scholarly journals Biofunctionalization of Porous Ti Substrates Coated with Ag Nanoparticles for Potential Antibacterial Behavior

Metals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 692
Author(s):  
Juliana Gaviria ◽  
Ana Alcudia ◽  
Belén Begines ◽  
Ana María Beltrán ◽  
José Antonio Rodríguez-Ortiz ◽  
...  
Keyword(s):  
Mechanical Performance ◽  
Stress Shielding ◽  
Basic Medium ◽  
Mechanical Resistance ◽  
Porous Ti ◽  
Biological Compatibility ◽  
Microbial Infections ◽  
In Situ Methods ◽  
Acidic Reagent

Ti prosthesis have shown better biological compatibility, mechanical performance, and resistance to corrosion in cases of bone replacements. Nevertheless, fully dense Ti in connection with bone-host tissues show stress-shielding phenomenon that, together with the development of frequent undesirable microbial infections, may lead to implant failures. To overcome these issues, the present study aimed at the development of a novel combination of a chemically functionalized porous Ti substrate with a potentially therapeutic AgNPs coating. Fully dense and porous Ti substrates (30 and 60 vol.%, 100–200 and 355–500 μm, as spacer particles) were studied. Ti surface was treated with acid or basic medium followed by silanization and deposition of AgNPs by “submerged” and “in situ” methods. In general, for similar porosity, mechanical resistance decreased as pore size increased. Acidic reagent and submerged methodology were the best combination for fully dense Ti substrates. Hence, they were also employed for porous Ti substrates. Depending on the porosity of the substrates, variations can be observed both in the size and degree of agglomeration of the deposited AgNPs, entailing differences in the antibacterial behavior of the samples.

LIGHTER-THAN-AIR (LTA) UNMANNED AERIAL SYSTEM (UAS) CARRIER CONCEPT FOR SURVAILLANCE AND DISASTER MANAGEMENT

2019 ◽  
Vol 3 ◽  
pp. 1255
Author(s):  
Ahmad Salahuddin Mohd Harithuddin ◽  
Mohd Fazri Sedan ◽  
Syaril Azrad Md Ali ◽  
Shattri Mansor ◽  
Hamid Reza Jifroudi ◽  
...  
Keyword(s):  
Unmanned Aerial Vehicles ◽  
Disaster Management ◽  
Unmanned Aerial Systems ◽  
Unmanned Aerial System ◽  
Border Control ◽  
Aerial Vehicles ◽  
Operational Safety ◽  
In Situ Methods ◽  
Aerial Systems

Unmanned aerial systems (UAS) has many advantages in the fields of SURVAILLANCE and disaster management compared to space-borne observation, manned missions and in situ methods. The reasons include cost effectiveness, operational safety, and mission efficiency. This has in turn underlined the importance of UAS technology and highlighted a growing need in a more robust and efficient unmanned aerial vehicles to serve specific needs in SURVAILLANCE and disaster management. This paper first gives an overview on the framework for SURVAILLANCE particularly in applications of border control and disaster management and lists several phases of SURVAILLANCE and service descriptions. Based on this overview and SURVAILLANCE phases descriptions, we show the areas and services in which UAS can have significant advantage over traditional methods.

scholarly journals Enhanced Tensile Strength of Monolithic Epoxy with Highly Dispersed TiO2-Graphene Nanocomposites

2021 ◽  
Vol 5 (7) ◽  
pp. 191
Author(s):  
Yanshuai Wang ◽  
Siyao Guo ◽  
Biqin Dong ◽  
Feng Xing
Keyword(s):  
Tensile Strength ◽  
Epoxy Resin ◽  
Mechanical Performance ◽  
Chemical Properties ◽  
High Mechanical Property ◽  
Graphene Nanocomposites ◽  
Highly Dispersed ◽  
Dispersion State ◽  
Physical And Chemical

The functionalization of graphene has been reported widely, showing special physical and chemical properties. However, due to the lack of surface functional groups, the poor dispersibility of graphene in solvents strongly limits its engineering applications. This paper develops a novel green “in-situ titania intercalation” method to prepare a highly dispersed graphene, which is enabled by the generation of the titania precursor between the layer of graphene at room temperature to yield titania-graphene nanocomposites (TiO2-RGO). The precursor of titania will produce amounts of nano titania between the graphene interlayers, which can effectively resist the interfacial van der Waals force of the interlamination in graphene for improved dispersion state. Such highly dispersed TiO2-RGO nanocomposites were used to modify epoxy resin. Surprisingly, significant enhancement of the mechanical performance of epoxy resin was observed when incorporating the titania-graphene nanocomposites, especially the improvements in tensile strength and elongation at break, with 75.54% and 176.61% increases at optimal usage compared to the pure epoxy, respectively. The approach presented herein is easy and economical for industry production, which can be potentially applied to the research of high mechanical property graphene/epoxy composite system.

scholarly journals Design and Characterization of Microscale Auxetic and Anisotropic Structures Fabricated by Multiphoton Lithography

Nanomaterials ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 446
Author(s):  
Ioannis Spanos ◽  
Zacharias Vangelatos ◽  
Costas Grigoropoulos ◽  
Maria Farsari
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Mechanical Performance ◽  
Element Analysis ◽  
Mechanical Responses ◽  
Multiphoton Lithography ◽  
Anisotropic Structures ◽  
Scanning Electron

The need for control of the elastic properties of architected materials has been accentuated due to the advances in modelling and characterization. Among the plethora of unconventional mechanical responses, controlled anisotropy and auxeticity have been promulgated as a new avenue in bioengineering applications. This paper aims to delineate the mechanical performance of characteristic auxetic and anisotropic designs fabricated by multiphoton lithography. Through finite element analysis the distinct responses of representative topologies are conveyed. In addition, nanoindentation experiments observed in-situ through scanning electron microscopy enable the validation of the modeling and the observation of the anisotropic or auxetic phenomena. Our results herald how these categories of architected materials can be investigated at the microscale.

scholarly journals Chemical Modification as a Method of Improving Biocompatibility of Carbon Nonwovens

Materials ◽  
2021 ◽  
Vol 14 (12) ◽  
pp. 3198
Author(s):  
Justyna Frączyk ◽  
Sylwia Magdziarz ◽  
Ewa Stodolak-Zych ◽  
Ewa Dzierzkowska ◽  
Dorota Puchowicz ◽  
...  
Keyword(s):  
Surface Modification ◽  
Cellular Response ◽  
Fiber Surface ◽  
Thermal Conversion ◽  
Cartilage Tissue ◽  
Polar Component ◽  
Nonwoven Fabrics ◽  
Biological Compatibility ◽  
Starting Point

It was shown that carbon nonwoven fabrics obtained from polyacrylonitrile fibers (PAN) by thermal conversion may be modified on the surface in order to improve their biological compatibility and cellular response, which is particularly important in the regeneration of bone or cartilage tissue. Surface functionalization of carbon nonwovens containing C–C double bonds was carried out using in situ generated diazonium salts derived from aromatic amines containing both electron-acceptor and electron-donor substituents. It was shown that the modification method characteristic for materials containing aromatic structures may be successfully applied to the functionalization of carbon materials. The effectiveness of the surface modification of carbon nonwoven fabrics was confirmed by the FTIR method using an ATR device. The proposed approach allows the incorporation of various functional groups on the nonwovens’ surface, which affects the morphology of fibers as well as their physicochemical properties (wettability). The introduction of a carboxyl group on the surface of nonwoven fabrics, in a reaction with 4-aminobenzoic acid, became a starting point for further modifications necessary for the attachment of RGD-type peptides facilitating cell adhesion to the surface of materials. The surface modification reduced the wettability (θ) of the carbon nonwoven by about 50%. The surface free energy (SFE) in the chemically modified and reference nonwovens remained similar, with the surface modification causing an increase in the polar component (ɣp). The modification of the fiber surface was heterogeneous in nature; however, it provided an attractive site of cell–materials interaction by contacting them to the fiber surface, which supports the adhesion process.

Material Reliability of Low-Temperature Boron Deposition for PureB Silicon Photodiode Fabrication

MRS Advances ◽  
2018 ◽  
Vol 3 (57-58) ◽  
pp. 3397-3402 ◽  
Author(s):  
L.K. Nanver ◽  
K. Lyon ◽  
X. Liu ◽  
J. Italiano ◽  
J. Huffman
Keyword(s):  
High Temperature ◽  
Layer Thickness ◽  
Vapor Deposition ◽  
Dark Current ◽  
Deposition Temperature ◽  
Chemical Vapor ◽  
Silicon Photodiode ◽  
In Situ Methods ◽  
Deposition Conditions

ABSTRACTThe chemical-vapor deposition conditions for the growth of pure boron (PureB) layers on silicon at temperatures as low as 400°C were investigated with the purpose of optimizing photodiodes fabricated with PureB anodes for minimal B-layer thickness, low dark current and chemical robustness. The B-deposition is performed in a commercially-available Si epitaxial reactor from a diborane precursor. In-situ methods commonly used to improve the cleanliness of the Si surface before deposition are tested for a deposition temperature of 450°C and PureB layer thickness of 3 nm. Specifically, high-temperature baking in hydrogen, and exposure to HCl are tested. Both material analysis and electrical diode characterization indicate that these extra cleaning steps degrade the properties of the PureB layer and the fabricated diodes.

In Situ Methods for Identifying the Stem Cell of the Normal and Cancerous Breast

2014 ◽  
pp. 151-182 ◽  
Author(s):  
Yanrong Su ◽  
Pedro J. Gutiérrez Diez ◽  
Julia Santucci-Pereira ◽  
Irma H. Russo ◽  
Jose Russo
Keyword(s):  
Stem Cell ◽  
In Situ Methods
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