scholarly journals Antioxidant capacity of pitcher (Nepenthes) extract on oxidative rancidity of sun-dried squid

Food Research ◽  
2021 ◽  
Vol 5 (5) ◽  
pp. 167-173
Author(s):  
N.P. Minh
Keyword(s):  
Peroxide Value ◽  
Thiobarbituric Acid ◽  
Acid Value ◽  
Butylated Hydroxyanisole ◽  
Oxidative Rancidity ◽  
Carbonyl Value ◽  
Promising Alternative ◽  
Great Capacity ◽  
Significant Difference ◽  
The Impact

Consumers demand new biologically natural-active ingredients with a great capacity to promote a healthier advantage and free from toxicity. Pitcher (Nepenthes) is one of the naturally carnivorous climber herbs. Extract from Nepenthes plant contains numerous beneficial bioactivity characteristics. This research compared the impact of 0.05% pitcher extract demonstrated with 10 ppm butylated hydroxyanisole on the accumulation of acid value, peroxide value, carbonyl value and thiobarbituric acid during 12 months of storage. Results showed that there was no significant difference between 0.05% pitcher extract and 10 ppm butylated hydroxyanisole in respect of acid value, peroxide value, carbonyl value and thiobarbituric acid during preservation of the dried squid. Pitcher extract would be a promising alternative to replace synthetic antioxidants to overcome oxidative rancidity in the dried seafood.

Characterization and Stability Studies of Egusi Melon Seed Oil (Citrullus colocynthis L.)

2021 ◽  
Vol 46 (2) ◽  
Author(s):  
C.O. Ajenu ◽  
M.E. Ukhun ◽  
C. Imoisi ◽  
E.E. Imhontu ◽  
L.E. Irede ◽  
...  
Keyword(s):  
Fatty Acid ◽  
Free Fatty Acid ◽  
Iodine Value ◽  
Peroxide Value ◽  
Seed Oil ◽  
Thiobarbituric Acid ◽  
Acid Value ◽  
Melon Seed ◽  
Thiobarbituric Acid Value ◽  
Melon Seed Oil

The physical value of oil depends upon its chemical composition, even today these values play a vital role while using different oil for industrial products and also, despite the vast nutritional and medicinal significance of egusi melon, there are little details on the shell life and stability of its oil over time. Therefore, the influence of time and temperature on melon seed oil was investigated at temperatures of 0oC and 30oC at different weeks to ascertain its physicochemical value and storage stability. For week zero, at 0oC and ambient temperature (30oC), the result revealed iodine value 124.09, Acid value 3.64 mgNaOH/g, Free Fatty Acid value 1.84 mgNaOH/g, Saponification 217.35 mgKOH/g, Peroxide value 1.25 mg/g oil, pH 5.89 and thiobarbituric acid value 0.1383 respectively. In the 5th week, at 30oC, the result revealed iodine value 91.1543, acid value 12.8921 mgNaOH/g, free fatty acid value 6.4988 mgNaOH/g, Saponification 346.42 mgKOH/g, Peroxide value 9.5mg/g oil, pH 3.2 and thiobarbituric acid value 0.413 respectively. Also at 0oC in the 5th week, the results were observed as follow: Iodine value 102.53, Acid value 7.96 mgNaOH/g, Free Fatty Acid value 4.01 mgNaOH/g, saponification 287.51 mgKOH/g, Peroxide value 6.1 mg/g oil, pH 5.05, and thiobarbituric acid value 0.2658 respectively. Refrigeration (0oC) of oil reduced the rate of most of the oxidative deterioration that produces rancidity. These values are within recommended range for edible oils. These results indicate that egusi melon oil could be a good source of table oil. The statistical results show that there was a significant difference between the melon seed oil stored at 0oC and 30oC (P < 0.001).

Compositional characteristics of cherry kernel oil as influenced by gamma irradiation and storage periods

2020 ◽  
pp. 108201322095673
Author(s):  
M Al-Bachir ◽  
Y Koudsi
Keyword(s):  
Refractive Index ◽  
Gamma Irradiation ◽  
Iodine Value ◽  
Peroxide Value ◽  
Research Work ◽  
Thiobarbituric Acid ◽  
Acid Value ◽  
Thiobarbituric Acid Reactive Substances ◽  
Saponification Value ◽  
And Storage

This research work was undertaken to evaluate the physicochemical parameters of oil from the cherry kernel non-irradiated and irradiated at 3 and 6 kGy of gamma irradiation for two storage periods (0 and 12 months). The acid value, peroxide value, thiobarbituric acid reactive substances value, iodine value, saponification value refractive index (peroxide value), and the color parameters of cherry kernel oils were determined. The results indicated that the extracted cherry kernel oils were liquid at room temperature with color varying from light yellow to deep red. The physicochemical properties of cherry kernel oils including acid value, peroxide value, thiobarbituric acid reactive substances, iodine value, saponification value, and refractive index values were 1.19 mg KOH g−1, 9.01 meq2 kg−1, 0.014 mg MDA kg−1, 99.48 KOH g−1 I2 100 g−1, 194.50 mg KOH g−1, and 1.472, respectively. Generally, gamma irradiation doses and storage time increased acid value, peroxide value, thiobarbituric acid reactive substances, and refractive index value of cherry kernel oils, whereas no significant (p > 0.05) change due to irradiation was recorded in iodine value, saponification value, and in color parameter (L*, a*, b*, and ΔE values) of cherry kernel oils. However, the properties of cherry kernel oils revealed that the cherry kernel is a good source of oil which could be used for industrial purposes.

Some Physical, Chemical and Sensory Properties of Fish Oil Extracted from Fish Wastes by Physical and Chemical Methods

2021 ◽  
Vol 5 (1) ◽  
pp. 152-162
Author(s):  
Anwar Salih
Keyword(s):  
Common Carp ◽  
Physical Method ◽  
Thiobarbituric Acid ◽  
Acid Value ◽  
Sensory Properties ◽  
Acid Fermentation ◽  
Chemical Methods ◽  
Physical Chemical ◽  
Significant Difference ◽  
Physical And Chemical

This study was carried out to assess some physical, chemical and sensory properties of fish waste oil extracted by two different methods: physical (boiling) and chemical (acid fermentation). Samples of common carp viscera were collected from local markets in the city of Basrah, which included viscera of the common carp Cyprinus carpio. The most prominent and significant difference was the extraction yield which amounted to 57.14% vs 35.71% (vol./wt.) for the physical and chemical methods, respectively. Other physical properties: refraction index, specific weight, specific gravity, viscosity, cloud point and pour point, Were superior in physical method of the physical method. Measured chemical indices (free fatty acids FFA, fatty acid profile, peroxide value, iodine number and Thiobarbituric acid value TBA) indicated some variability between oil types, the most obvious was FFA which increased significantly from 0.107 to 0.205% for physical and chemical methods, respectively. The sensory tests (color and odor) were in favor of oil extracted with the physical method characterized by a light amber color and a mild fishy flavor.

Study on Antioxidative Effect of Lycopene to the Photosensitized Oxidation of Soybean Oil

2011 ◽  
Vol 250-253 ◽  
pp. 3971-3974
Author(s):  
Xi Hong Li ◽  
Jin Du ◽  
Chang Liu ◽  
Sen Wan ◽  
Yao Tang ◽  
...  
Keyword(s):  
Fatty Acid ◽  
Soybean Oil ◽  
Peroxide Value ◽  
Free Acid ◽  
Control Sample ◽  
Thiobarbituric Acid ◽  
Acid Value ◽  
Mean Value ◽  
Antioxidative Effect ◽  
Photosensitized Oxidation

A research was designed to study the effect on inhibiting the photosensitized oxidation of natural (lycopene) and synthetic (tertiary butylhydroquinon, TBHQ) antioxidant in soybean oil. In the presence of light, mean value of all samples revealed that a significant increase in peroxide value, free acid value and thiobarbituric acid (TBA) assay. The addition of lycopene and TBHQ reduced the peroxide value of control sample from 12.810 to 7.378 and 9.882 meq/kg, respectively. And TBA was found to be 0.163 in control sample, while the values of lycopene and TBHQ treatments were 0.080 and 0.134. Meanwhile, the oil samples were treated with different does of lycopene under light, the rate of oxidation increased considerably with a corresponding decrease in the content of lycopene. The data showed that oils containing 300 ppm lycopene had the lowest levels of free fatty acid value.The results indicated that lycopene in soybean oil exposed to light were found to be effective in inhibiting lipid oxidation.

BIOCHEMICAL CHANGES IN BEEF PATTIES BOILED WITH ETHANOL EXTRACT OF THE ROOT OF Glycyrrhiza glabra LINN

2021 ◽  
Vol 5 (1) ◽  
pp. 202-209
Author(s):  
C. O. Ugbeni ◽  
D. O. Idiakheua ◽  
U. O. Ejovwokoghene
Keyword(s):  
Peroxide Value ◽  
Iron Content ◽  
Storage Time ◽  
Statistical Difference ◽  
Ethanol Extract ◽  
Acid Value ◽  
Heme Iron ◽  
Glycyrrhiza Glabra ◽  
Malondialdehyde Content ◽  
Significant Difference

The use of spices in boiling of meat is a common phenomenon. The root of Glycyrrhiza glabra is used locally as spice for met. This work was design to determine the effect of ethanol extract of Glycyrrhiza glabra on malondialdehyde content, percentage Metmyoglobin content, acid value, Heme-iron content and peroxide value of beef stored at 4oc for a storage time of 0 to 18 hours was evaluated. Samples were taken at interval of 6 hours for analysis of the biochemical parameters under study. The statistical difference observed in Acid value, Malondialdehyde content, Heme iron content and peroxide value showed no significant difference, all having P≥0.05 in beef treated with ethanol extract of Glycyrrhiza glabra when compared to the control. On the other hand, the statistical difference in percentage metmyoglobin content when compared to the control at 0 hour interval was significant having P≤0.05, then at other distinct time interval showed no significant difference having P≥0.05. Thus, this study revealed that the extract of Glycyrrhiza glabra have a decreased antioxidant property against rancidity in beef samples and peroxide formation, although the stability of antioxidant, antimicrobial properties of Glycyrrhiza glabra decreases with storage time resulting in the variation of percentage Metmyoglobin values, Malondialdehyde values and Heme iron values, Acid value and peroxide value of beef, which indicates it may not be a good spice for beef

scholarly journals AKTIVITAS SENYAWA BIOAKTIF SELADA LAUT (Ulva lactuca) SEBAGAI ANTIOKSIDAN PADA MINYAK IKAN The Activity of Bioactive Compounds from Sea Lettuce (Ulva lactuca) as Antioxidant in Fish Oil

2017 ◽  
Vol 12 (1) ◽  
pp. 12
Author(s):  
Basyrowi Arbi ◽  
Widodo Farid Ma’ruf ◽  
Romadhon Romadhon
Keyword(s):  
Fatty Acids ◽  
Fish Oil ◽  
Peroxide Value ◽  
Storage Time ◽  
Unsaturated Fatty Acids ◽  
Fatty Acid Content ◽  
Thiobarbituric Acid ◽  
Ulva Lactuca ◽  
Research Results ◽  
Significant Difference

ABSTRAK Minyak ikan adalah produk perikanan yang mempunyai asam lemak tak jenuh tinggi yang rentan akan oksidasi. Penghambatan oksidasi dilakukan dengan penambahan antioksidan pada minyak. Penggunaan bahan alami sebagai antioksidan dari U. lactuca mampu menghambat oksidasi tersebut. Tujuan penelitian ini adalah untuk mengetahui efektifitas antioksidan selada laut (U. lactuca) dalam menghambat oksidasi.  Materi yang digunakan dalam penelitian ini adalah ekstrak U. lactuca, dan minyak ikan. Metode penelitian yang digunakan adalah experimental laboratories dengan menggunakan Rancangan Acak Lengkap (RAL) faktorial yaitu faktor konsentrasi ekstrak U. lactuca (0%; 0,1%; 0,2% dan 0,3%) dan faktor lama penyimpanan (hari ke-0, hari ke-5 dan hari ke-10). Data peroxide value (PV) dan thiobarbituric acid (TBA) dianalisis menggunakan uji ANOVA, dilakukan uji lanjut Beda Nyata Jujur (BNJ), jika ada interaksi perlakuan. Hasil penelitian pendahuluan didapatkan rendemen ekstrak U. lactuca dengan pelarut etanol 96% sebesar 13,549%, nilai fenol 4,59%, flavonoid 0,59% dan aktivitas antioksidan IC50 sebesar 60,975 ppm (kuat). Hasil uji asam lemak pada minyak ikan dengan GC-MS menunjukkan kandungan asam lemak yang paling banyak adalah asam lemak tak jenuh (asam linoleat (omega -6) dan (omega-3)). Hasil penelitian utama didapatkan nilai PV berkisar antara 20,141 sampai 38,196 mEq/kg, dan nilai TBA berkisar antara 10,794 sampai 32,592 mg malonaldehid/kg pada hari ke-0. Berdasarkan hasil penelitian menunjukkan bahwa adanya interaksi antara konsentrasi ekstrak U. lactuca dan lama penyimpanan berpengaruh nyata (P<0,05).  Ekstrak U. lactuca 0,2% menghasilkan angka peroksida  terendah  yaitu 25,606±0,116 mEq/kg, dan  0,1% menghasilkan angka TBA terendah yaitu 26,802  ±0,309 malonaldehide/kg pada hari ke-10. Kata kunci: Ekstrak U. lactuca, Oksidasi, Minyak Ikan,  Antioksidan  ABSTRACT Fish oil is a fishery product that contains  high amount of unsaturated fatty acids, which was easily  oxidated. This oxidation process can be inhibited by adding antioxidants. The use of natural antioxidants from U. lactuca known  can inhibits the oxidation. The aim of this research was  examinated the effectiveness of antioxidants from sea lettuce (U. lactuca) in inhibiting oxidation. Materials used in this research were U. lactuca extract, and fish oil. The methods used are experimental laboratories, and analyzed using Completely Randomized Design (CRD) factorial pattern is divided by a factor of U. lactuca extract concentrations (0%, 0.1%, 0.2% and 0.3%) and factor storage time (days 0, day 5 and day 10). The peroxide value (PV) and thiobarbituric acid (TBA) were analyzed using ANOVA test, then further carried test Honestly Significant Difference (HSD), a treatment interaction. Preliminary results obtained were the yield of U. lactuca extract with 96% ethanol was 13.549%, the phenol content  was 4.59%, flavonoids was 0.59%, and the antioxidant activity of IC50 was 60.975 ppm (strong). The results analyzing of fatty acids in fish oil by GC-MS showed that the fatty acid content is at most unsaturated fatty acids. The main research results were PV values obtained were range from 20.141 to 38.196 mEq/kg, and TBA values were ranged from 10.794 to 32.592 mg/kg. Based on the research results show that the interaction between U. lactuca extract concentration and storage time significantly (P<0,05) . The result of 0,2% U. lactuca exctract  contain peroxide value 25,606±0,116 mEq/kg, and  0,1 % exctract containt TBA value 26,802±0,309 malonaldehide/kg  in  the tenth day. Keywords: U. lactuca, Oxidation, Fish Oil, Antioxidant

scholarly journals Determination of Physico-chemical Properties, Cholesterol and Vitamin A Levels of Vegetable Oils commonly Sold in Ado Ekiti Metropolis

2021 ◽  
pp. 53-61
Author(s):  
F. A. Ishaya ◽  
A. A. Oladejo ◽  
A. B. Olaoye
Keyword(s):  
Vitamin A ◽  
Vegetable Oils ◽  
Peroxide Value ◽  
Essential Fatty Acids ◽  
Chemical Properties ◽  
Acid Value ◽  
Cholesterol Content ◽  
Human Beings ◽  
Wide Range ◽  
Significant Difference

Edible vegetable oils are very important resource that are in high demand globally, and used in a variety of ways as they are considered a concentrated source of energy for human beings and carriers of oil-soluble vitamins which supply the essential fatty acids that are required for a wide range of biological and physiological functions. This work was aimed at evaluating the physicochemical properties, cholesterol content and analyzes the vitamin A contents of commonly sold vegetable oils in Ado Ekiti metropolis. The physicochemical parameters such as density, acid value, iodine value, peroxide value and saponin value, cholesterol content as well as Vitamin A content were all analyzed using standard analytical methods. Results of the physicochemical analysis showed that there was no significant difference (p>0.05) in the densities of the oil samples, It was observed that sample 4 oil showed maximum (1.58 mgKOH/g) and sample 6 showed minimum (1.38 mg KOH/g) acid values. Highest iodine values were observed in sample 8 (68.13 g/I2/100g) and lowest in sample 4 (56.38 g/I2/100g). Peroxide value was found to range from 2.18 meq O2/kg to 2.67 meq O2/kg, while saponin value was highest in sample 6 (130.3 mg KOH/g) and lowest in sample 8 (122.4 mg KOH/g). All the oil samples were found to contain cholesterol which ranged from 1.21±0.04 mg/dl (sample 1) to 4.58±0.01 mg/dl (sample 4), while the vitamin A content ranged from 674.80±10.26 IU/g (sample 2) to 877.97±20.52 IU/g (sample 8). Findings from this research showed that the researched oils meet the acceptable physicochemical standard. However, the cholesterol levels were against the inscriptions of cholesterol free on the labels.

Oxidative Deterioration of Canned Lake Whitefish (Coregonus clupeaformis) Treated with Antioxidants

1975 ◽  
Vol 32 (2) ◽  
pp. 227-232 ◽  
Author(s):  
C. A. Biggar ◽  
N. A. M. Eskin ◽  
M. Vaisey ◽  
B. Johnston
Keyword(s):  
Control Sample ◽  
Storage Period ◽  
Thiobarbituric Acid ◽  
Butylated Hydroxytoluene ◽  
Butylated Hydroxyanisole ◽  
Coregonus Clupeaformis ◽  
Lake Whitefish ◽  
Oxidative Deterioration ◽  
Significant Difference

Lake whitefish (Coregonus clupeaformis) was canned with one of two antioxidant mixtures, AX1 (20% butylated hydroxyanisole, 20% butylated hydroxytoluene) or AX2 (10% butylated hydroxyanisole, 10% butylated hydroxytoluene, 6% citric acid, and 6% propyl gallate), and compared to untreated control samples. The flavor and quality of the fish were examined at intervals during 4 days of open refrigerated storage using sensory, chemical, and physical methods. Both thiobarbituric acid (TBA) values and the results of paired flavor comparisons by an eight-member trained sensory panel demonstrated that the greatest degree of oxidative deterioration was always associated with the untreated fish, while AX1-treated fish exhibited the least amount of "off-flavor" over the storage period. The relative degree of "off-flavor" as evaluated by the panelists tended to increase on storage; TBA values showed a linear relationship with time. Tristimulus readings using the Hunter Colorimeter showed a significant difference between the control sample and the two antioxidant-treated samples with respect to the pink color of freshly opened canned whitefish.

scholarly journals Rapid and Sensitive Determination of Lipid Oxidation Using the Reagent Kit Based on Spectrophotometry (FOODLABfatSystem)

2016 ◽  
Vol 2016 ◽  
pp. 1-6 ◽  
Author(s):  
Chang Woo Kwon ◽  
Kyung-Min Park ◽  
Jeong Woong Park ◽  
JaeHwan Lee ◽  
Seung Jun Choi ◽  
...  
Keyword(s):  
Lipid Oxidation ◽  
Human Error ◽  
Time Course ◽  
Edible Oils ◽  
Regression Line ◽  
Acid Value ◽  
Standard Mixture ◽  
Promising Alternative ◽  
Significant Difference ◽  
Time Course Study

The reliability and availability of FOODLABfatsystem for determining acid value (AV) and peroxide value (POV) were assessed during the hydrolytic rancidification and lipid oxidation of edible oils. This reagent kit based on spectrophotometry was compared to the official methods (ISO 660 and 3960 protocols) based on manual titration employing the standard mixture for the simulated oxidation models and edible oils during the thermally induced oxidation at 180°C. The linear regression line of standard mixture and the significant difference of thermally oxidized time course study determined between them showed high correlations (R2=0.998andp<0.05) in both AVs and POVs. Considering ISO protocols with a probability of human error in manual titration, the rapidness and simplicity of the reagent kit based on spectrophotometry make it a promising alternative to monitor the lipid oxidation of edible oils and lipid-containing foods.

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