Formation of nanoscale sodium dodecahydro-closo- dodecaborate Na2[B12H12] on silicate matrix surface
Keyword(s):
X Ray
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The method of nanoscaled sodium dodecahydro-closo-dodecaborate Na2[B12H12] synthesis is presented. The composite is heated to 200°C to yield the desired product, forming with the introduction of triethyl- ammonium salt [Et3NH]2[B12H12] into the silicate matrix of a sodium liquid glass. The morphology and phase composition of the synthesized sample are studied through SEM and X-ray diffraction methods, in comparison to those of a standard salt sample Na2[B12H12]. Based on the obtained data, the sample under study is an amorphous composite, on the surface of which nanoscale crystals of Na2[B12H12] form.
2020 ◽
Vol 86
(6)
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pp. 29-35
2017 ◽
Vol 12
(1)
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pp. 63-77
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Spark Plasma Sintering of Paper-Derived Ti3AlC2-Based Composites: Influence of Sintering Temperature
2021 ◽
Vol 1016
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pp. 1790-1796
Keyword(s):
X Ray
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2012 ◽
Vol 465
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pp. 76-79
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2009 ◽
Vol 289-292
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pp. 541-550
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