scholarly journals In-Situ Analysis Of Incipient Melting And Characterization Of A Novel Al-Cu Alloy for Cylinder Head Applications

2021 ◽  
Author(s):  
Bernoulli Andilab

Incipient melting of secondary phases during solution heat treatment of Al alloys is detrimental to their mechanical properties. In this research, incipient melting was analyzed in-situ using a high temperature Laser Scanning Confocal Microscope (LSCM) in a novel Al-Cu alloy. Thermal analysis and microstructural analysis were carried out on the alloy cast at fast and slow cooling rates to examine the resulting solidification and microstructural characteristics. The results showed that incipient melting was accompanied by a clustering liquid droplets followed by a complete melting of Al2Cu which occurred at approximately 548 ℃. Additionally, the use of LSCM enabled an understanding of the underlying mechanisms behind incipient melting. It was also found that incipient melting led to microstructure that consisted of a higher presence of ultra-fine eutectic clusters, needle-like Al2Cu and porosity along the grain boundaries. Lastly, the solution heat treatment temperature was optimized for the Al-Cu alloy using the data from LSCM, Differential Scanning Calorimetry and solution heat treatment experiments.

2021 ◽  
Author(s):  
Bernoulli Andilab

Incipient melting of secondary phases during solution heat treatment of Al alloys is detrimental to their mechanical properties. In this research, incipient melting was analyzed in-situ using a high temperature Laser Scanning Confocal Microscope (LSCM) in a novel Al-Cu alloy. Thermal analysis and microstructural analysis were carried out on the alloy cast at fast and slow cooling rates to examine the resulting solidification and microstructural characteristics. The results showed that incipient melting was accompanied by a clustering liquid droplets followed by a complete melting of Al2Cu which occurred at approximately 548 ℃. Additionally, the use of LSCM enabled an understanding of the underlying mechanisms behind incipient melting. It was also found that incipient melting led to microstructure that consisted of a higher presence of ultra-fine eutectic clusters, needle-like Al2Cu and porosity along the grain boundaries. Lastly, the solution heat treatment temperature was optimized for the Al-Cu alloy using the data from LSCM, Differential Scanning Calorimetry and solution heat treatment experiments.


2015 ◽  
Vol 828-829 ◽  
pp. 226-231 ◽  
Author(s):  
Pfarelo Daswa ◽  
Heinrich Möller ◽  
Gonasagren Govender

This paper investigates the optimization of the solution heat treatment parameters of the rheo-high pressure die cast (R-HPDC) 2139 aluminium alloy. Differential Scanning Calorimetry (DSC) and optical microscopy were used to investigate the incidence of incipient melting and therefore determine suitable solution heat treatment temperatures. A three-step solution heat treatment where the alloy was heat treated from 400°C to 513°C using controlled heating conditions and held at 513°C for 2 hours and finally heated up from 513°C to 525°C and held there for 16 hours was done. R-HPDC is known to produce surface liquid segregation and when processing the alloys these areas are most prone to incipient melting. The applicability of a single (525°C for 16h) and three-step solution heat treatments on the R-HPDC 2139 aluminium alloy was also investigated. A single-step solution heat treatment results in incipient melting, whereas this is mostly eliminated using the three-step solution heat treatment. However, a high volume fraction of undissolved phases remain in the liquid segregated areas, even after the three-step solution heat treatment.


2014 ◽  
Vol 217-218 ◽  
pp. 259-264 ◽  
Author(s):  
Pfarelo Daswa ◽  
Heinrich Möller ◽  
Madeleine du Toit ◽  
Gonasagren Govender

The 6xxx series alloys are well known for desirable combinations of high strength, weldability, corrosion resistance and formability. This paper investigates the influence of chemical composition on the solution heat treatment parameters of rheo-high pressure die cast (R-HPDC) 6xxx series aluminium alloys. The presence of copper in the 6xxx series aluminium alloys affects the solution heat treatment by promoting incipient melting. The incidence of incipient melting is investigated for the R-HPDC alloys using Differential Scanning Calorimetry (DSC) and optical microscopy. R-HPDC is known to produce surface liquid segregation and centre-line liquid segregation when processing the alloys and these areas are the most susceptible to incipient melting. The applicability of single and multiple step solution heat treatments are investigated. The alloys used for this study include the Cu-free alloy 6082, as well as the Cu-containing alloys 6013 and 6111.


2013 ◽  
Vol 212 ◽  
pp. 15-20
Author(s):  
Kazimierz J. Ducki ◽  
Jacek Mendala ◽  
Lilianna Wojtynek

The influence of prolonged ageing on the precipitation process of the secondary phases in an Fe-Ni superalloy of A-286 type has been studied. The samples were subjected to a solution heat treatment at 980°C for 2 h and water quenched, and then aged at temperatures of 715, 750 and 780°C at holding times from 0.5 to 500 h. Structural investigations were conducted using TEM and X-ray diffraction methods. The X-ray phase analyses performed on the isolates were obtained by anodic dissolution of the solid samples. After solution heat treatment the alloy has the structure of twinned austenite with a small amount of undissolved precipitates, such as carbide TiC, carbonitride TiC0.3N0.7, nitride TiN0.3, carbosulfide Ti4C2S2, Laves phase Ni2Si, and boride MoB. The application of ageing causes precipitation processes of γ-Ni3(Al,Ti), G (Ni16Ti6Si7), η (Ni3Ti), β (NiTi) and σ (Cr0.46Mo0.40Si0.14) intermetallic phases, as well as the carbide M23C6. It was found that the main phase precipitating during alloy ageing was the γ intermetallic phase.


2013 ◽  
Vol 765 ◽  
pp. 496-500 ◽  
Author(s):  
Dawid Kapinos ◽  
Marcin Szymanek ◽  
Bogusław Augustyn ◽  
Maciej Gawlik

The article presents the change in mechanical properties of AlZn9Mg2.5Cu1.8 alloy resulting from the process of solution heat treatment and aging. The heat treatment was performed on a unique UMSA (Universal Metallurgical Simulator and Analyzer) device. The aim of the study was to determine optimum heat treatment parameters for the tested alloy of ultrafine grain structure obtained by Rapid Solidification (RS). To achieve this purpose, heat treatment to the T4 and T6 condition was carried out. The solution heat treatment was carried out at a constant temperature of 460 °C for 2 hours, while the time - temperature parameters of the aging process varied. The treatment undertaken resulted in improved mechanical properties.


2021 ◽  
Author(s):  
Anthony Lombardi

Lightweighting has become an important factor in the automotive industry due to stringent government regulations on fuel consumption and increased environmental awareness. Aluminum alloys are 65% lighter than cast iron enabling significant weight reduction. However, there are several significant challenges associated to the use of hypoeutectic Al-Si alloys in engine block applications. This dissertation investigated the factors influencing the susceptibility of in-service cylinder distortion as it is deleterious to engine operating efficiency, leading to environmental (increased carbon emissions) and economic (expensive recalls) repercussions. The initial segment of this dissertation sought to quantitatively confirm the cause of cylinder distortion by investigating distorted and undistorted service tested engine blocks. This analysis involved measurement of macro-distortion using a co-ordinate measuring machine, in-depth microstructural analysis, measurement of tensile properties, and residual stress mapping along the length of the cylinder bores (neutron diffraction). Upon determining the cause of distortion, the second phase of this project optimized the solution heat treatment parameters to mitigate future distortion in the engine blocks. This optimization was carried out by varying heat treatment parameters to maximize engine block strength. In addition, a pioneering application of in-situ neutron diffraction, along with a unique engine heating system, was used to develop a time-dependent correlation of residual stress relief during heat treatment, assisting in process optimization. The results indicate that the distorted engine block had high tensile residual stress, specifically at cylinder depths greater than 30 mm, while the undistorted block had mainly compressive stress. The maximum distortion occurred near the center portion of the cylinder (~60 mm), which had a combination of coarse microstructure (lower strength) and high tensile residual stress. As such,distortion can be prevented via maximization of strength and reduction in tensile residual stress. Lab scale castings and in-situ neutron diffraction were used to successfully develop an optimal heat treatment process to increase engine block integrity. These experiments found that solution heat treatment at 500 °C for 2 h increased tensile yield strength by 15-20% over engines produced using the current process. Furthermore, tensile residual stress was completely relieved by this heat treatment, reducing the susceptibility to in-service distortion. Solutionizing at temperatures above 500 °C was deemed unsuitable for engine block production due to incipient melting, which deteriorates strength.


Sign in / Sign up

Export Citation Format

Share Document