scholarly journals Effects of organic acid on the physicochemical properties of gelatine extracted from Fringescale sardinella (Sardinella fimbriata) bones

Food Research ◽  
2021 ◽  
Vol 5 (4) ◽  
pp. 294-302
Author(s):  
N.M. Arshad ◽  
M. Abd. Ghaffar ◽  
N.F. Mohtar

Gelatine from marine sources especially from the fish becomes a popular alternative to replace the commercial gelatines from bovine and porcine. Fringescale sardinella (Sardinella fimbriata) is commonly used in the fish processing industry and has a high potential to produce gelatine from its by-products. The extraction of gelatine is one of the most important steps that influence its functional properties. Inorganic acid was commonly used in the extraction, however, nowadays it faces some issues due to health safety and its effect on the environment. The aim of this study was to assess the effects of organic acid (fruit vinegar) as a replacement for inorganic acid (hydrochloric acid) during extraction on the physicochemical properties of S. fimbriata gelatine. The extracted gelatines were characterized in terms of their physico-chemical properties such as the yield percentage, gel strength, melting point, molecular weight, structural composition, and amino acid analyses. Results showed that gelatine extracted with organic acid demonstrated low yield percentage (2.9±0.01%) and poor gel strength (75.9±1.06 g) and melting point (22.0±1.00°C) values compared to the standard. This gelatine also demonstrated a low amount of proline and hydroxyproline contents, which were 43.77±8.21 g/mg and 34.99±6.50 g/mg, respectively. Overall findings have suggested that different types of acid used in the extraction resulted in different physico-chemical properties of the gelatine. Such findings suggested that S. fimbriata bone hold the potential to be an alternative source for vast applications in industries. Further studies may focus on different concentrations of acid used in the extraction process. Such findings will help to improve S. fimbriata bone gelatine properties for extended uses in various industries.

2021 ◽  
Vol 134 (3) ◽  
pp. 11-17
Author(s):  
I. G. Yashchenko ◽  
◽  
Y. M. Polishchuk ◽  

The article is devoted to the urgent problem of studying the features of the properties of poorly studied oils at great depths (more than 4,500 m), the need for development of which is caused by the continuing decline in oil production in traditional oil producing provinces. The analysis of the spatial distribution of reserves across the continents and countries of deep-seated oils and changes in their physico-chemical properties and the occurrence conditions, which made it possible to identify their main features. The studies used information on 21067 oil samples from 167 oil-bearing basins of the world, obtained from the database on the physicochemical properties of oils. The features of the physicochemical properties of deep-seated oils have been established, which are manifested in a decrease in the density and viscosity of oils, in a decrease in the content of sulfur and asphalt-resinous substances, and in an increase in the content of light fractions and oil gas in comparison with oils of small and medium depths.


2017 ◽  
Vol 103 ◽  
pp. 07012
Author(s):  
S.W. Yeo ◽  
Felix N. L. Ling ◽  
V. S. Low ◽  
K. L. Toh

RSC Advances ◽  
2019 ◽  
Vol 9 (34) ◽  
pp. 19828-19836 ◽  
Author(s):  
Li Yuan ◽  
Jiamei Yu ◽  
Jianlou Mu ◽  
Tong Shi ◽  
Quancai Sun ◽  
...  

This work studied the effects of KGM with different degrees of deacetylation (DDs) on the physicochemical properties of silver carp (Hypophthalmichthys molitrix) surimi gels.


LWT ◽  
2019 ◽  
Vol 114 ◽  
pp. 108414 ◽  
Author(s):  
Aleksandra Torbica ◽  
Dubravka Škrobot ◽  
Elizabet Janić Hajnal ◽  
Miona Belović ◽  
Na Zhang

2017 ◽  
Vol 5 (3) ◽  
pp. 263-273 ◽  
Author(s):  
Sirikhwan Tinratat ◽  
Monnipha Sila-asna

The utilization of fish processing waste for value-added by-products has attracted considerable attention. The present study aims to evaluate the gelatin extracted from fish skin and bone for application to Panna cotta products. The optimum conditions of gelatin extraction from Sea Bass, Nile tilapia and Red tilapia skin and bone were at 80 and 90 °C for 2.5 h, respectively. Nile tilapia skin and bone gelatins represent the most hydroxyproline content of 45.38 ±1.32 and 23.28±1.12 g, respectively (p0.05). Nile tilapia skin gelatin has the strength gel of 860.50 g which higher than Nile tilapia bone. The foaming ability normally increases at pH 3 to 6 and has emulsifier ability. Sodium chloride (NaCl) and activated carbon have effecting to remove the color and odor of extracted gelatin. Nile tilapia bone gelatin is the most suitable as an ingredient for Panna Cotta recipe. Panna Cotta milk mix berries has the maximum satisfaction levels in the female and male group of 4 to 5 (like very much to like extremely) for their flavor and texture by surveying satisfaction of customer in 5 points hedonic scale (30 persons). The average costs of production are between 0.56-0.71 US$/cup (200 g). Therefore, it can be concluded that fish gelatin can apply the ingredient in Panna Cotta Recipe or cook with another kind of foods. The extracted fish gelatin has desirable chemical and physical properties. It is suitable as a food ingredient which aspects as an alternative source of mammalian gelatin.


2020 ◽  
Vol 8 (1) ◽  
pp. 14
Author(s):  
Miftakhul Ulumiah ◽  
Mochammad Amin Alamsjah ◽  
Kustiawan Tri Pursetyo

Gelatin is a simple protein obtained from the partial hydrolysis of collagen from the skin, bones, joints and connective tissue of animals. One potential material for the manufacture of gelatin is fish bone milkfish (Chanos chanos). Gelatin derived from fish bones with acid process is able to change the triple helix collagen fibers into a single chain, whereas the solvent base only produce double chain. Demineralization of bone or fish skin should use a weak acid is acetic acid, because when using strong acids will produce a strong scent and color gelatin becomes dark. This study aims to determine the effect of the use of acetic acid to the production of fish bone gelatin and the concentration of acetic acid is necessary to produce gelatin with physical and chemical properties of the best. This study uses a Completely Randomized Design (CRD) with four treatments and five replications. The treatments used in this study is the concentration of acetic acid 2%, 4%, 6% and 8%. Based on the research, it was found that the acetic acid solvent effect on the value of the yield and gel strength, but has no effect on the pH value and viscosity. Acetic acid concentration 8% give 4.102% yield value; pH value (acidity) 4.98; 134.313 bloom gel strength and viscosity of 3.6 cP. FTIR analysis results indicate that the fish bone gelatin produced from this research have the same functional group with commercial gelatin.


2013 ◽  
Vol 1 (1) ◽  
pp. 77-82 ◽  
Author(s):  
D Gernah ◽  
P Gbakaan

Effect of storage and concentration of potassium carbonate (K2CO3) on the viscosity and related physico – chemical properties of genger (Bombax costatum) powder was determined. Genger powder was stored for a period of four (4) months (May-August) at 30oc ± 5oc under varying concentrations of K2CO3: 0%, 5%, 10% and 15% in two containers (plastic, giving samples A – D and metal tins, giving samples A1 – D1). Thereafter, the moisture and crude fat contents, water absorption capacity, least gelation concentration, effect of K2CO3 concentration on gel strength and viscosity of the stored powders were determined, using standard methods of analysis, with fresh powder (analyzed before storage) as control. Moisture content decreased significantly (p < 0.05) from 8.37% to 3.04% and 2.00% in samples D and D1 respectively, while crude fat content increased significantly (p < 0.05) from 2.50% to 7.50% and 10.05% in the same samples. Water absorption capacity also increased significantly (p < 0.05) from 6.4g/g to 6.40g/g in the fresh sample to 7.30g/g and 8.30g/g in samples D and D1 respectively. Gelation capacity increased considerably, with 15% K2CO3 giving very strong gels at 1.50% concentration. The overall viscosity increased significantly (p < 0.05) with increase in concentration of (K2CO3) from 64.00FN to 110.00FN after storage. Generally, samples stored in metal tin gave better results than those in the plastic container.


2019 ◽  
Vol 9 (4-s) ◽  
pp. 338-342
Author(s):  
Shyam Bihari Sharma ◽  
Suman Jain ◽  
K. Ganesan

Microspheres are one of the novel drug delivery system which possess several applications and are made up of assorted polymers. Microspheres can be defined as solid, approximately spherical particles ranging in size from 1 to 1000 μm range in diameter having a core of drug and entirely outer layers of polymers as coating material. They are made up of polymeric, waxy or other protective materials i.e. biodegradable synthetic polymer and modified natural products such as starches, gums, proteins, fats and waxes. Preformulation is a group of studies that focus on the physicochemical properties of a new drug candidate that could affect the drug performance and the development of a dosage form. This couldprovide important information for formulation design or support the need for molecular modification. Every drug has intrinsic chemical and physical properties which has been consider before development of pharmaceutical formulation. This property provides the framework for drugs combination with pharmaceutical ingredients in the fabrication of dosage form. Objective of preformulation study is to develop the elegant, stable, effective and safe dosage form by establishing kinetic rate profile, compatibility with the other ingredients and establish Physico-chemical parameter of new drug substances. The purpose of the present study was to systematically investigate some of the important physicochemical properties of pralidoxime chloride for preparation of microspheres. The physicochemical properties such as solubility, pKa, dissolution, melting point, assay development, excipient compatibility etc. of pralidoxime chloride was carried out. Before selection of excipients, the Preformulation study of drug pralidoxime is completed for successful formulation of microspheres. The result of Preformulation studies shows good flow properties, excipient compatibility, solubility efficiency and melting point. From this study we concluded that pralidoximewith HPMC and EC can be used to formulate pralidoxime microspheres for modified release. Keywords: Microspheres, Preformulation, Pralidoxime chloride, Physico-chemical parameter.


2020 ◽  
Vol 32 (6) ◽  
pp. 1433-1436 ◽  
Author(s):  
Tran Thi Kim Ngan ◽  
Nguyen Van Muoi ◽  
Pham Minh Quan ◽  
Mai Huynh Cang

This study attempted the extraction of essential oils from the peels of pomelo (Citrus grandis L.) grown in Ben Tre province, Vietnam through hydrodistillation method. In addition, the chemical composition and physio-chemical properties of the essential oils were reported. The results showed that the extraction yield of the extraction process achieved about 1.67%. The physico-chemical index of essential oils is determined by specific gravity (0.8572 g/cm3), acid index (0.3556 mg KOH/g), ester index (2.4216 mg KOH/g), and refractive index (1.476). The GC-MS analyses of the oil indicated the component with highest content in the oil was α-limonene (96.491%), followed by α-pinene (0.686%), β-pinene (0.248%), β-myrcene (1.644%), α-phellandrene (0.793%) and β-cis-ocimene (0.138%). These results suggested that wastes from fruit peeling process can be converted into a new material source with great potential for industrial use.


Author(s):  
Meysam Shirmohammadi ◽  
Esmat Mohammadinasab ◽  
Zakiyeh Bayat

: In the present study the applicability of various molecular descriptors was tested for the QSPR study on 40 quinolones derivatives. The relationship between some of the molecular indices with physicochemical properties such as refractive index (n), polarizability (α) and HOMO-LUMO energy gap (ΔEH-L) was represented. At first, the chemical structure of quinolones derivatives was optimized by Gaussian 98 program and ab initio method at the #HF/6-31++G**level, and then the physicochemical properties such as refractive index, polarizability and HOMO-LUMO energy gap were calculated. Genetic algorithm using multiple linear regression (GA-MLR) with backward method by SPSS software was used for obtaining properties. The analytical powers of the established theoretical models were discussed using leave-one-out (LOO) cross-validation technique. A multi-parametric equation containing maximum three descriptors with suitable statistical qualities was obtained for predicting the studied properties.


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