scholarly journals Effect of Co Leaching on the Vertical Turning Lathe Wear Properties of Polycrystalline Diamond Compact Manufactured by High Temperature and High Pressure Sintering Process

2020 ◽  
Vol 58 (7) ◽  
pp. 480-487
Author(s):  
Min-Seok Baek ◽  
Ji-Won Kim ◽  
Bae-Gun Park ◽  
Hee-Sub Park ◽  
Kee-Ahn Lee

Polycrystalline diamond compact (PDC) has excellent wear resistance, high impact resistance, superior fatigue properties, and has been used in the oil and gas drilling industries. This study investigated the effect of Co leaching on the microstructure, vertical turning lathe (VTL) wear properties of PDCs manufactured by high-temperature and high-pressure (HTHP) sintering. The VTL wear test has the advantage of simulating the actual oil drilling environment by using granite as the workpiece. PDC sintered material that did not receive Co leaching was named HTHP sintered PDC-A, and the material subjected to Co leaching was called Co-leached PDC-B in this study. As a result of XRD analysis of both PDCs, diamond and WC peaks were detected, and only the HTHP sintered PDC-A exhibited some Co peaks. In the HTHP sintered PDC-A, the binder WC and Co were evenly distributed at the diamond interface. However, in the Co-leached PDC-B, some empty spaces were observed at the diamond interface. The HTHP sintered PDCA exhibited a similar or slightly higher VTL wear resistance than the Co-leached PDC-B, but only in the short sliding distance. In the long sliding distance after 9 km, Co-leached PDC-B showed significantly superior wear resistance compared to the HTHP sintered PDC-A. The HTHP sintered PDC-A exhibited both abrasive and adhesive wear behaviors, while the Co-leached PDC-B showed only abrasive wear. Based on the above results, the VTL wear mechanism of PDCs, and ways of improving wear resistance were also discussed.

2020 ◽  
Vol 10 (1) ◽  
Author(s):  
Qiang Li ◽  
Guodong Zhan ◽  
Dong Li ◽  
Duanwei He ◽  
Timothy Eric Moellendick ◽  
...  

AbstractDiamond is the hardest naturally occurring material found on earth but single crystal diamond is brittle due to the nature of catastrophic cleavage fracture. Polycrystalline diamond compact (PDC) materials are made by high pressure and high temperature (HPHT) technology. PDC materials have been widely used in several industries. Wear resistance is a key material property that has long been pursued for its valuable industrial applications. However, the inevitable use of catalysts introduced by the conventional manufacturing process significantly reduces their end-use performance and limits many of their potential applications. In this work, an ultra-strong catalyst-free polycrystalline diamond compact material has been successfully synthesized through innovative ultra-high pressure and ultra-high temperature (UHPHT) technology. These results set up new industry records for wear resistance and thermal stability for PDC cutters utilized for drilling in the oil and gas industry. The new material also broke all single-crystal diamond indenters, suggesting that the new material is too hard to be measured by the current standard single-crystal diamond indentation method. This represents a major breakthrough in hard materials that can expand many potential scientific research and industrial applications.


Author(s):  
Deepak Mehra ◽  
M.M. Mahapatra ◽  
S. P. Harsha

The purpose of this article is to enhance the mechanical properties and wear resistance of the RZ5 alloy used in the aerospace application by adding TiC particles. The present study discusses processing of in-situ RZ5-TiC composite fabricated by self-propagating high temperature (S.H.S.) method and its wear behavior. The effects of TiC particle on mechanical and microstructural properties of the composite are studied. The wear test is performed by varying the sliding distance and applied load. The composite is characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDS). The results exhibited the properties like strength and hardness of RZ5-10wt%TiC composite has been increased considerably, while grain size is decreased as compared to the RZ5 alloy. The fractography indicated mixed mode (quasi-cleavage and ductile feature) failure of the composites. The wear results showed improvement in wear resistance of the composite. The FESEM showed dominate wear mechanisms are abrasion, ploughing grooves.


Author(s):  
E. F. Koch

Because of the extremely rigid lattice structure of diamond, generating new dislocations or moving existing dislocations in diamond by applying mechanical stress at ambient temperature is very difficult. Analysis of portions of diamonds deformed under bending stress at elevated temperature has shown that diamond deforms plastically under suitable conditions and that its primary slip systems are on the ﹛111﹜ planes. Plastic deformation in diamond is more commonly observed during the high temperature - high pressure sintering process used to make diamond compacts. The pressure and temperature conditions in the sintering presses are sufficiently high that many diamond grains in the sintered compact show deformed microtructures.In this report commercially available polycrystalline diamond discs for rock cutting applications were analyzed to study the deformation substructures in the diamond grains using transmission electron microscopy. An individual diamond particle can be plastically deformed in a high pressure apparatus at high temperature, but it is nearly impossible to prepare such a particle for TEM observation, since any medium in which the diamond is mounted wears away faster than the diamond during ion milling and the diamond is lost.


2019 ◽  
Vol 285 ◽  
pp. 63-68 ◽  
Author(s):  
Mnel A. Abdelgnei ◽  
M. Zaidi Omar ◽  
Mariyam Jameelah Ghazali

Earlier work has shown that Al-5.7Si-2Cu-0.3Mg aluminium alloy is suitable for thixoforming process. Here, the dry sliding wear behaviour of the alloy, in the as-cast and thixoformed conditions were investigated. The cooling slope technique was used to produce the alloy with globular microstructure for the thixoforming process. Both the thixoformed and cast samples were subjected to T6 heat treatments prior to the wear tests. The tests were carried out using a pin-on-disc tribometer, against a hardened M2 tool steel disc of 62 HRC at different loads, under dry sliding conditions at fixed sliding speed and sliding distance of 1 m.s–1 and 5 km respectively. The microstructural response, worn surfaces were thoroughly and carefully examined using various methods such as scanning electron microscopy, energy dispersive spectroscopy, and differential scanning calorimetry. The density of the heat treated thixoformed alloys showed significant increase in the hardness property, among others, due to its reduced porosity. Their wear test results also observed that the weight loss of materials increase with an increase in the input load and the sliding distance for all samples. However, the as-cast alloy displayed higher wear rate compared with the thixoformed alloys. In general, the wear mechanisms showed a mixture of abrasive, oxidative and delamination wear (mild wear) at low applied loads and mainly an adhesive (severe wear) at high applied loads.


1985 ◽  
Vol 107 (4) ◽  
pp. 534-542 ◽  
Author(s):  
C. L. Hough ◽  
B. Das

The wear characteristics of polycrystalline diamond compact (PDC) drill bits were investigated in the context of drilling small holes in a hard abrasive medium. An efficient method for measuring wear of the PDC drill bits was developed. The wear test results were grouped or categorized in terms of rotary speed, feed and wear or failure characteristics. Contrary to the three classical wear phases (break-in, uniform wear and rapid breakdown) of the single material cutters, four distinctive wear phases were formed for the PDC cutters: I–break-in, II–diamond wear, III–carbide wear, and IV–rapid breakdown. The characteristics of the wear phases were identified and some suggestions were made to alleviate the wear problem.


Materials ◽  
2020 ◽  
Vol 13 (24) ◽  
pp. 5757
Author(s):  
Mateusz Kukliński ◽  
Aneta Bartkowska ◽  
Damian Przestacki ◽  
Grzegorz Kinal

In this study, wear properties of Monel 400 after laser alloying with boron are described. Surfaces were prepared by covering them with boron paste layers of two different thicknesses (100 µm and 200 μm) and re-melting using diode laser. Laser beam power density was equal to 178.3 kW/cm2. Two laser beam scanning velocities were chosen for the process: 5 m/min and 50 m/min. Surfaces alloyed with boron were investigated in terms of wear resistance, and the surface of untreated Monel 400 was examined for comparison. Wear tests were performed using counterspecimen made from steel 100Cr6 and water as a lubricant. Both quantitative and qualitative analysis of surfaces after wear test are described in this paper. Additionally, microstructures and properties of obtained laser alloyed surfaces are presented. It was found that the wear resistance increased from four to tens of times, depending on parameters of the laser boriding process. The wear mechanism was mainly adhesive for surfaces alloyed with initial boron layer 100 µm thick and evolves to abrasive with increasing boron content and laser beam scanning velocity. Iron particles detached from counterspecimens were detected on each borided surface after the wear test, and it was found that the harder the surface the less built-ups are present. Moreover, adhered iron particles oxidized during the wear test.


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