scholarly journals Issuing Cast Lead Coins in Byzantine Cherson: A Local Phenomenon or a Technological “Flaw”?

2021 ◽  
pp. 447-458
Author(s):  
Nikolay A., Alekseienko ◽  
Anna V. Antipenko
Keyword(s):  
Laboratory Research ◽  
Specific Kind ◽  
Standard Samples ◽  
Special Equipment ◽  
The Caucasus ◽  
Pure Lead ◽  
X Ray ◽  
Long Time ◽  
Byzantine Period ◽  
The One

Although the aspects of the production of Byzantine-Cherson cast coins and the technological nuances of their manufacture have been repeatedly studied in Russian scholarship, every time there appeared various hypotheses and assumptions, mostly remain highly debatable so far. For a long time, the lack or difficulties of access to the special equipment allowing the one to determine coin alloys allowed the researchers to draw conclusions about the coin material only against the background of some definitions from the scholarship and visual indicators. Among the disputable aspects is the casting of Cherson-Byzantine lead coins. In this connection, we have studied 30 specimens of coins by laboratory research of the alloy composition by X-ray fluorescent analysis. The samples selected for examination visually suggested a high content of lead. It has been found out that in the samples examined have similar elemental composition of coin alloy, lead with additions of arsenic. It is possible that, in the Byzantine Period, the Taurica received lead from the mines located in the Caucasus area, which were typical of a high content of arsenic. The most part of the of samples (27 specimens) contained more than 2/3 of lead; the alloy of three coins contained similar proportions of copper and lead. Taking the said results into account, we can suppose that the “almost pure” lead coins most likely were a specific kind of technological “flaw” in the casting in Cherson. It is still possible that, in the sorting of the ready-made coins, the specimens not corresponding to the standard samples and having casting defects (partial casting of the mould or lead casts) were withdrawn and returned to remaking. This interpretation explains why the so-called “lead” coins are relatively rare: they occurred mostly in the coinages from the age of Basil I and Leo VI, though in some series they were unique or unknown.

scholarly journals DEVELOPMENT OF METHODS FOR ASSESSMENT AND SELECTION OF UNMANNED AERIAL VEHICLE FOR MINE RECONNAISSANCE

ScienceRise ◽  
2020 ◽  
pp. 44-50
Author(s):  
Vadym Neroba
Keyword(s):  
Unmanned Aerial Vehicle ◽  
Comparative Assessment ◽  
Problem Solution ◽  
Special Equipment ◽  
Long Time ◽  
Aerial Vehicle ◽  
Scientific Results ◽  
The One ◽  
Selection Of ◽  
Technological Product

Object of research: comparative assessment and selection of an unmanned aerial vehicle for mine reconnaissance sample. Investigated problem: substantiation of the methodological apparatus for comparative assessment and selection of an unmanned aerial vehicle for mine reconnaissance sample, taking into consideration the presence of both quantitative and qualitative indicators. Main scientific results: the methods of comparative assessment and selection of an unmanned aerial vehicle for mine reconnaissance sample is developed. The technique is based on an expert method, which allows a drone sample to be evaluated and selected objectively, taking into consideration the presence of both quantitative and qualitative indicators. At the same time, group interaction and discussion of experts are realized. When the judgments do not coincide, an artificial consensus is not imposed. The number of experts is not limited. The experts are not linked in any way. The need to ensure transitive consistency (10–12 %) makes it possible to record attempts by an expert (experts) to artificially overestimate the indicators of one of the drone samples (or the one being evaluated), therefore, the indicators of another sample will automatically deteriorate. The principle of impartiality and fairness is maintained. A well-trained objective coordinator is not required, and the reality is that the absence of the disrupting the problem solution possibility is due to a change in the psychological situation among the experts. Area of practical use of research results: humanitarian demining in the interests of ensuring the detection of mines for various purposes by sappers from a safe distance. At the same time, an increase within the probability of mines detecting is ensured due to special equipment installed onboard the drone. Innovative technological product: a technique has been developed that allows not only assessing the drone samples for mine reconnaissance objectively, but making an objective choice of a sample for specific requirements also. Scope of application of the innovative technological product: clearance of the terrain remaining after the end of hostilities. With the help of unmanned aerial vehicles, a significant acceleration of the demining process is possible, especially in those territories where mines are installed and being for a sufficiently long time.

The f-Ratio Quantification Method for X-ray Microanalysis Applied to Mg–Al–Zn Alloys

2019 ◽  
Vol 25 (1) ◽  
pp. 58-69 ◽  
Author(s):  
Chaoyi Teng ◽  
Hendrix Demers ◽  
Xin Chu ◽  
Raynald Gauvin
Keyword(s):  
Binary Systems ◽  
Beam Current ◽  
Ratio Method ◽  
Standard Samples ◽  
X Ray ◽  
Quantification Method ◽  
Long Time ◽  
Quantification Accuracy ◽  
The Stability ◽  
Accurate Quantification

AbstractThe f-ratio quantitative X-ray microanalysis method has been recently developed for binary systems based on a scanning electron microscope/energy dispersive spectroscopy (SEM/EDS) system. This method incorporates traditional EDS experiments and Monte Carlo simulations, and calibration factors are calculated with standard samples to evaluate the differences between them. In this work, the f-ratio method was extended to Mg–Al–Zn multi-element systems using a cold field emission SEM and a tungsten emission SEM. Results show that the stability of the beam current does not influence the f-ratio quantification accuracy. Thus, the f-ratio method is suitable for quantitative X-ray mapping with a long-time acquisition or even an unstable beam current. Comparing with other quantitative techniques including the routine standardless analysis and the standard-based k-ratio method, the f-ratio method is a simple and accurate quantification method.

Alkohol im Tank – Bio-Kraftstoffe und die Grenzen moderner Mobilität

2004 ◽  
Vol 34 (136) ◽  
pp. 455-468
Author(s):  
Hartwig Berger
Keyword(s):  
Third World ◽  
Fossil Fuel ◽  
Energy Resources ◽  
The Third ◽  
Political Conflicts ◽  
The Future ◽  
Long Time ◽  
Food Market ◽  
The One ◽  
The Third World

The article discusses the future of mobility in the light of energy resources. Fossil fuel will not be available for a long time - not to mention its growing environmental and political conflicts. In analysing the potential of biofuel it is argued that the high demands of modern mobility can hardly be fulfilled in the future. Furthermore, the change into using biofuel will probably lead to increasing conflicts between the fuel market and the food market, as well as to conflicts with regional agricultural networks in the third world. Petrol imperialism might be replaced by bio imperialism. Therefore, mobility on a solar base pursues a double strategy of raising efficiency on the one hand and strongly reducing mobility itself on the other.

Sorption of Se (IV) from aqueous solutions with subsequent determination by X-ray fluorescence analysis

2020 ◽  
Vol 86 (10) ◽  
pp. 5-9
Author(s):  
D. G. Filatova ◽  
A. A. Arkhipenko ◽  
M. A. Statkus ◽  
V. V. Es’kina ◽  
V. B. Baranovskaya ◽  
...  
Keyword(s):  
Inductively Coupled Plasma ◽  
Fluorescence Analysis ◽  
Standard Samples ◽  
Phase Contact Time ◽  
Sorbent Phase ◽  
X Ray ◽  
Fundamental Parameters ◽  
Inductively Coupled ◽  
Subsequent Determination

An approach to sorptive separation of Se (IV) from solutions on a novel S,N-containing sorbent with subsequent determination of the analyte in the sorbent phase by micro-x-ray fluorescence method is presented. The sorbent copolymethylenesulfide-N-alkyl-methylenamine (CMA) was synthesized using «snake in the cage» procedure and proven to be stable in acid solutions. Conditions for quantitative extraction of Se (IV) were determined: sorption in 5 M HCl or 0.05 M HNO3 solutions when heated to 60°C, phase contact time being 1 h. The residual selenium content in the solution was determined by inductively coupled plasma mass spectrometry (ICP-MS) using 82Se isotope. The absence of selenium losses is proved and the mechanism of sorption interaction under specified conditions is proposed. The method of micro-x-ray fluorescence analysis (micro-RFA) with mapping revealed a uniform distribution of selenium on the sorbent surface. The possibility of determining selenium in the sorbent phase by micro-RFA is shown. When comparing the obtained results with the results of calculations by the method of fundamental parameters, it is shown the necessity of using standard samples of sorbates to obtain correct results of RFA determination of selenium in the sorbent phase.

Making it abstract, making it contestable: Gender/sex as a politicized concept

2020 ◽  
Author(s):  
Claudia Mazzuca ◽  
Matteo Santarelli
Keyword(s):  
Social Sciences ◽  
Main Question ◽  
Abstract Concepts ◽  
Biological Feature ◽  
Dynamic Approach ◽  
Cognitive Sciences ◽  
Long Time ◽  
Cultural Construct ◽  
Science Framework ◽  
The One

The concept of gender has been the battleground of scientific and political speculations for a long time. On the one hand, some accounts contended that gender is a biological feature, while on the other hand some scholars maintained that gender is a socio-cultural construct (e.g., Butler, 1990; Risman, 2004). Some of the questions that animated the debate on gender over history are: how many genders are there? Is gender rooted in our biological asset? Are gender and sex the same thing? All of these questions entwine one more crucial, and often overlooked interrogative. How is it possible for a concept to be the purview of so many disagreements and conceptual redefinitions? The question that this paper addresses is therefore not which specific account of gender is preferable. Rather, the main question we will address is how and why is even possible to disagree on how gender should be considered. To provide partial answers to these questions, we suggest that gender/sex (van Anders, 2015; Fausto-Sterling, 2019) is an illustrative example of politicized concepts. We show that no concepts are political in themselves; instead, some concepts are subjected to a process involving a progressive detachment from their supposed concrete referent (i.e., abstractness), a tension to generalizability (i.e., abstraction), a partial indeterminacy (i.e., vagueness), and the possibility of being contested (i.e., contestability). All of these features differentially contribute to what we call the politicization of a concept. In short, we will claim that in order to politicize a concept, a possible strategy is to evidence its more abstract facets, without denying its more embodied and perceptual components (Borghi et al., 2019). So, we will first outline how gender has been treated in psychological and philosophical discussions, to evidence its essentially contestable character thereby showing how it became a politicized concept. Then we will review some of the most influential accounts of political concepts, arguing that currently they need to be integrated with more sophisticated distinctions (e.g., Koselleck, 2004). The notions gained from the analyses of some of the most important accounts of political concepts in social sciences and philosophy will allow us to implement a more dynamic approach to political concepts. Specifically, when translated into the cognitive science framework, these reflections will help us clarifying some crucial aspects of the nature of politicized concepts. Bridging together social and cognitive sciences, we will show how politicized concepts are abstract concepts, or better abstract conceptualizations.

scholarly journals On Performance of Sparse Fast Fourier Transform Algorithms Using the Aliasing Filter

Electronics ◽  
2021 ◽  
Vol 10 (9) ◽  
pp. 1117
Author(s):  
Bin Li ◽  
Zhikang Jiang ◽  
Jie Chen
Keyword(s):  
Fourier Transform ◽  
Fast Fourier Transform ◽  
High Efficiency ◽  
Theory And Practice ◽  
Long Time ◽  
And Performance ◽  
Binary Tree Search ◽  
The One ◽  
Sparse Fast Fourier Transform ◽  
L1 And L2

Computing the sparse fast Fourier transform (sFFT) has emerged as a critical topic for a long time because of its high efficiency and wide practicability. More than twenty different sFFT algorithms compute discrete Fourier transform (DFT) by their unique methods so far. In order to use them properly, the urgent topic of great concern is how to analyze and evaluate the performance of these algorithms in theory and practice. This paper mainly discusses the technology and performance of sFFT algorithms using the aliasing filter. In the first part, the paper introduces the three frameworks: the one-shot framework based on the compressed sensing (CS) solver, the peeling framework based on the bipartite graph and the iterative framework based on the binary tree search. Then, we obtain the conclusion of the performance of six corresponding algorithms: the sFFT-DT1.0, sFFT-DT2.0, sFFT-DT3.0, FFAST, R-FFAST, and DSFFT algorithms in theory. In the second part, we make two categories of experiments for computing the signals of different SNRs, different lengths, and different sparsities by a standard testing platform and record the run time, the percentage of the signal sampled, and the L0, L1, and L2 errors both in the exactly sparse case and the general sparse case. The results of these performance analyses are our guide to optimize these algorithms and use them selectively.

scholarly journals ZnOTe Compounds Grown by DC-Magnetron Co-Sputtering

Coatings ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 570
Author(s):  
Olga Sánchez ◽  
Manuel Hernández-Vélez
Keyword(s):  
Molar Fraction ◽  
Variable Parameter ◽  
Point Of View ◽  
X Ray Diffraction ◽  
X Ray ◽  
Sample Series ◽  
Solid Phases ◽  
The One ◽  
High Bulk ◽  
Substrate Sample

ZnOTe compounds were grown by DC magnetron cosputtering from pure Tellurium (Te) and Zinc (Zn) cathodes in O2/Ar atmosphere. The applied power on the Zn target was constant equal to 100 W, while the one applied on the Te target took two values, i.e., 5 W and 10 W. Thus, two sample series were obtained in which the variable parameter was the distance from the Te targets to the substrate. Sample compositions were determined by Rutherford Backscattering Spectroscopy (RBS) experiments. Structural analysis was done using X-Ray diffraction (XRD) spectrometry and the growth of the hexagonal w-ZnO phase was identified in the XRD spectra. RBS results showed high bulk homogeneity of the samples forming ZnOTe alloys, with variable Te molar fraction (MF) ranging from 0.48–0.6% and from 1.9–3.1% for the sample series obtained at 5 W and 10 W, respectively. The results reflect great differences between the two sample series, particularly from the structural and optical point of view. These experiments point to the possibility of Te doping ZnO with the permanence of intrinsic defects, as well as the possibility of the formation of other Te solid phases when its content increases. The results and appreciable variations in the band gap transitions were detected from Photoluminescence (PL) measurements.

scholarly journals Bottom-Up Generation of Peak Demand Scenarios in Water Distribution Networks

2020 ◽  
Vol 13 (1) ◽  
pp. 31
Author(s):  
Enrico Creaco ◽  
Giacomo Galuppini ◽  
Alberto Campisano ◽  
Marco Franchini
Keyword(s):  
Water Distribution ◽  
Distribution Networks ◽  
Water Distribution Networks ◽  
Peak Demand ◽  
Long Time ◽  
Cross Correlations ◽  
User Demand ◽  
One Year ◽  
The One ◽  
Best Fit

This paper presents a two-step methodology for the stochastic generation of snapshot peak demand scenarios in water distribution networks (WDNs), each of which is based on a single combination of demand values at WDN nodes. The methodology describes the hourly demand at both nodal and WDN scales through a beta probabilistic model, which is flexible enough to suit both small and large demand aggregations in terms of mean, standard deviation, and skewness. The first step of the methodology enables generating separately the peak demand samples at WDN nodes. Then, in the second step, the nodal demand samples are consistently reordered to build snapshot demand scenarios for the WDN, while respecting the rank cross-correlations at lag 0. The applications concerned the one-year long dataset of about 1000 user demand values from the district of Soccavo, Naples (Italy). Best-fit scaling equations were constructed to express the main statistics of peak demand as a function of the average demand value on a long-time horizon, i.e., one year. The results of applications to four case studies proved the methodology effective and robust for various numbers and sizes of users.

scholarly journals Nanostructural Arrangements and Surface Morphology on Ureasil-Polyether Films Loaded with Dexamethasone Acetate

Nanomaterials ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 1362
Author(s):  
Joao Augusto Oshiro ◽  
Angelo Lusuardi ◽  
Elena M. Beamud ◽  
Leila Aparecida Chiavacci ◽  
M. Teresa Cuberes
Keyword(s):  
Film Surface ◽  
Crystalline Phases ◽  
Essential Information ◽  
X Ray ◽  
Force Microscopy ◽  
Ether Oxygen ◽  
Dexamethasone Acetate ◽  
Poly Ethylene ◽  
The One ◽  
Poly Propylene

Ureasil-Poly(ethylene oxide) (ureasil-PEO500) and ureasil-Poly(propylene oxide) (u-PPO400) films, unloaded and loaded with dexamethasone acetate (DMA), have been investigated by carrying out atomic force microscopy (AFM), ultrasonic force microscopy (UFM), contact-angle, and drug release experiments. In addition, X-ray diffraction, small angle X-ray scattering, and infrared spectroscopy have provided essential information to understand the films’ structural organization. Our results reveal that while in u-PEO500 DMA occupies sites near the ether oxygen and remains absent from the film surface, in u-PPO400 new crystalline phases are formed when DMA is loaded, which show up as ~30–100 nm in diameter rounded clusters aligned along a well-defined direction, presumably related to the one defined by the characteristic polymer ropes distinguished on the surface of the unloaded u-POP film; occasionally, larger needle-shaped DMA crystals are also observed. UFM reveals that in the unloaded u-PPO matrix the polymer ropes are made up of strands, which in turn consist of aligned ~180 nm in diameter stiffer rounded clusters possibly formed by siloxane-node aggregates; the new crystalline phases may grow in-between the strands when the drug is loaded. The results illustrate the potential of AFM-based procedures, in combination with additional physico-chemical techniques, to picture the nanostructural arrangements in polymer matrices intended for drug delivery.

scholarly journals Determination of the Height of Hard X-Ray Sources in the Solar Atmosphere by Measurement of Photospheric Albedo Photons

1975 ◽  
Vol 68 ◽  
pp. 239-241
Author(s):  
John C. Brown ◽  
H. F. Van Beek
Keyword(s):  
Solar Atmosphere ◽  
The Other ◽  
X Ray ◽  
Theoretical Predictions ◽  
Source Models ◽  
The One

SummaryThe importance and difficulties of determining the height of hard X-ray sources in the solar atmosphere, in order to distinguish source models, have been discussed by Brown and McClymont (1974) and also in this Symposium (Brown, 1975; Datlowe, 1975). Theoretical predictions of this height, h, range between and 105 km above the photosphere for different models (Brown and McClymont, 1974; McClymont and Brown, 1974). Equally diverse values have been inferred from observations of synchronous chromospheric EUV bursts (Kane and Donnelly, 1971) on the one hand and from apparently behind-the-limb events (e.g. Datlowe, 1975) on the other.

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