X-ray TV inspection of the quality of welding polyethylene pipes

2021 ◽  
Vol 2021 (3) ◽  
pp. 33-36
Author(s):  
M.M. Karmanov ◽  
◽  
S.R. Mikhailov ◽  
R.O. Pastovenksyi ◽  
V.Yu. Glukhіvskyi ◽  
...  
Keyword(s):  
X Ray ◽  
Polyethylene Pipes

X-ray fluorescence determination of zinc sulfate in acidic zinc plating electrolyte

2020 ◽  
Vol 86 (10) ◽  
pp. 18-22
Author(s):  
K. N. Vdovin ◽  
K. G. Pivovarova ◽  
N. A. Feoktistov ◽  
T. B. Ponamareva
Keyword(s):  
Zinc Sulfate ◽  
Zinc Coating ◽  
Electrolyte Composition ◽  
Complexometric Titration ◽  
X Ray ◽  
Fluorescence Determination ◽  
Zinc Plating ◽  
Zinc Determination

Zinc sulfate is the main component in the composition of the acidic zinc plating electrolyte. Deviation in the electrolyte composition from the optimum content leads to destabilization of the electrolysis process and deteriorate the quality of the resulting zinc coating. The proper quality of a zinc coating obtained by galvanic deposition can be ensured only with timely monitoring and adjustment of the electrolyte composition. A technique of X-ray fluorescence determination of zinc (in terms of zinc sulfate) in an acidic zinc plating electrolyte is proposed. The study was carried out using an ARL Quant’X energy dispersive spectrometer (Thermo Fisher Scientific, USA) with a semiconductor silicon-lithium detector. The features of the spectrometer design are presented. The optimal parameters of excitation and detection of zinc radiation were specified when the electrolyte sample was diluted 1:1000. The ZnKα1 line was used as an analytical line. The plotted calibration graph is linear, the correlation coefficient being 0.999234. The results of zinc determination according to the developed method were compared with the data of the reference method of complexometric titration to prove the reliability of the procedure. The results are characterized by good convergence and accuracy. The proposed method of X-ray fluorescence zinc determination in a zinc plating electrolyte equals complexometric titration in the limiting capabilities and even exceeds the latter in terms of the simplicity of sample preparation and rapidity. The developed method of X-ray fluorescence determination of zinc is implemented in analysis of the electrolyte used in the continuous galvanizing unit at «METSERVIS LLC».

Counterfeit Parts Recognition and Detection for Failure Analysts

2010 ◽  
Author(s):  
Katherine V. Whittington
Keyword(s):  
Thermal Cycle ◽  
Visual Inspection ◽  
Acoustic Microscopy ◽  
Scanning Acoustic Microscopy ◽  
3D Measurement ◽  
X Ray ◽  
Wide Range ◽  
Electronic Parts ◽  
Testing Awareness

Abstract The electronics supply chain is being increasingly infiltrated by non-authentic, counterfeit electronic parts, whose use poses a great risk to the integrity and quality of critical hardware. There is a wide range of counterfeit parts such as leads and body molds. The failure analyst has many tools that can be used to investigate counterfeit parts. The key is to follow an investigative path that makes sense for each scenario. External visual inspection is called for whenever the source of supply is questionable. Other methods include use of solvents, 3D measurement, X-ray fluorescence, C-mode scanning acoustic microscopy, thermal cycle testing, burn-in technique, and electrical testing. Awareness, vigilance, and effective investigations are the best defense against the threat of counterfeit parts.

OSTEOPOROSIS AND RISK FACTORS IN THE PATIENTS ON CHRONIC HEMODIALYSIS

2015 ◽  
pp. 50-58
Author(s):  
Thi Dung Nguyen ◽  
Tam Vo
Keyword(s):  
Quality Of Life ◽  
Risk Factors ◽  
Bone Density ◽  
Region Of Interest ◽  
Cross Sectional Study ◽  
Chronic Hemodialysis ◽  
Cross Sectional ◽  
X Ray ◽  
Density Reduction

Background: The patients on hemodialysis have a significantly decreased quality of life. One of many problems which reduce the quality of life and increase the mortality in these patients is osteoporosis and osteoporosis associated fractures. Objectives: To assess the bone density of those on hemodialysis by dual energy X ray absorptiometry and to examine the risk factors of bone density reduction in these patients. Patients and Method: This is a cross-sectional study, including 93 patients on chronic hemodialysis at the department of Hemodialysis at Cho Ray Hospital. Results: Mean bone densities at the region of interest (ROI) neck, trochanter, Ward triangle, intertrochanter and total neck are 0.603 ± 0.105; 0.583 ± 0.121; 0.811 ± 0.166; 0.489 ± 0.146; 0.723 ± 0.138 g/cm2 respectively. The prevalences of osteoporosis at those ROI are 39.8%, 15.1%; 28%; 38.7%; and 26.9% respectively. The prevalences of osteopenia at those ROI are 54.8%; 46.3%; 60.2%; 45.2% and 62.7% respectively. The prevalence of osteopososis in at least one ROI is 52.7% and the prevalence of osteopenia in at least one ROI is 47.3%. There are relations between the bone density at the neck and the gender of the patient and the albuminemia. Bone density at the trochanter is influenced by gender, albuminemia, calcemia and phosphoremia. Bone density at the intertrochanter is affected by the gender. Bone density at the Ward triangle is influenced by age and albuminemia. Total neck bone density is influenced by gender, albuminemia and phosphoremia. Conclusion: Osteoporosis in patients on chronic hemodialysis is an issue that requires our attention. There are many interventionable risk factors of bone density decrease in these patients. Key words: Osteoporosis, DEXA, chronic renal failure, chronic hemodialysis

scholarly journals X-ray diffraction analysis of kaolin M1 and M2 via the Williamson–Hall and Warren–Averbach methods

2021 ◽  
pp. 174751982098472
Author(s):  
Lalmi Khier ◽  
Lakel Abdelghani ◽  
Belahssen Okba ◽  
Djamel Maouche ◽  
Lakel Said
Keyword(s):  
Grain Size ◽  
High Temperature ◽  
Low Temperature ◽  
Diffraction Analysis ◽  
Mechanical Resistance ◽  
X Ray Diffraction ◽  
Integral Breadth ◽  
X Ray ◽  
Mullite Phase

Kaolin M1 and M2 studied by X-ray diffraction focus on the mullite phase, which is the main phase present in both products. The Williamson–Hall and Warren–Averbach methods for determining the crystallite size and microstrains of integral breadth β are calculated by the FullProf program. The integral breadth ( β) is a mixture resulting from the microstrains and size effect, so this should be taken into account during the calculation. The Williamson–Hall chart determines whether the sample is affected by grain size or microstrain. It appears very clearly that the principal phase of the various sintered kaolins, mullite, is free from internal microstrains. It is the case of the mixtures fritted at low temperature (1200 °C) during 1 h and also the case of the mixtures of the type chamotte cooks with 1350 °C during very long times (several weeks). This result is very significant as it gives an element of explanation to a very significant quality of mullite: its mechanical resistance during uses at high temperature remains.

scholarly journals Mobility and Bioavailability of Metal(loid)s in a Fluvial System Affected by the Mining and Industrial Processing of Pb

Geosciences ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 167
Author(s):  
Unai Cortada ◽  
María Carmen Hidalgo ◽  
Julián Martínez ◽  
María José de la Torre
Keyword(s):  
Total Concentration ◽  
Rare Metal ◽  
Mining District ◽  
X Ray ◽  
Industrial Processing ◽  
Solids Concentration ◽  
Mobile Fraction ◽  
Type Water ◽  
The Impact

The abandoned mining district of Linares (South Spain) is marked with waste from the mining and the processing of metal ores that pose an environmental hazard to watercourses. A combined analysis of waste, sediments and water was carried out to analyse the impact of a smelter on Baños Creek. The composition of the facility waste was determined using X-ray diffractometry and scanning electron microscopy. The total contents of the metal(loid)s in the waters and sediments of the watercourse were analysed, and sequential metal(loid) extraction of solid samples was carried out. The facility wastes consisted mainly of secondary minerals, such as natropharmacosiderite and spertiniite, as well as rare metal salts, such as mopungite and NaPb2(CO3)2(OH). The leachates generated by these wastes were highly alkaline, with a pH of 10 and a total dissolved solids concentration of approximately 9 g L−1. This Na-bicarbonate-type water had an As concentration above 200 mg L−1 and elevated levels of Pb, Sb and Zn (5029 µg L−1, 841 µg L−1 and 525 µg L−1, respectively). This highly contaminated lixiviate had a significant effect on the chemical quality of the waters and the bioavailability of metal(loid)s in the creek sediments, especially in the headwaters. In this zone, the As, Pb, Sb and Zn concentrations in the most mobile fraction of the sediments reached 1035 mg kg−1, 261 mg kg−1, 45 mg kg−1 and 30 mg kg−1, respectively. By comparison, smelter slag and mining waste have a much lower impact on the waters and the mobile fraction of the sediments, while significantly increasing the total concentration of these potentially toxic elements in creek sediments.

scholarly journals Automated evaluation of the surface point quality in dimensional X-ray computed tomography

2020 ◽  
Vol 87 (2) ◽  
pp. 111-121 ◽  
Author(s):  
Andreas Michael Müller ◽  
Lorenz Butzhammer ◽  
Florian Wohlgemuth ◽  
Tino Hausotte
Keyword(s):  
Computed Tomography ◽  
Surface Point ◽  
Random Measurement Error ◽  
X Ray ◽  
Random Measurement ◽  
Automated Evaluation ◽  
Dimensional Measurements ◽  
X Ray Computed ◽  
Model Measurement

AbstractX-ray computed tomography (CT) enables dimensional measurements of numerous measurands with a single scan, including the measurement of inner structures. However, measurement artefacts complicate the applicability of the technology in some cases. This paper presents a methodology to assess the surface point quality of computed tomography measurements without the requirement of a CAD model. Measurement artefacts lowering the surface point quality can therefore automatically be detected. The correlation of quality values with the random measurement error is demonstrated. The presented method can in principle be used to weight single fit points to reduce the measurement uncertainty of CT measurements.

Die Bonding Issues on Silicon Carbide Diodes

2006 ◽  
Vol 527-529 ◽  
pp. 875-878 ◽  
Author(s):  
Seung Yong Lee ◽  
Jang Sub Lee ◽  
Tae Hong Kim ◽  
Sung Yong Choi ◽  
Hak Jong Kim ◽  
...  
Keyword(s):  
Shear Test ◽  
Vertical Structure ◽  
Optical Microscope ◽  
Device Fabrication ◽  
Cleaning Process ◽  
X Ray ◽  
The Third ◽  
Bottom Side ◽  
Die Bonding

We report on the die bonding processes and how the surface roughness and metallization schemes affect the processes of die bonding in 4H-SiC device fabrication using a soldering test and die shear test (DST) with differently prepared 4H-SiC samples. The first set of samples (FZ#1 and FZ#2) was capped with sequentially evaporated Ti and Au on an annealed Ni layer. The second set of samples (FZ#3 and FZ#4) and the third set of samples (FZ#5 and FZ#6) were prepared by 4μm-thick Au electroplating on an annealed Ni layer and an un-annealed Ni layer, respectively. The quality of the soldering, such as the solder coverage, void, and adhesion, was characterized by optical microscope, X-ray microprobe, and DST. We found that the samples (FZ#4 and FZ#6) deposited by Au electroplating on C-face (bottom-side) 4H-SiC provided a satisfactory result for the tests of solder coverage, void, and DST and also realized the cleaning process prior to the electroplating and soldering was the most crucial in the die packaging processes of vertical structure devices. The void fraction measured by X-ray microprobe for the samples, FZ#4 and FZ#6 was 2.2% (average for 5 samples) and 0.8% (average for 3 samples), respectively.

Study of the quality of GaAs thin film on Si substrate by X-ray diffraction method

1990 ◽  
Vol 7 (7) ◽  
pp. 308-311
Author(s):  
Li Chaorong ◽  
Mai Zhenhong ◽  
Cui Shufan ◽  
Zhou Junming ◽  
Yutian Wang
Keyword(s):  
Thin Film ◽  
Diffraction Method ◽  
X Ray Diffraction ◽  
Si Substrate ◽  
X Ray

X-ray analysis of the technological quality of silicocalcium

2007 ◽  
Vol 37 (2) ◽  
pp. 99-100
Author(s):  
G. L. Borshchevskaya ◽  
G. M. Tirakov ◽  
V. I. Dmitrienko ◽  
R. A. Gizatulin
Keyword(s):  
X Ray ◽  
Technological Quality

scholarly journals Short-pulse laser-driven x-ray radiography

2016 ◽  
Vol 4 ◽  
Author(s):  
E. Brambrink ◽  
S. Baton ◽  
M. Koenig ◽  
R. Yurchak ◽  
N. Bidaut ◽  
...  
Keyword(s):  
Pulse Laser ◽  
Short Pulse ◽  
Incident Angle ◽  
Laboratory Astrophysics ◽  
Signal To Noise ◽  
High Quality ◽  
X Ray ◽  
Short Pulse Laser ◽  
Short Pulse Lasers

We have developed a new radiography setup with a short-pulse laser-driven x-ray source. Using a radiography axis perpendicular to both long- and short-pulse lasers allowed optimizing the incident angle of the short-pulse laser on the x-ray source target. The setup has been tested with various x-ray source target materials and different laser wavelengths. Signal to noise ratios are presented as well as achieved spatial resolutions. The high quality of our technique is illustrated on a plasma flow radiograph obtained during a laboratory astrophysics experiment on POLARs.

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