength, SEM imaging, heat-cured acrylic resin, hydroxyapatite.

2021 ◽  
Vol 15 (2) ◽  
pp. 129-132
Author(s):  
Mohammad Forough Reyhani ◽  
Sheida Hosseinian Ahangarnezhad ◽  
Negin Ghasemi ◽  
Amin Salem Milani

Background. Calcium-enriched mixture (CEM) cement has been introduced and marketed as a biomaterial for use in furcal perforation repair and apexogenesis procedures, in which the compressive strength that indicates the material’s resistance against crushing is of utmost importance. This study evaluated the effect of various liquid-to-powder ratios on CEM cement’s compressive strength. Methods. One gram of the cement was mixed with 0.5, 0.34, and 0.25 mL of demineralized water and transferred to stainless steel molds (6 and 4 mm in height and diameter, respectively). Five cells in the mold were considered for each group. The compressive strength test was conducted using the universal testing machine after incubating for seven days under 95% humidity at 37°C. One-way ANOVA was applied for data analysis at P≤0.05 significance level. Results. The mean compressive strength in the liquid-to-powder ratios of 0.5, 0.34, and 0.25 were 3.4456, 3.2960, and 3.3485, respectively, with no significant differences between them. Conclusion. Under this study’s limitations, changing the liquid-to-powder ratio did not affect CEM cement’s compressive strength.


2016 ◽  
Vol 4 (2) ◽  
pp. 132-140
Author(s):  
Rezy Kurnia ◽  
Hidayati Hidayati

Disinfection is needed to avoid transmission of infectious agents. One of disinfectant solution used is sodium hypochlorite. Disinfection should be done without changing the quality of gypsum models, so the technique of mixing a disinfectant solution on gypsum powder can be used as an alternative. The purpose of this study was to determined the effect of mixing sodium hypochlorite to the compressive strength of type III gypsum product. The study was conducted at the Laboratory of Materials and Structures, Faculty of Engineering, Andalas University using laboratory experimental method with 30 pieces of type III gypsum models as samples. Samples were divided into 5 groups, that were mixed using 0.5% sodium hypochlorite, 1% sodium hypochlorite, 2% sodium hypochlorite, 5% sodium hypochlorite and distilled water as a control group. Measurement of the compressive strength was performed with a Universal Testing Machine (UTM). The results showed that the models were mixed with 0.5% sodium hypochlorite, 1% sodium hypochlorite, 2% sodium hypochlorite and 5% sodium hypochlorite reduced the average of the compressive strength compared to the models that are mixed with distilled water. One Way ANOVA test showed that was significantly differences (p<0.05) among groups of 0.5% sodium hypochlorite, 1% sodium hypochlorite, 2% sodium hypochlorite, 5% sodium hypochlorite and distilled water as a control group. It was concluded that there were effect of mixing sodium hypochlorite to reduced the compressive strength of type III gypsum product. Keywords: type III gypsum, compressive strength, sodium hypochlorite


2020 ◽  
Vol 2 (1) ◽  
pp. 001-011
Author(s):  
Dharma Satya Aprianto ◽  
Zullia Taftyanti

Among various ways to clean the denture based material is by its immersion  in disinfectant solution, such as sodium hypochlorite. Heat polymerized acrylic is denture based material that is easily broken because of its low transverse strength. This study was aimed to observe the transverse strength of denture based material heat polymerized acrylic resin after immersion in sodium hypochlorite. This research used 24 samples of heat cured acrylic resin plates measuring 65 mm long, 10 mm wide and 2.5 mm thick. The samples being divided into 4 groups were immersed in sodium hypochlorite 1% and water for 8 hours and 24 hours in 7 days. The transverse strength of acrylic plate were then  tested using universal testing machine. The measurement results were statistically analyzed employing “one way ANOVA”. The  result showed no significant changes on transverse strength of heat-cured acrylic plate. It was concluded that sodium hypochlorite solution did not provide any significant changes in the transverse strength of heat cured acrylic resin.


2020 ◽  
Vol 25 (6) ◽  
pp. 2095-2102
Author(s):  
LUMINIȚA OANCEA ◽  
◽  
LORELAI GEORGETA BILINSCHI ◽  
MIHAI BURLIBAȘA ◽  
ALEXANDRU PETRE ◽  
...  

Purpose of the study: The aim of the study is to analyze the way the disinfectants embedded in the plaster affect the setting linear dimensional stability, flexural and compressive strength of dental stone models. Material and Methods: Samples were made of type IV dental stone in which different disinfectants had been incorporated (sodium hypochlorite 1%, chlorhexidine 2%) in two concentrations (50%, 100%), thus obtaining four test groups. Mentioned parameters are measured using a micro comparison device and an universal testing machine, analyzing statistically the results in comparison with the control group, prepared by standard indications. Results: Disinfectants cause a decrease of the setting expansion value (ΔL) compared to the standard group in all type of mixing percentage. Variations of compressive and flexural strength are statistically significant, particularly when adding 100% of hypochlorite 1%. Conclusions: Within the limits of this study, replacing the distilled water with disinfectants, alter the value of setting expansion and cause the model dental stone to be brittle in compression and bending.


2019 ◽  
Vol 8 (1) ◽  
pp. 17
Author(s):  
Sefty Aryani Harahap ◽  
Lasminda Syafiar ◽  
Yosepha Yulinda Esdaria Lubis

Disinfectant by microwave energy is highly recommended as a solution to solve the problem of chemical disinfection on denture bases. One of the denture base materials is heat cured acrylic resin. Aim, to evaluate the effect of disinfectant by microwave energy with different time on the transversal strength of heat cured acrylic resin. 30 plates (n = 6) of heat cured acrylic resin with size 65x10x2,5 mm were divided into 5 groups (control; and microwave energy disinfected for 2, 4 , 6, and 8 minutes with 650 Watts of power). Transversal strength test was carried out using Torsee's Electronic System Universal Testing Machine with a test speed of 0.1 mm / second, and a load cell of 50 kgf. Data analyzed using one-way ANOVA and LSD pos hoc. Results, there were significant differences in the transverse strength among all groups (p <0.05). Mean values of all groups were 103.59 ± 0.66 MPa; 112.02 ± 2.10 MPa; 117.48 ± 1.73 MPa; 125.46 ± 2.25 MPa; and 135.89 ± 1.56 MPa respectively. Conclusion, the longer it is disinfected by microwave energy, the higher the transversal strength of heat cured acrylic resin.


Materials ◽  
2020 ◽  
Vol 13 (16) ◽  
pp. 3542
Author(s):  
Maja Bilić-Prcić ◽  
Valentina Brzović Rajić ◽  
Ana Ivanišević ◽  
Ana Pilipović ◽  
Sevil Gurgan ◽  
...  

The purpose of this study was to evaluate the effects of the incorporation of hydroxyapatite (HA) derived from cuttlefish bone on the mechanical properties of glass ionomer cements (GIC). Fuji II LC and Fuji IX GP Extra (GC Corporation, Tokyo, Japan) were used in the study. There were four groups (n = 11–18) for each material: a group without the addition of HA particles and three groups modified by incorporation of 2, 5, and 10 wt% HA. The tests were performed on a universal testing machine (Shimadzu, Duisburg, Germany) and descriptive statistics, two-way analysis of variance (ANOVA) for the comparison of three mechanical properties, and one-way ANOVA for the comparison of different concentrations for each material were performed. Regarding the Fuji IX groups, compressive strength (CS) and flexural strength (FS) were highest in the group without HA particles added. The differences in CS between the Fuji IX group without HA particles and the Fuji IX groups with 2 wt% HA and 10 wt% HA were significant. The Fuji II 5 wt% HA group exhibited higher diametral tensile strength (DTS) and CS than other Fuji II groups, but not significantly. The Fuji II group, modified with 10 wt% HA, exhibited significantly higher FS than the Fuji II group without HA particles (p < 0.05). Porous HA incorporated into the Fuji IX groups had a significant impact on mechanical properties only in the Fuji IX 5 wt% HA group. Fuji II groups modified with 10 wt% HA showed the most favorable results with respect to FS.


2015 ◽  
Vol 26 (4) ◽  
pp. 390-392
Author(s):  
Ana Paula Perroni ◽  
Érica Alves Gomes ◽  
Amália Machado Bielemann ◽  
Bruna Baseggio ◽  
Leonardo Federizzi ◽  
...  

<p>This study evaluated the tension force of cast frameworks made by the technique of framework cemented on prepared abutments using two different resin cements. Forty multi-unit abutment analogs were individually fixed with chemically cured acrylic resin inside PVC cylinders using a parallelometer. Brass cylindrical abutments were tightened to the multi-unit abutments to be used as spacers and then castable UCLA abutments were positioned above. These abutments were cast with Ni-Cr and then divided into 4 groups (n=10): cemented with RelyX U100(r); cemented with RelyX U100(r) and simulation of acrylic resin polymerization process; cemented with Multilink(r); and cemented with Multilink(r) and simulation of acrylic resin polymerization process. Abutments were cemented according to manufacturers' instructions. In a universal testing machine, tensile strength was applied in the direction of the long axis of the abutments at 1 mm/min crosshead speed until displacement of the luted abutments was obtained. The values of maximum tensile force (N) required for the displacement of the luted abutments were tabulated and analyzed statistically by one-way ANOVA with a 95% confidence level. No statistically significant difference was found among the groups (p>0.05). There was an increase in mean tension force when the specimens were subjected to the simulation of acrylic resin polymerization process, but the results did not differ statistically. Both resin cements presented positive results as regards the retention of luted abutments on their respective multi-unit abutments. Both materials may be indicated for the technique of framework cemented on prepared abutments when professionals pursuit better adaptation of implant-supported frameworks.</p>


2017 ◽  
Vol 4 (02) ◽  
pp. 183
Author(s):  
Zuriah Sitorus ◽  
Awan Maghfirah ◽  
Yoshephin Romania ◽  
Syahrul Humaidi

<p>The research is aimed to investigate the possibility of acrylic-reinforced glass fibre as a denture. Short glass fibre was made by variation of 4mm, 6 mm and 8mm. The results showed a good adhesion between glass fibre and acrylic resin with an optimum composition of the denture (acrylic: oil : glass fibre = 10 gr : 4.5 mL : 0.13 gr) was achieved. The density test was conducted by using Archimedes’ method, whereas compressive strength and tensile strength by using Universal Testing Machine (UTM). The results showed that glass fibre can be used to enhance the mechanical properties of acrylic resin. The optimum composition was achieved when 6 mm fibre had been added-in with a density of 1.2256 gr/cm3. A compressive strength of 76.623 MPa and a tensile strength of 71.207 MPa were recorded, these values can be applied as a denture.</p>


2018 ◽  
Vol 30 (3) ◽  
pp. 189
Author(s):  
Actara Rahmadita ◽  
Dwi Tjahyaning Putranti

Pendahuluan: Resin akrilik polimerisasi panas (RAPP) merupakan bahan basis gigi tiruan yang paling banyak digunakan, namun memiliki sifat kekuatan tarik dan tekan yang rendah, sehingga diperlukan modifikasi dengan penambahan bahan penguat pada RAPP berupa aluminium oksida (Al2O3) atau alumina. Tujuan penelitian untuk menganalisi pengaruh penambahan aluminium oksida pada bahan basis gigi tiruan RAPP terhadap kekuatan tarik dan tekan. Metode: Jenis penelitian eksperimental laboratoris. Sebanyak 25 sampel berbentuk flat dumbbell shaped berukuran 60x12x3,9 (mm) untuk uji kekuatan tarik dan 25 sampel  berbentuk balok dengan ukuran 10x10x4 (mm) untuk uji kekuatan tekan. Pencampuran bubuk resin-aluminium oksida konsentasi 0,5%, 1,5%, 2,5% dan 3,5% dengan cairan resin dilakukan secara manual. Sampel direndam dalam air dan dimasukkan ke dalam inkubator. Uji dilakukan menggunakan universal testing machine dengan beban 1000N dan kecepatan crosshead 1mm/menit. Data dianalisis dengan uji ANOVA satu arah dan uji LSD. Hasil: Nilai kekuatan tarik kelompok kontrol dan keempat kelompok perlakuan penambahan aluminium oksida 0,5%, 1,5%, 2,5 %, 3,5% berturut turut adalah 50,867 MPa, 47,895 MPa, 45,107 MPa, 42,476 MPa, dan 39,753 MPa; sedangkan nilai kekuatan tekan kelompok kontrol dan keempat kelompok perlakuan penambahan aluminium oksida 0,5%, 1,5%, 2,5%, 3,5% berturut turut adalah 88,267 MPa, 106,085 MPa, 122,283 MPa, 135,367 MPa, dan 156,571 MPa. Penambahan bubuk aluminium oksida pada RAPP dapat menurunkan kekuatan tarik dan meningkatkan kekuatan tekan secara signifikan (p=0,0001 (p<0,05)), seiring dengan meningkatnya jumlah konsentrasi aluminium oksida yang ditambahkan. Simpulan: Penambahan aluminium oksida pada bahan basis gigi tiruan resin akrilik polimerisasi panas berpengaruh terhadap kekuatan tarik dan tekan.Kata kunci: Resin akrilik polimerisasi panas, aluminium oksida, kekuatan tarik, kekuatan tekan. ABSTRACT            Introduction: Heat-polymerised acrylic resin (HPAR) is the most widely used denture base material but has a low tensile and compressive strength thus modification is needed by adding reinforcement in the form of aluminium oxide (Al2O3) or alumina. The research objective was to analyse the effect of adding aluminium oxide on the tensile and compressive strength of HPAR denture base material. Methods: An experimental laboratory research was conducted towards the total of 25 samples in the form of flat dumbbell shape sized 60 x 12 x 3.9 mm for the tensile strength test, and 25 samples in the form of blocks with the size of 10 x 10 x 4 mm for the compressive strength test. The mixture of powdered aluminium oxide resin with the concentrations of 0.5%, 1.5%, 2.5%, and 3.5% with a liquid resin was carried out manually. The sample was then immersed in the water and put in an incubator. The test was performed using a universal testing machine with 1000 N loads and 1 mm/minute crosshead speed. Data obtained were analysed using the one-way ANOVA and LSD test. Result: The tensile strength values of the control group and all four treatment groups added with 0.5%, 1.5%, 2.5%, and 3.5% aluminum oxide were 50.867 MPa, 47.895 MPa, 45.107 MPa, 42.4476 MPa and 39.753 MPa respectively, while the compressive strength values were 88.267 MPa, 106.085, 122.283 MPa, 135.367 MPa, and 156.571 MPa consecutively. Addition of aluminium oxide powder to the HPAR can significantly reduce the tensile and compressive strength (p = 0.0001 (p < 0.05)) along with increasing concentration. Conclusion: Addition of aluminium oxide towards the HPAR denture base affected its tensile and compressive strength.Keywords: Heat-polymerised acrylic resin, aluminium oxide, tensile strength, compressive strength.


e-GIGI ◽  
2014 ◽  
Vol 2 (2) ◽  
Author(s):  
Dwi Cahya Fitriyana ◽  
D. H. C. Pangemanan ◽  
Juliatri .

Abstract: The immersion of GIC type II in acid drink like isotonic drink could reduce the compressive strength (CS) of GIC type II. This is due to the matrix degradation process of  GIC in acid condition. But on the other hand, there is artificial saliva that can neutralize this condition. Purpose: Purpose of this study was to evaluate the effect of artificial saliva on compressive strength of GIC type II immersed in isotonic drink. Method: The GIC specimens of 6mm x 6mm x 12mm (length x width x depth) were immersed for 24 hours in water, 24 hours in isotonic drink, 24 hours in isotonic drink and continue with 72 hours in artificial saliva, 48 hours in isotonic drink, and 48 hours in isotonic drink and continue with 144 hours in artificial saliva. The compressive strength was determined using Universal Testing Machine with a crosshead speed of 0.5 mm/min. Statistical analysis was performed by one-way ANOVA and post-hoc LSD test ( = 0.05). Result: Statistic test shows significant difference of CS (p<0,05). Conclusion: conclusion of this study artificial saliva gives effect to the rising of the compressive strength of GIC type II immersed in isotonic drink. Keywords: Isotonic drink, artificial saliva, compressive strength, Glass Ionomer Cement       type II.  Abstrak: Perendaman SIK tipe II dalam minuman asam seperti minuman isotonik dapat mengurangi kekuatan tekan SIK tipe II. Hal ini disebabkan proses degradasi matriks SIK pada kondisi asam. Namun di sisi lain, saliva buatan yang dapat menetralkan kondisi ini. Tujuan: untuk untuk mengetahui pengaruh saliva buatan terhadap kekuatan tekan SIK yang direndam dalam minuman isotonik. Metode: Spesimen SIK tipe II berukuran 6mm x 6mm x 12 mm (panjang x lebar x tinggi) direndam selama 24 jam dalam air, 24 jam di dalam minuman isotonik, 24 jam di dalam minuman isotonik dan lanjutkan dengan 72 jam pada saliva buatan, 48 jam di minuman isotonik, dan 48 jam di minum isotonik dan lanjutkan dengan 144 jam dalam saliva buatan. Kekuatan tekan diukur menggunakan Universal Testing Machine dengan kecepatan 0,5 mm / min. Analisis statistik dilakukan dengan one-way ANOVA dan post-hoc uji LSD ( = 0,05). Hasil: Uji statistik menunjukkan perbedaan yang signifikan dari kekuatan tekan (p <0,05). Simpulan: terdapat pengaruh saliva buatan terhadap kekuatan tekan SIK tipe II yang direndam dalam minuman isotonik. Kata kunci: minuman isotonik, saliva buatan, kekuatan tekan, Semen Ionomer Kaca tipe II.


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