Research on the Technical Conditions on Synthesizing Calcium Zirconate Material

2011 ◽  
Vol 287-290 ◽  
pp. 1765-1770
Author(s):  
Jie Gang You ◽  
Guo Dong Zhang ◽  
Dian Li Qu

The synthesizing CaZrO3are prepared with fused zirconia powder (0.044mm), monoatomic zirconia powder (0.044mm), desilication zirconia powder (0.044mm) and calcium oxide powder (0.044mm). The effect of different moulding pressure and firing temperature on synthesizing CaZrO3has been studied in this paper. The test results show that: The impurity composition SiO2and Al2O3in raw material have participated in reaction, and generated liquid, accelerated transmission quality speed of reaction. Desilication ZrO2is the best ZrO2raw material to synthesizing CaZrO3in above three ZrO2raw materials, firing temperature markedly influence the synthetic rate of CaZrO3, but moulding pressure is not this. Desilication ZrO2and CaO as raw material, firing 1600°C for 3h, pressure at 160Mpa and one stage burning process are the best technical conditions to synthesize CaZrO3.

2019 ◽  
pp. 1-10 ◽  
Author(s):  
Dinda Widu Ramasari ◽  
Evi Liviawaty ◽  
Atikah Nurhayati ◽  
Rusky Intan Pratama ◽  
Eddy Afrianto

Aims: To determine the level of preference of panelists for Nori based on the condition of raw materials of dry and semi-dried Kappaphycus alvarezii (formerly Eucheuma cottonii) seaweed. Study Design: The research was conducted experimentally. Place and Duration of Study: Organoleptic tests were carried out in the Laboratory of Fisheries Product Processing Faculty of Fisheries and Marine Sciences, University of Padjadjaran. Physical tests and chemical tests conducted at the Laboratory of Research and Biological Resources and Biotechnology Research Institute at the Society (LPPM), IPB, between March 2019 and April 2019. Methodology: The research was conducted experimentally consisted of 3 treatments with 20 semi-trained panelists as replication from Fisheries students of Fisheries and Marine Science Faculty, University of Padjadjaran who had experienced the organoleptic assessment. Hedonic tests were to determine the level of panelists preference for the products which included appearance, aroma, texture, and flavor, the results were statistically analyzed using Friedman Test and Bayes Test. Physical tests (thickness and hardness) and chemical tests (water content and crude fiber content) were carried out on the most preferred treatment product and analyzed descriptively. Results: The organoleptic test results of Nori from Kappaphycus alvarezii (formerly Eucheuma cottonii) seaweed with dry raw material conditions had the highest average value on each characteristic compared to other treatments, appearance of 7.70, aroma of 7.00, texture of 7.50, and flavor of 7.90. The Bayes test results on the treatment of Nori from Kappaphycus alvarezii (formerly Eucheuma cottonii) seaweed with dry raw materials conditions having the highest alternative which was 8.54 with the most influential taste criteria for the assessment. The thickness of the Nori was 0.108 mm, the hardness was 1916.16 gf, water content of Nori was 17.23% and crude fiber content was 10.10%. Conclusion: The treatment of Nori with raw materials of dry conditions was the most preferred by panelists.


2016 ◽  
Vol 690 ◽  
pp. 109-113 ◽  
Author(s):  
Sutthima Sriprasertsuk ◽  
Phatthiya Suwannason ◽  
Wanna T. Saengchantara

This work investigated the recycling of fly ash waste and cullet as the raw materials for lightweight bodies produced by heat treatment and using sodium silicate as the binder. Borax was mixed with fly ash and cullet, and put into the block in dimension 10x10x2 cm3. The lightweight materials thus produced were then sintered at temperature of 800 °C. Density, compressive strength and thermal conductivity were determined. Borax showed a positive sintering effect on the porosity of lightweight material during the heat process. The compressive strength of lightweight material diminished with the reduction of density and thermal conductivity. Lightweight material manufactured with borax showed the lower density and thermal conductivity accompanied by the higher compressive strength. The test results indicated that using fly ash and cullet as the raw material with borax could obtain the lightweight material, thus enhancing the possibility of its reuse in a sustainable way.


2016 ◽  
Vol 10 (3) ◽  
pp. 173-180
Author(s):  
Wahyu wahyu Garinas

Penelitian ini merupakan bagian dari kegiatan mencari bahan baku untuk pembuatan isolator keramik porselen. Bahan baku untuk pembuatan benda uji keramik sebagian besar menggunakan bahan baku lokal.Proses pengolahan bahan baku pada penelitian ini  : pembuatan komposisi, pengolahan bahan dan pembuatan benda uji.Metode yang akan dilakukan dalam pengolahan ini  yaitu proses pemisahan dengan cara basah dan kering.Untuk mengetahui kualitas kelistrikan dari bahan baku keramik maka dibuat benda uji dan dilakukan uji tegangan tembus listrik.Hasil uji terhadap benda uji ternyata  semua benda uji masih belum memenuhi standar IEC maupun ASTM. Nilai hasil uji terhadap sampel  sekitar   (7,99 - 9,35) kV/mm dan semua sampel  belum memenuhi  standar yang direkomendasikan oleh PLN (9,85 kV/mm). Hasil uji tersebut menunjukkan bahwa sampel no. 5 dan 6 yang mendekati standar dari PLN. Perlu evaluasi terhadap  komposisi , bahan dan proses pembuatan dari benda uji keramik. Kata Kunci : Bahan mentah keramik (kaolin, felspar, ball clay,kuarsa), pengujian  benda uji, pengujian tegangan tembus, kualitas bahan keramik. Abstract This study is part of the looking for raw materials for the manufacture of ceramic porcelain insulators.The raw material for the manufacture of ceramic test specimens mostly using local raw materials.The processing of the raw material in this study: preparing a composition, materials processing and manufacturing of the test object. The method will be done in this processing is the separation process by means of wet and dry.To know the the quality of the electrical ceramic raw materials then created of the test specimen and test the electrical Puncture Voltage.The test results of the test specimen it turns out all specimens still does not meet PLN (IEC and ASTM) standards.Value test results on samples approximately (7.99 to 9.35) kV / mm and all samples do not meet the standards recommended by PLN.The test results showed that the samples no. 5 and 6 are closer to a standard of PLN.Needs to be evaluation of the composition, materials and manufacturing process of ceramic test specimen. Keywords :  raw material ceramic, specimens test, puncture voltage test, ceramic material quality.


2018 ◽  
Vol 39 (3) ◽  
Author(s):  
Holisoh Holisoh

The utilization of condensate is currently not optimal yet, where most of its production are mixed with crude oil which results in significant shrinkage in oil volume. As a hydrocarbon product, condensate can be utilized as a raw material for petrochemical industry, fuel and solvent. Currently raw materials of petrochemical industry in Indonesia are imported from other countries. To optimize the utilization of condensate it is necessary to conduct a characteristic test of several types of condensate and then conducted a utilization analysis based on their number and its nature. Paraffin, Olefin, Naphthenic and Aromatic (PONA) test results showed that the six samples of condensate in the test had a fairly high paraffin content of above 60%. The highest paraffin content was 82.84% for condensate B and the lowest was 61.4% for condensate E. The six condensate samples contain higher paraffin, which are suitable for use as raw material for petrochemical olefin.The results of the economic calculation of the construction unit Olefin Process Center with a capacity of 100,000 BPSD, which is an IRR as 22.8 %, the NPV as of US $ 1,801,491,951.12 , POT for 4.1 years, and PI as 1.87. Developing of Olefin Process Unit Center being constructed in Indonesia is economical worthy.


2020 ◽  
Vol 9 (1) ◽  
pp. 13-25
Author(s):  
Trisa Mushandry Pratiwi ◽  
Hardiani Hardiani ◽  
Adi Bhakti

The purpose of this study is (1) To analyze the socioeconomic characteristics of Producers in the Shrimp Crackers Home Industry in the Village of Lambur Luar Tanjung Jabung Timur Regency, (2) To analyze the effect of capital, labor, prices and raw materials on production in the Home Industry Shrimp Crackers in Lambur Luar Village, Tanjung Jabung Timur Regency. The results showed that all independent variables (capital, labor, prices and raw materials) affected the production of the shrimp cracker industry in Lambur Luar Village. Judging from the test results obtained by the coefficient of determination ( ) of 0.963460. This is aimed at capital, labor, prices and raw materials able to influence production by 96.34 percent and the remaining 3.66 percent for other variables not included in this study. Whereas if tested partially, capital, labor, price and raw material variables have a positive and significant effect on production in the shrimp cracker industry in Lambur Luar Village.


2015 ◽  
Vol 9 (3) ◽  
pp. 157-166
Author(s):  
Wahyu Garinas

Ball clay quality are derived from within the country is very variety and generally rather difficult to get raw materials as needed. This research used ball clay from the West Kalimantan and West Java area.Ball clay is one of the most important raw materials for the manufacture of fine ceramic. To get the ball clay raw materials in accordance with the standards it is necessary to processing of raw materials. Processing of ball clay in this research conducted by precipitation and filtration magnet. Testing of ball clay raw materials are : test chemical composition by wet methods (SNI. 15-0449-1989) and grain size of raw material (SNI.15-0578-1996). Ball clay that has been processed will be tested with the same method of SNI. Test results before and processed will be compared with a standard of quality ball clay(SNI, NGK, India) for fine ceramic materials. The test results of chemical composition and grain size ball clay raw material showed that samples from west kalimantan qualified for fine ceramic materials and samples from other areas did not meet the standards (SNI, NGK, India). ABSTRAKMutu ballclay yang terdapat di dalam negeri sangat beragam dan umumnya agak sulit mendapatkan bahan baku yang sesuai dengan kebutuhan. Pada penelitian ini digunakan ball clay yang berasal dari daerah Kalimantan Barat, Jawa Barat dan Jawa Timur. Ball clay merupakan salah satu bahan baku penting untuk pembuatan keramik halus. Untuk mendapatkan bahan baku ball clay sesuai dengan standar maka perlu dilakukan pengolahan bahan baku. Pengolahan ball clay dalam penelitian ini dilakukan dengan cara pengendapan dan penyaringan magnet. Pengujian terhadap bahan mentah ball clay meliputi : uji komposisi kimia dengan metode basah (SNI. 15-0449-1989) dan pengujian besar butir (SNI.15-0578-1996). Ball clay yang sudah diolah nantinya akan diuji dengan metode SNI yang sama. Hasil uji sebelum dan terolah akan dibandingkan dengan standar mutu ball clay untuk bahan keramik halus. Hasil uji dari komposisi kimia dan besar butir ball clay bahan mentah menunjukan bahwa sampel dari Kalbar memenuhi syarat untuk bahan keramik halus dan sampel dari daerah lainnya ternyata tidak memenuhi standar (SNI, NGK. India).


MRS Advances ◽  
2017 ◽  
Vol 2 (35-36) ◽  
pp. 1889-1909
Author(s):  
Catherine Klesner ◽  
Jay A. Stephens ◽  
Emilio Rodriguez-Alvarez ◽  
Pamela B. Vandiver

ABSTRACTDecorative, polychrome ceramics from Corinth, Greece, produced during the 8th-6th centuries B.C.E. were luxury goods widely traded throughout Greece and the Mediterranean. Corinthian pottery is the first 5-color polychrome ceramic technology, having slip-glazes in distinctive white, black, red, yellow, and purple colors, and in a variety of surface finishes from glossy, to semi-matte, to matte. The firing temperature range, 925-1075°C, was determined experimentally to be to be higher than previously reported, similar to the Corinthian amphorae and other ceramic products. This firing range is higher than that of the better known, more prestigious Athenian Black-figure and Red-figure ceramics. In this study three examples of Corinthian and one example of Athenian Black-figure ceramics from the Marie Farnsworth collection at the University of Arizona were tested and compared to thirteen clays from Corinth. Analytical techniques included Fourier-transform infrared spectroscopy (FTIR), scanning-electron microscopy with energy-dispersive spectroscopy (SEM-EDS), micro-Raman spectroscopy, and wavelength-dispersive electron microprobe (EPMA with BSE-SEM).Artisans in Corinthian workshops experimented to change the colors of the slips by varying the type and amount of iron-rich raw material, as well as the composition of the clay used as a binder and the amount of flux used as a sintering aid to promote glass formation. Corinthian artisans developed not only different recipes to produce the various colors, but also they were able to control raw-material particle size and composition to produce variations in surface luster (matte, semi-matte and glossy). This research suggests that Corinthian polychrome-slip technology was based on careful control of particle processing, of compositional control of raw materials and their admixtures, and of firing temperature. The behavior or practice of adding different ratios of pigments and glass-forming fluxes to form various optical effects implies a detailed knowledge of what happens when these are heated and fired. This is a process of experimentation focused on developing a distinctive craft practice, which produced a distinctive and highly valued material. The Corinthians developed a more complex, easily recognizable, and culturally distinctive ceramic technology that was intentionally established as a cultural brand, and probably as a luxury brand of high socio-economic value. This research deepens our understanding of the complex pigment processing and firing technologies employed in the production of Corinthian ceramics.


2021 ◽  
Vol 1 (1) ◽  
pp. 31-41
Author(s):  
Nurlita Utami ◽  
Sena Atmaja ◽  
Yogi Priyo Istiyono

Thermo Plastic Acrylic resin has an important role in the manufacture of spray paint, namely as a binder or binder. The resin in paint has a function as a film formation, has adhesion to the substrate as well as pigment binders and additives, so that to produce a spray paint with good quality mechanical properties, PT X must be selective in controlling the quality of the raw material for Thermo Plasic Acrylic Resin. The purpose of this study was to determine the problems faced by PT X related to the quality of Thermo Plastic Acrylic Resin raw materials, to identify the most dominant factors affecting the quality of these raw materials and to formulate the most appropriate solutions to be applied in improving the quality of these raw materials. This research uses observation, interview, and literature study methods. Sources of data came from stakeholders and quality control staff of PT X. This study used check sheets, histogram diagrams, u-control maps, and fishbone diagrams to complete the analysis process. From the test results of the Thermoplastic Acrylic Resin raw material, it is known that the factor that causes rejection is due to adhesion, namely 53.57%, gloss 33.33%, and dry touch 13.10%, all three of the total raw materials that are rejected when the raw material is applied in form paint and spray on the film plate. The most dominant cause of reject was poor adhesion, namely 53.57% of the total reject raw materials.


2020 ◽  
Vol 3 (3) ◽  
pp. 40-46 ◽  
Author(s):  
V. Men'shikova ◽  
L. Demina

the paper raises questions about the search for the possibility of obtaining a construction ceramic material using a special type of raw material component. Diopside concentrate was chosen as the basis for the ceram-ic masses due to its positive parameters necessary to improve the strength properties of the material and to support local deposits of raw materials in the East Siberian region. To reduce the optimal firing temperature, an aqueous-alkaline solution of sodium silicate was used in small quantities. The chemical composition of the diopside rock showed mainly the presence of silicon oxides. X-ray diffraction analysis revealed the presence of diopside, quartz and calcite. Sodium-silicate glass is characterized by a full content of silica and a modulus of 3. Using the state diagram of three-component systems, the temperature limits necessary for sintering ceramic masses are established. The fusibility curves show that at a temperature of 1040oC, the values of the primary melt for various compositions are 4-14%, and the total melt content is observed at 1475oC. The parameters of physical and mechanical properties of the ceramic material were determined, where at the firing temperature of 1000-1100oC the value of fire shrinkage was no more than 1%, water ab-sorption up to 10%, and compressive strength up to 31 MPa. Moreover, with an increase in the amount of diopside to 90% by weight, the strength increases, and shrinkage decreases. X-ray phase analysis of the compositions determined mainly analytical lines of diopside, which begin to decrease by 1000oC, which de-termines the relationship with the liquid glass. The DTA and TG curves of the thermogram showed endo-thermic and exothermic effects due to the release of adsorbed water and crystallization of glass. The possi-bility of obtaining high-strength low-shrink ceramics using diopside raw materials as the basis of ceramic masses when adding sodium-silicate glass in the form of a melt is established.


2013 ◽  
Vol 14 (1) ◽  
pp. 109-114 ◽  
Author(s):  
Ramesh Man Singh ◽  
Mridaney Sharma Poudel

Mikania micrantha (mile- a-minute in English) is assessed as one of the six high risks posed IAS in terrestrial ecosystem in Nepal and is as a considered second biggest threat after deforestation to biodiversity conservation. It is becoming pervasive and estimated to have covered over 20% of the Chitwan National Park. A survey was conducted jointly with NTNC, TCN and NAST to establish the estimates of available Mikania biomass raw material. After being cut, it can even regenerate by old rootstocks, runners and suckers. It does not have much use after manual removal. So, using dried biomass for briquetting to get fuel may be an option for its utilization. Different types of briquettes using biomass as well as char were made from its raw materials. Various physical and fuel characteristics of the briquette fuels and combustion tests were performed and studied as an alternative fuel. Different test results show that the use of this weed to produce briquette fuel will generate a potential source of alternative energy and will also help in conserving biodiversity in long run. Nepal Journal of Science and Technology Vol. 14, No. 1 (2013) 109-114 DOI: http://dx.doi.org/10.3126/njst.v14i1.8930


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