Oxidation Study of Pure Fe and Fe-36Ni Alloy at Elevated Temperature

2013 ◽  
Vol 328 ◽  
pp. 784-788
Author(s):  
Sang An Ha ◽  
Shun Myung Shin ◽  
Jung Yeul Yun ◽  
Jei Pil Wang
Keyword(s):  
Grain Size ◽  
Elevated Temperature ◽  
Oxidation Rate ◽  
Cold Work ◽  
Iron And Steel ◽  
Fine Grained ◽  
Oxidation Study ◽  
Different Temperatures ◽  
Forming Temperature ◽  
Cold Worked

There have been many studies on the oxidation of pure iron and steel at different temperatures and pressures. D. Caplan et al. demonstrated the effect of cold-work and metal grain size on the oxidation rate of iron. It was concluded that the oxidation rate of iron was accelerated with temperature, cold-work, and increased oxygen pressure, while the oxidation rate of iron, coarse-or fine-grained, cold-worked or annealed, was found to be the same at the FeO-forming temperature range [1-3].

Microstructure and Elevated Temperature Flow Properties of Rapidly Solidified TiAl-Base Alloys

1988 ◽  
Vol 133 ◽  
Author(s):  
J. A. Graves ◽  
A. K. Ghosh
Keyword(s):  
Grain Size ◽  
Elevated Temperature ◽  
Fine Grained ◽  
Alloy Chemistry ◽  
Property Evaluation ◽  
Metastable Structure ◽  
Equilibrium Solidification ◽  
Solidification Pathway ◽  
The Stability ◽  
Temperature Exposure

ABSTRACTRapid solidification processing (RSP) of TiAl-base alloys often results in the formation of metastable crystalline products (e.g., Ti3Al) A key parameter controlling both the solidification pathway and the stability of the metastable structure is alloy chemistry. This study focuses upon the influence of minor alloy additions on the microstructure and properties of Ti52Al48 alloys produced by RSP. While alloys having minor Ta addi ions (<1 at.%) maintain near-equilibrium solidification structures similar to the binary alloy, the addition of Cr at a level of 5 at.% results in a nearly 100 vol.% metastable Ti3Al structure containing a fine dispersion of TiCr2 grain boundary precipitates. These precipitates limit grain growth during elevated temperature exposure, maintaining the fine (TiAl) grain size created during decomposition of the metastable product structure. Mechanical property evaluation of the consolidated RSP material indicates a greatly reduced flow stress for the fine grained Cr modified alloys. A preliminary analysis attributes this to the reduction in grain size and enhanced elevated temperature diffusion rates for the Cr containing TiAl-base alloys.

Elevated temperature deformation of fine-grained La0.9Sr0.1MnO3

1996 ◽  
Vol 11 (3) ◽  
pp. 657-662 ◽  
Author(s):  
J. Wolfenstine ◽  
T. R. Armstrong ◽  
W. J. Weber ◽  
M. A. Boling-Risser ◽  
K. C. Goretta ◽  
...  
Keyword(s):  
Activation Energy ◽  
Grain Size ◽  
Elevated Temperature ◽  
Perovskite Oxides ◽  
Lattice Diffusion ◽  
Diffusional Creep ◽  
Temperature Deformation ◽  
Creep Data ◽  
Fine Grained ◽  
Fine Grain

Compressive creep behavior of fine-grained (5 μm) La0.9Sr0.1MnO3with a relative theoretical density between 85 and 90% was investigated over the temperature range 1150–1300 °C in air. The fine grain size, brief creep transients, stress exponent close to unity, and absence of deformation-induced dislocations, suggested that the deformation was controlled by a diffusional creep mechanism. The activation energy for creep of La0.9Sr0.1MnO3was 490 kJ/mole. A comparison of the activation energy for creep of La0.9Sr0.1MnO3with existing diffusion and creep data for perovskite oxides suggested that the diffusional creep of La0.9Sr0.1MnO3was controlled by lattice diffusion of the cations, either lanthanum or manganese.

Nanopowder and Fine-Grained Ceramics for Multilayer PTCR Elements

2008 ◽  
Vol 368-372 ◽  
pp. 453-455 ◽  
Author(s):  
Jun Zhao ◽  
Shu Ping Gong ◽  
Chun Fang Cheng ◽  
Zhi Ping Zheng ◽  
Huan Liu ◽  
...  
Keyword(s):  
Grain Size ◽  
Sintering Temperature ◽  
Boundary Effect ◽  
Sol Gel ◽  
Tape Casting ◽  
Casting Technique ◽  
Fine Grained ◽  
Average Grain Size ◽  
Sol Gel Process ◽  
Different Temperatures

BaTiO3 nanopowders prepared by sol-gel process were used for multilayer PTCR ceramics in order to utilize grain boundary effect and lower sintering temperature. The precursor gel was calcined at different temperatures and the powders were characterized by XRD and TEM. The average grain size was about 26nm when calcined at 800°C for 2h. Effects of acceptor/donor concentration and sintering temperature on PTCR ceramics were also investigated. The optimal concentration of the donor was found to be 0.6mol with the acceptor concentration being 1/8 of the donor. Multilayer PTCR elements were fabricated by tape-casting technique. The jump ratio of PTCR chips sintered at 1240°C was above 103 with the average grain size smaller than 1~2 μm, which is suitable for the multilayer PTCR elements.

J&L TYPE 309

Alloy Digest ◽  
2003 ◽  
Vol 52 (12) ◽  
Keyword(s):  
Stainless Steel ◽  
Corrosion Resistance ◽  
High Temperature ◽  
Elevated Temperature ◽  
Physical Properties ◽  
Heat Treating ◽  
Good Combination ◽  
Resistance To Oxidation ◽  
Cold Worked ◽  
Specialty Steel

Abstract Type 309 (UNS S30900) is an austenitic chromium-nickel stainless steel widely used for elevated-temperature services. It has a good combination of oxidation resistance and corrosion-resisting properties. The alloy is essentially nonmagnetic when annealed and become slightly magnetic when cold worked. It is intended primarily for high-temperature applications at 816 deg C (1500 deg F) or higher where resistance to oxidation and/or corrosion is required. This datasheet provides information on composition, physical properties, hardness, and tensile properties as well as creep. It also includes information on corrosion resistance as well as forming, heat treating, and joining. Filing Code: SS-896. Producer or source: J & L Specialty Steel Inc.

Small-scale plasticity of ultra-fine grained alloy and nanostructured nanocomposite: Ambient and elevated-temperature nanoindentation

2021 ◽  
Vol 807 ◽  
pp. 140873
Author(s):  
F. Khodabakhshi ◽  
A.P. Gerlich ◽  
D. Verma ◽  
M. Nosko ◽  
M. Haghshenas
Keyword(s):  
Elevated Temperature ◽  
Small Scale ◽  
Fine Grained

scholarly journals Submarine lava deltas of the 2018 eruption of Kīlauea volcano

2021 ◽  
Vol 83 (4) ◽  
Author(s):  
S. Adam Soule ◽  
Michael Zoeller ◽  
Carolyn Parcheta
Keyword(s):  
Grain Size ◽  
Pore Pressure ◽  
Mechanistic Model ◽  
Large Fraction ◽  
Volcanic Hazards ◽  
Lava Flows ◽  
Coarse Grained ◽  
Fine Grained ◽  
Fine Grain ◽  
Delta Formation

AbstractHawaiian and other ocean island lava flows that reach the coastline can deposit significant volumes of lava in submarine deltas. The catastrophic collapse of these deltas represents one of the most significant, but least predictable, volcanic hazards at ocean islands. The volume of lava deposited below sea level in delta-forming eruptions and the mechanisms of delta construction and destruction are rarely documented. Here, we report on bathymetric surveys and ROV observations following the Kīlauea 2018 eruption that, along with a comparison to the deltas formed at Pu‘u ‘Ō‘ō over the past decade, provide new insight into delta formation. Bathymetric differencing reveals that the 2018 deltas contain more than half of the total volume of lava erupted. In addition, we find that the 2018 deltas are comprised largely of coarse-grained volcanic breccias and intact lava flows, which contrast with those at Pu‘u ‘Ō‘ō that contain a large fraction of fine-grained hyaloclastite. We attribute this difference to less efficient fragmentation of the 2018 ‘a‘ā flows leading to fragmentation by collapse rather than hydrovolcanic explosion. We suggest a mechanistic model where the characteristic grain size influences the form and stability of the delta with fine grain size deltas (Pu‘u ‘Ō‘ō) experiencing larger landslides with greater run-out supported by increased pore pressure and with coarse grain size deltas (Kīlauea 2018) experiencing smaller landslides that quickly stop as the pore pressure rapidly dissipates. This difference, if validated for other lava deltas, would provide a means to assess potential delta stability in future eruptions.

scholarly journals Mudrock Microstructure: A Technique for Distinguishing between Deep-Water Fine-Grained Sediments

Minerals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 653
Author(s):  
Shereef Bankole ◽  
Dorrik Stow ◽  
Zeinab Smillie ◽  
Jim Buckman ◽  
Helen Lever
Keyword(s):  
Grain Size ◽  
Deep Water ◽  
Sedimentary Facies ◽  
X Ray Diffraction ◽  
Weak Current ◽  
Large Area ◽  
Fine Grained ◽  
Mean Size ◽  
The Mean ◽  
Water Facies

Distinguishing among deep-water sedimentary facies has been a difficult task. This is possibly due to the process continuum in deep water, in which sediments occur in complex associations. The lack of definite sedimentological features among the different facies between hemipelagites and contourites presented a great challenge. In this study, we present detailed mudrock characteristics of the three main deep-water facies based on sedimentological characteristics, laser diffraction granulometry, high-resolution, large area scanning electron microscopy (SEM), and the synchrotron X-ray diffraction technique. Our results show that the deep-water microstructure is mainly process controlled, and that the controlling factor on their grain size is much more complex than previously envisaged. Retarding current velocity, as well as the lower carrying capacity of the current, has an impact on the mean size and sorting for the contourite and turbidite facies, whereas hemipelagite grain size is impacted by the natural heterogeneity of the system caused by bioturbation. Based on the microfabric analysis, there is a disparate pattern observed among the sedimentary facies; turbidites are generally bedding parallel due to strong currents resulting in shear flow, contourites are random to semi-random as they are impacted by a weak current, while hemipelagites are random to oblique since they are impacted by bioturbation.

scholarly journals Strain-Rate and Grain‒Size Effects in Ice

1987 ◽  
Vol 33 (115) ◽  
pp. 274-280 ◽  
Author(s):  
David M. Cole
Keyword(s):  
Grain Size ◽  
Strain Rate ◽  
Transition Point ◽  
Boundary Migration ◽  
Peak Stress ◽  
Strain Rates ◽  
Thin Sections ◽  
Fine Grained ◽  
Lower Strain ◽  
Polycrystalline Ice

AbstractThis paper presents and discusses the results of constant deformation-rate tests on laboratory-prepared polycrystalline ice. Strain-rates ranged from 10−7to 10−1s−1, grain–size ranged from 1.5 to 5.8 mm, and the test temperature was −5°C.At strain-rates between 10−7and 10−3s−1, the stress-strain-rate relationship followed a power law with an exponent ofn= 4.3 calculated without regard to grain-size. However, a reversal in the grain-size effect was observed: below a transition point near 4 × 10−6s−1the peak stress increased with increasing grain-size, while above the transition point the peak stress decreased with increasing grain-size. This latter trend persisted to the highest strain-rates observed. At strain-rates above 10−3s−1the peak stress became independent of strain-rate.The unusual trends exhibited at the lower strain-rates are attributed to the influence of the grain-size on the balance of the operative deformation mechanisms. Dynamic recrystallization appears to intervene in the case of the finer-grained material and serves to lower the peak stress. At comparable strain-rates, however, the large-grained material still experiences internal micro-fracturing, and thin sections reveal extensive deformation in the grain-boundary regions that is quite unlike the appearance of the strain-induced boundary migration characteristic of the fine-grained material.

Hole Expansion by Using Al-Alloy Specimen and 0.45% Carbon Steel Specimen

2010 ◽  
Vol 452-453 ◽  
pp. 601-604
Author(s):  
Muhammed Sohel Rana ◽  
Md. Shafiul Ferdous ◽  
Chobin Makabe ◽  
Masaki Fujikawa
Keyword(s):  
Aluminum Alloy ◽  
Fatigue Life ◽  
Carbon Steel ◽  
Cold Work ◽  
Fatigue Crack Initiation ◽  
Steel Specimen ◽  
Expansion Method ◽  
Al Alloy ◽  
2024 Aluminum Alloy ◽  
Cold Worked

The enhancement method of fatigue life and the crack initiate and growth behavior of a holed specimen was investigated by using the 2024 Aluminum alloy and 0.45% Carbon steel. The purpose of present study is to propose a simple technical method for enhancement of fatigue life in a notched specimen. Also, the effect of local plastic deformation by cold work on fatigue crack initiation behavior was examined. This paper presents a basic experimental kinematic cold expansion method by inserting and removing a pin through the specimen hole. The shape of cross-section of pin was a circle or an ellipse. It was shown that the fatigue life of the specimen with the cold-worked hole was longer than that of the specimen with non-cold-worked hole for the case of same stress level in aluminum alloy and carbon steel. Also, the fatigue strength was higher in the case of the cold expanded hole. In this study, a methodology of lengthening of fatigue life of holed specimen is shown. Also, the improvement conditions of fatigue life were significantly affected by shape of pin, local hardening and residual stress conditions. The fatigue life improvement of the damaged component of structures was studied.

scholarly journals New Brightener for Zn-Fe Alloy Plating from Sulphate Bath

2011 ◽  
Vol 2011 ◽  
pp. 1-8 ◽  
Author(s):  
B. M. Praveen ◽  
T. V. Venkatesha
Keyword(s):  
Grain Size ◽  
Metal Ion ◽  
Condensation Product ◽  
Spectroscopic Studies ◽  
Sem Images ◽  
Alloy Electrodeposition ◽  
Fine Grained ◽  
Polarization Studies ◽  
Uv Visible ◽  
Sulphate Bath

Zn-Fe alloy electrodeposition was carried out in the presence of condensation product 2-{[(1E)-(3,4-dimethoxyphenyl)methylidene]amino}-3-hydroxypropanoic acid formed between veratraldehyde and serine in acid sulphate bath. Hull cell was used for optimizing the operating parameters and bath constituents. During deposition, the potential was shifted towards cathodic direction in the presence of addition agents and brightener. The polarization studies show that deposition taking place in basic bath and optimum bath was 1.08 and 1.15 V, respectively. Current efficiency and throwing power were reached around 85% and 26%, respectively. The SEM images of bright deposit indicated its fine-grained nature and appreciable reduction in the grain size. XRD studies have showed that the grain size of the deposit generated from optimum bath was 16 nm. UV-visible spectroscopic studies confirm the formation of complex between metal ion and brightener.

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