scholarly journals Bond Strength and Failure Pattern of Orthodontic Tubes Adhered to a Zirconia Surface Submitted to Different Modes of Application of a Ceramic Primer

Materials ◽  
2019 ◽  
Vol 12 (23) ◽  
pp. 3922
Author(s):  
Francisco da Silva Araújo Milagres ◽  
Dauro Douglas Oliveira ◽  
Giordani Santos Silveira ◽  
Emanuelle de Fátima Ferreira Oliveira ◽  
Alberto Nogueira da Gama Antunes

The aim of this study was to evaluate the shear bond strength of orthodontic tubes adhered to ceramics with the Transbond™ XT bonding resin (3M, Maplewood, MN, USA) while varying the surface treatment. Then, the adhesive remaining index (ARI) was verified, and the representative fracture patterns were evaluated via scanning electron microscopy. Forty-eight zirconia blocks were divided into three groups, varying the number of layers of the 10-methacryloyloxy-decyl dihydrogen phosphate (MDP) primer: one, two, or three applications. In addition, 16 lithium disilicate IPS E.max ceramic disks (Ivoclar Vivadent, Schaan, Liechtenstein) were conditioned with 10% hydrofluoric acid for 20 s and underwent a single-layer primer application regimen. The four groups were further stratified to undergo bond testing after either 24 h (control) or 5000 cycles in a thermocycling machine. A shear bond strength test was performed (0.5 mm/min), and the MPa values obtained were submitted to a two-way analysis of variance and Tukey’s test. There was no statistical difference among the control group ceramics that received the varying surface treatments. After thermocycling, it was verified that both the E.max disks and the zirconia ceramics with three primer applications obtained the highest bond strength values. In the 24 h groups, a total displacement of the resin from the orthodontic tubes was observed (ARI of 1). After thermocycling, the highest prevalence of an ARI of 5 (adhesive failure) was observed among the zirconia ceramics with single-coat primer application, followed by those with triple-coat primer application (mixed failure). Three applications of the MDP-containing ceramic primer achieved the best result in the present study. Zirconia surface should be treated with three coats of MDP primer to achieve a level of bond strength similar to silica-rich phase ceramic.

2012 ◽  
Vol 512-515 ◽  
pp. 447-450
Author(s):  
Qi Liu ◽  
Long Quan Shao ◽  
Chen Hu ◽  
Yuan Fu Yi ◽  
Bin Deng ◽  
...  

To investigate the bond strength of different adhesive luting materials bond to zirconia ceramics. 40 (30mm×5mm×5mm) Cercon Smart Ceramics samples were divided into groups: (1) glass-ionomer bonded (control group), (2) Clearfil™ Repair bonded, (3) Panavia F bonded, (4) Variolink N bonded. Tensile bond strength and shear bond strength were evaluated after 24h storage at 37°C in distilled water. Each group had 10 samples for different test. Data were evaluated using ANOVA analysis (α=0.05). The experiment groups are statistically significant differences with control group (P<0.05). The shear bond strength of the Glass ionomer FX Ι, the Clearfil™ Repair, Panavia F and Variolink N groups were 14.23±4.48 MPa, 21.95±1.32 MPa, 31.16±1.50 MPa and 43.54±1.97 MPa, separately. Comparisons among groups were significant differences (P<0.001). Variolink N bonded ceramics achieved highest tensile and shear bond strength. Different adhesive materials significantly influence the bond strength of zirconia ceramics.


Materials ◽  
2020 ◽  
Vol 13 (1) ◽  
pp. 235 ◽  
Author(s):  
Francesco Valente ◽  
Luan Mavriqi ◽  
Tonino Traini

To date, numerous materials in the dental field are marketed to ensure stable adhesive cementation of zirconia ceramics (Y-TZP). The aims of this study were to assess the shear bond strength of the new experimental cement Surgi Dual Flo’ Zr to Y-TZP compared to Panavia V5 cement, and to evaluate the effect of 10-MDP (10-methacryloyloxydecyl dihydrogen phosphate) containing primer on their bond strength. Twenty composite cylinders and Y-TZP disks were adhesively luted and divided into four groups based on cement type used and application or not of 10-MDP. The groups (n = 5 each) were S 10MDP (Surgi Dual Flo’ Zr with 10-MDP); S no 10MDP (Surgi Dual Flo’ Zr without 10-MDP); P 10MDP (Panavia V5 with 10-MDP); P no 10MDP (Panavia V5 without 10-MDP). Maximum load resistance (ML) and shear bond strength (SBS) were tested and mode of failure qualitative documented via scanning electron microscopy. The data were analyzed with one-way ANOVA, Holm-Sidak method, and Bayesian analysis. ML and SBS were significantly higher in S 10MDP than in S no 10MDP; and in P 10MDP than in P no 10MDP (p < 0.05). No significant differences were found between S 10MDP and P 10MDP; S no 10MDP and P no 10MDP (p > 0.05). Cohesive, adhesive, and mixed failure occurred among the groups. Bond strength between the experimental resin-based cement and Y-TZP was adequate for clinical application when 10-MDP was added. 10-MDP containing primer was effective improving the bond strength to Y-TZP more than the different type of resinous cement.


2020 ◽  
Vol 62 (1) ◽  
pp. 84-88
Author(s):  
Xiuju Liu ◽  
Xue Jiang ◽  
Tong Xu ◽  
Qi Zhao ◽  
Song Zhu

2020 ◽  
pp. 1-11
Author(s):  
Anip K. Roy ◽  
Govind N. Prasad ◽  
Tushar V. Bhagat ◽  
Saurabh Chaturvedi ◽  
Vishwanath Gurumurthy ◽  
...  

BACKGROUND: The increased strength of zirconia has resulted in its widespread application in clinical dentistry. Nevertheless, the fracture of veneering porcelains remains one of the key reasons of failure. OBJECTIVE: The objective of this study was to compare and analyze the influence of surface conditioning methods on the core-veneer bond strength of zirconia restorations. METHODS: Thirty specimens of zirconia core with sizes 10 × 5 × 5 mm were layered with porcelain of sizes 5 × 3 × 3 mm. On the basis of different surface conditioning methods, four groups were made: Group I: abrasion with airborne alumina particles of 110 μm size, Group II: sandblasting with silica coated alumina particles of 50 μm in size, Group III (modified group): alteration with a coating of zirconia powder prior to sintering, and Group IV (control group): metal core specimens. The shear force of all specimens was tested using a universal testing machine with a 0.5 mm/min crosshead speed. One-way analysis of variance (ANOVA) and Tukey’s post hoc pair wise comparison (p= 0.05) were performed to analyze the shear bond strength. A scanning electron microscope was used to assess the fractured specimens. RESULTS: A statistically significant difference was noted between the groups. The mean value of shear bond strength was 40.25 MPa for Group I, 41.93 MPa for Group II, 48.08 MPa for Group III and 47.01 MPa for Group IV. CONCLUSIONS: The modified zirconia group and control group demonstrated a significantly higher mean bond strength than that of Group I, where airborne particle abrasion was used. The scanning electron microscope showed that cohesive fracture in the porcelain veneers was the main problem of failure in altered zirconia. The modified zirconia specimens in Group III demonstrated significantly improved values of shear bond strength.


2014 ◽  
Vol 2014 ◽  
pp. 1-7 ◽  
Author(s):  
Ahmed Mohammed Hassan ◽  
Ahmed Ali Goda ◽  
Kusai Baroudi

Objective. The aim of this study was to evaluate the effect of different disinfectant agents on bond strength of two types of resin composite materials.Methods. A total of 80 sound posterior teeth were used. They were divided into four groups(n=20)according to the dentin surface pretreatment (no treatment, chlorhexidine gluconate 2%, sodium hypochlorite 4%, and EDTA 19%). Each group was divided into two subgroups according to the type of adhesive (prime and bond 2.1 and Adper easy one). Each subgroup was further divided into two subgroups according to the type of resin composite (TPH spectrum and Tetric EvoCeram). Shear bond strength between dentin and resin composite was measured using Universal Testing Machine. Data collected were statistically analyzed byt-test and one-way ANOVA followed by Tukey’spost hoctest.Results. It was found that dentin treated with EDTA recorded the highest shear bond strength values followed by sodium hypochlorite and then chlorhexidine groups while the control group showed the lowest shear bond strength.Conclusions. The surface treatment of dentin before bonding application has a great effect on shear bond strength between resin composite and dentin surface.


2013 ◽  
Vol 18 (3) ◽  
pp. 101-106 ◽  
Author(s):  
Sissy Maria Mendes Machado ◽  
Diego Bruno Pinho do Nascimento ◽  
Robson Costa Silva ◽  
Sandro Cordeiro Loretto ◽  
David Normando

OBJECTIVE: To evaluate in vitro the effects of tooth whitening using gel with Amorphous Calcium Phosphate (ACP) on the bond strength of metal brackets. METHODS: Thirty-six bovine incisors were sectioned at the crown-root interface, and the crowns were then placed in PVC cylinders. The specimens were divided into 3 groups (n = 12) according to whitening treatment and type of gel used, as follows: G1 (control) = no whitening; G2 = whitening with gel not containing ACP (Whiteness Perfect - FGM), G3 = whitening with gel containing ACP (Nite White ACP - Discus Dental). Groups G2 and G3 were subjected to 14 cycles of whitening followed by an interval of 15 days before the bonding of metal brackets. Shear bond strength testing was performed on a Kratos universal test machine at a speed of 0.5 mm/min. After the mechanical test, the specimens were assessed to determine the adhesive remnant index (ARI). The results were subjected to ANOVA, Tukey's test and Kruskal-Wallis test (5%). RESULTS: Significant differences were noted between the groups. Control group (G1 = 11.10 MPa) showed a statistically higher shear bond strength than the groups that underwent whitening (G2 = 5.40 Mpa, G3 = 3.73 MPa), which did not differ from each other. There were no significant differences between the groups in terms of ARI. CONCLUSION: Tooth whitening reduces the bond strength of metal brackets, whereas the presence of ACP in the whitening gel has no bearing on the results.


2004 ◽  
Vol 12 (3) ◽  
pp. 200-204 ◽  
Author(s):  
Gisele Maria Correr ◽  
Angela S. Caldo-Teixeira ◽  
Roberta Caroline Bruschi Alonso ◽  
Regina Maria Puppin-Rontani ◽  
Mário Alexandre Coelho Sinhoreti ◽  
...  

The aim of this study was to evaluate the effect of saliva contamination (SCT) and re-etching time (RET) on the shear bond strength (SBS) of the Fluroshield sealant. Forty-five extracted third molars were sectioned and flattened until reach an enamel surface area. Then, all samples were etched for 30 sec with 35% phosphoric acid and then they were distributed into 9 groups (n=10) according to SCT and RET (seconds), respectively: G1- control (no SCT and no RET); G2- 30s and 0s; G3- 60s and 0s; G4-30s and 2s; G5- 30s and 5s; G6- 30s and 15s; G7-60s and 2s; G8- 60s and 5s; G9- 60s and 15s. The sealant was applied according to the manufacturer's instructions. The samples were stored in distilled water at 37ºC for 72h and subjected to the SBS test. The results indicated that there was no statistically significant difference between the groups (p>0.05). However, it could be noticed that: 1- the longer the SCT, the lower the SBS values; 2 - the longer the RET, the higher the SBS values. It could be concluded that there was a tendency to the shortest SCT (30s) associated to the longest RET (5 and 15s) to reach similar SBS values for the control group.


2014 ◽  
Vol 15 (6) ◽  
pp. 688-692 ◽  
Author(s):  
Sukumaran Anil ◽  
Farouk Ahmed Hussein ◽  
Mohammed Ibrahim Hashem ◽  
Elna P Chalisserry

ABSTRACT Objective The purpose of the current in-vivo study was to assess the effect of using 0.12% chlorhexidine (CHX) mouth rinse, before bonding, on shear bond strength of polycarbonate brackets bonded with composite adhesive. Subjects and methods Eighteen orthodontic patients with a mean age 21.41 ± 1.2 years, who were scheduled to have 2 or more first premolars extracted, were included in this study. Patients were referred for an oral prophylaxis program which included, in part, the use of a mouth rinse. Patients were divided into 2 groups, a test group of 9 patients who used 0.12% CHX gluconate mouth rinse twice daily and a control group of 9 patients who used a mouth rinse without CHX, but with same color. After 1 week, polycarbonate brackets were bonded to first premolars with Transbond XT composite adhesive. Premolars were extracted after 28 days and tested for shear bond strength on a universal testing machine. Student's t-test was used to compare shear bond strengths of both groups. Results No statistically significant difference was found in bond strengths’ values between both groups. The test group (with CHX) has mean shear bond strength of 14.21 ± 2.42 MPa whereas the control group (without CHX) revealed a mean strength of 14.52 ± 2.31 MPa. Conclusion The use of 0.12% CHX mouth rinse, for one week before bonding, did not affect the shear bond strength of polycarbonate brackets bonded with Transbond composite. Furthermore, these brackets showed clinically acceptable bond strength. How to cite this article Hussein FA, Hashem MI, Chalisserry EP, Anil S. The Impact of Chlorhexidine Mouth Rinse on the Bond Strength of Polycarbonate Orthodontic Brackets. J Contemp Dent Pract 2014;15(6):688-692.


Author(s):  
Hoseinali Mahgoli ◽  
Mahnaz Arshad ◽  
Kamran Rasouli ◽  
Ali Akbar Sobati ◽  
Ahmad Reza Shamshiri

  Objectives: This study aimed to assess the effect of application of two types of zirconia primers on repair bond strength of composite to zirconia ceramic. Materials and Methods: In this in vitro, experimental study, 60 zirconia blocks were divided into five groups and subjected to the application of Z-Prime Plus (ZPP), Monobond Plus (MBP), Porcelain Bonding Resin (PBR), ZPP followed by PBR (ZPP+PBR) and MBP followed by PBR (MBP+PBR). They were then bonded to Z100 composite. The samples were then immersed in water at 37°C for 24 hours, thermocycled for 1000 cycles between 5-55°C and subjected to shear bond strength (SBS) test. The mode of failure was determined under a stereomicroscope and a scanning electron microscope (SEM). Results: The mean bond strength was the highest in ZPP+PBR group followed by MBP+PBR, ZPP, PBR and MBP group (22.29±8.86, 15.75±2.81, 12.02±3.24, 3.60±2.92 and 2.92±1.78 MPa, respectively). The effects of type of zirconia primer and use/no use of PBR on SBS were significant (P<0.05). The frequency of adhesive failure in MBP and PBR groups was significantly higher than that in MBP+PBR and ZPP+PBR groups (P<0.05). The cohesive failure was significantly more frequent in ZPP+PBR group than in ZPP, MBP and PBR groups (P<0.05). Conclusion: Simultaneous application of zirconia primer and PBR is the most efficient technique for repair of all-ceramic zirconia restorations with composite resin.


2011 ◽  
Vol 82 (1) ◽  
pp. 30-35
Author(s):  
Shinya Horiuchi ◽  
Shingo Kuroda ◽  
Masahiro Hiasa ◽  
Toshiyuki Suge ◽  
Seitaro Saku ◽  
...  

Abstract Objective: To determine the reinforcement of bond strength of a self-etching system by applying a pretreatment agent. Materials and Methods: Sixty extracted human premolars were used in this study. The enamel surfaces were treated with four pretreatment agents—phosphoric acid, polyacrylic acid, citric acid, and ammonium hexafluorosilicate (SiF)—and were examined under a scanning electron microscope. Afterward, orthodontic brackets were bonded with a self-etching adhesive system (n  =  10 for each agent), and shear bond strength was measured through a debonding process. The adhesive remnant index (ARI) was also assessed. Results: Enamel surfaces treated with polyacrylic acid seemed almost the same as intact enamel. Treatment with SiF induced slight shallow depressions compared with the intact enamel. On the other hand, enamel surfaces treated with citric acid and phosphoric acid showed severe etching patterns. All pretreatments increased the bond strength, but SiF-treated specimens revealed the greatest strength (12.201 ± 1.048 MPa), followed by polyacrylic acid (12.030 ± 2.103 MPa). The control group with no pretreatment showed the least strength (9.078 ± 1.678 MPa). All pretreatments increased ARI score compared with the control group. Conclusions: Surface conditioning before bracket adhesion could reinforce the bond strength of the self-etching adhesive system, resulting in a more reliable bonding system.


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