Rheological Characteristics of Residue Binder from Low Penetration Grade Bitumen Emulsion

2012 ◽  
Vol 509 ◽  
pp. 328-332 ◽  
Author(s):  
Guang Ji Xu ◽  
Mei Zhu Chen ◽  
Shao Peng Wu ◽  
Martin Van de Ven ◽  
Steven Mookhoek
Keyword(s):  
Phase Angle ◽  
Large Range ◽  
Complex Modulus ◽  
Rheological Characteristics ◽  
Curing Process ◽  
Master Curves ◽  
Recovery Method ◽  
Stabilization Process ◽  
Bitumen Emulsion ◽  
Three Stages

In this study, residue binders from low penetration grade bitumen emulsions were investigated on the basis of rheology and were compared to the neat bitumen binders of which they were produced. The recovery method proposed by EN 13074 (including both recovery and stabilization process at moderate temperatures) was selected to obtain the residue binders used in the analysis, and the corresponding neat binders were treated the same for comparison. The rheological properties of residue binder from low penetration grade bitumen emulsion were evaluated using Dynamic Shear Rheometer (DSR). During the curing process, three stages were divided, and master curves of complex modulus and phase angle were constructed to allow comparison of the residue binder over a large range of frequencies for each stage. The results showed that the complex modulus increases while the phase angle decreases with curing process for the residues, indicating a better performance in terms of elasticity and stiffness.

scholarly journals Influence of Different Modifiers on Bonding Strength and Rheological Performance of Bitumen Emulsion

Materials ◽  
2019 ◽  
Vol 12 (15) ◽  
pp. 2414 ◽  
Author(s):  
Changluan Pan ◽  
Deqiang Liang ◽  
Liantong Mo ◽  
Martin Riara ◽  
Juntao Lin
Keyword(s):  
Phase Angle ◽  
Bonding Strength ◽  
Complex Modulus ◽  
Low Frequency ◽  
Epoxy Adhesive ◽  
Styrene Butadiene Rubber ◽  
Butadiene Rubber ◽  
Modified Bitumen ◽  
Bitumen Emulsion ◽  
Rheological Performance

Styrene butadiene rubber latex (SBR), waterborne epoxy adhesive (WE) and colloidal silica sol (SiO2) were used to prepare modified bitumen emulsion for cold mix asphalt. The modification effects of the individual modifiers and the combination of these modifiers were investigated by using bonding strength and dynamic shear rheological property. Test results showed that the modifier dosage helped to balance the performance of modified bitumen emulsion by improving its bonding strength without compromising its rheological properties. The critical dosage at which the peak bonding strength occurred was 4%, 12% and 4% for SBR, WE and SiO2 respectively. Improved rheological performance on the master curves was well distinguished, in particular, by increased complex modulus and reduced phase angle at the low frequency region. Abrupt changes, especially on phase angle occurred when the modifier dosage was beyond 12%. The measured ratio between bonding strength and complex shear modulus could vary ranging from 10−2 to 102. Highly-modified bitumen emulsion with good adhesion, rheology and compatibility can be prepared by using the combination of SBR, WE and SiO2. It is important to carefully select the type and dosage of modifier for a particular combination to optimize the performance of modified bitumen emulsion.

Investigation of Ultraviolet Ageing on Rheological Characteristics of Bitumen

2011 ◽  
Vol 71-78 ◽  
pp. 1954-1957
Author(s):  
Jian Ying Yu ◽  
Yong Sheng Liang ◽  
Zhen Gang Feng
Keyword(s):  
Low Temperature ◽  
Phase Angle ◽  
Low Temperatures ◽  
Complex Modulus ◽  
Rheological Parameters ◽  
Rheological Characteristics ◽  
Dynamic Shear ◽  
Dynamic Shear Rheometer ◽  
Uv Ageing ◽  
Rheometer Test

The influence of ultraviolet (UV) ageing on complex modulus, phase angle and low-temperature fatigue factor was studied by dynamic shear rheometer test. The ageing degree of the bitumen was evaluated by the rheological parameters. The results show that UV ageing causes an increase in complex modulus and fatigue factor, as well as a decrease in phase angle, indicating that the bitumen becomes more elastic after UV ageing process and is apt to crack at low temperatures. Different bitumen exhibits diverse changes in the rheological parameters after UV ageing, which is much dependent on the sources of bitumen.

Phase angle master curves of sulfur-extended asphalt modified with recycled polyethylene waste

2021 ◽  
Vol 6 (2) ◽  
Author(s):  
Yasser M. Alghrafy ◽  
El-Sayed M. Abd Alla ◽  
Sherif M. El-Badawy
Keyword(s):  
Phase Angle ◽  
Master Curves ◽  
Recycled Polyethylene

Dynamic Viscoelastic Properties of SBS Modified Asphalt Based on DSR Testing

2012 ◽  
Vol 598 ◽  
pp. 473-476 ◽  
Author(s):  
Yong Mei Guo ◽  
Wei Chen
Keyword(s):  
Complex Modulus ◽  
Superposition Principle ◽  
Asphalt Binder ◽  
Asphalt Binders ◽  
Frequency Range ◽  
Master Curves ◽  
Temperature Property ◽  
Low Frequencies ◽  
High Temperature Property ◽  
Frequency Sweeps

Five SBS modified asphalts and one base asphalt were selected to carry out frequency sweeps over a wider frequency range using the dynamic shear rheometer (DSR). Six asphalt binders were subjected to sinusoidal loading at 30°C-90°C within the linear viscoelastic limits, and master curves of complex modulus (G*) and phase angle (δ) could be constructed by means of the time-temperature superposition principle (TTSP). The results show that the G* values of SBS modified asphalts are significantly greater than those of base asphalt at low frequencies, but are slightly smaller at high frequencies. Compared with the base asphalt, SBS modified asphalts have narrower master curves of complex modulus, and their phase angles are much smaller within the whole frequency range. This indicates that various properties of SBS modified asphalts, such as high-temperature property, low-temperature property, temperature susceptibility and elastic recoverability, are superior to those of the base asphalt. The G* values of the rolling thin-film oven (RTFO) aged asphalt are larger than those of the unaged asphalt in the whole range of frequencies, demonstrating that the anti-rutting performance of asphalt binder is improved after short-term aging.

A procedure for characterizing the curing process of cold recycled bitumen emulsion mixtures

2018 ◽  
Vol 173 ◽  
pp. 754-762 ◽  
Author(s):  
Andrea Graziani ◽  
Christian Iafelice ◽  
Simone Raschia ◽  
Daniel Perraton ◽  
Alan Carter
Keyword(s):  
Curing Process ◽  
Bitumen Emulsion

scholarly journals Predict the Phase Angle Master Curve and Study the Viscoelastic Properties of Warm Mix Crumb Rubber-Modified Asphalt Mixture

Materials ◽  
2020 ◽  
Vol 13 (21) ◽  
pp. 5051
Author(s):  
Fei Zhang ◽  
Lan Wang ◽  
Chao Li ◽  
Yongming Xing
Keyword(s):  
Phase Angle ◽  
Dynamic Modulus ◽  
Master Curve ◽  
Loss Modulus ◽  
Asphalt Mixture ◽  
Crumb Rubber ◽  
Asphalt Mixtures ◽  
Master Curves ◽  
Modified Asphalt ◽  
Sigmoidal Model

To identify the most accurate approach for constructing of the dynamic modulus master curves for warm mix crumb rubber modified asphalt mixtures and assess the feasibility of predicting the phase angle master curves from the dynamic modulus ones. The SM (Sigmoidal model) and GSM (generalized sigmoidal model) were utilized to construct the dynamic modulus master curve, respectively. Subsequently, the master curve of phase angle could be predicted from the master curve of dynamic modulus in term of the K-K (Kramers–Kronig) relations. The results show that both SM and GSM can predict the dynamic modulus very well, except that the GSM shows a slightly higher correlation coefficient than SM. Therefore, it is recommended to construct the dynamic modulus master curve using GSM and obtain the corresponding phase angle master curve in term of the K-K relations. The Black space diagram and Wicket diagram were utilized to verify the predictions were consistent with the LVE (linear viscoelastic) theory. Then the master curve of storage modulus and loss modulus were also obtained. Finally, the creep compliance and relaxation modulus can be used to represent the creep and relaxation properties of warm-mix crumb rubber-modified asphalt mixtures.

scholarly journals Evaluation of the Rheological Property of Binder-Filler Systems after Oxidation Based on a Simple Film Oven Aging Method

2019 ◽  
Vol 9 (12) ◽  
pp. 2542
Author(s):  
Hongmei Li ◽  
Jiwang Jiang ◽  
Song Li ◽  
Xiang Ma
Keyword(s):  
Rheological Property ◽  
Complex Modulus ◽  
Aging Effect ◽  
Test Results ◽  
Master Curves ◽  
Oxidative Aging ◽  
Aging Index ◽  
Frequency Sweep Test ◽  
Simple Film ◽  
Mineral Aggregates

Asphalt mastic is a combination of binder and filler. The binder-filler system within asphalt mixtures plays an important role in adhesion between mineral aggregates. The aging of binders in pavement always happens with fillers inside or contact with mineral aggregates, so it is critical to investigate the evolved rheological property of binder-filler systems during oxidative aging. In this study, simple film oven aging methods for the aging of mastics (binder-filler system) were conducted and verified by comparing the master-curves of aged mastics at different oven positions or different aging times. The frequency sweep test was performed to measure the changing stiffness of mastics with a different combination of binders and filler contents. Test results show that oven positions could influence the aging effect of the mastics significantly, given the influence of circulation. With increasing aging times, the complex modulus increases while phase angle decreases. Comparing the mastics which were first aged then mixed with mastics which were first mixed then aged, it was observed that fillers inside the binder could accelerate aging of the mastics. Additionally, the aging index of mastics with different combinations showed that both the modification of binders and filler contents could affect the aging rate of the mastics.

scholarly journals Characteristics of the complex modulus of recycled cold mix with foamed bitumen and recycled concrete aggregate

2019 ◽  
Vol 262 ◽  
pp. 05002 ◽  
Author(s):  
Przemysław Buczyński ◽  
Marek Iwański
Keyword(s):  
Phase Angle ◽  
Complex Modulus ◽  
Asphalt Pavement ◽  
Recycled Concrete ◽  
Time Range ◽  
Concrete Aggregate ◽  
Reclaimed Asphalt Pavement ◽  
Recycled Concrete Aggregate ◽  
Reclaimed Asphalt ◽  
Foamed Bitumen

This article presents research on recycled cold mix with foamed bitumen (MCAS) containing recycled concrete aggregate. The primary concept driving this research was to determine if recycled concrete aggregate (RC) could be used as a substitute for reclaimed asphalt pavement (RAP). Recycled concrete aggregate was used in the MCAS mix in amounts ranging from 20%, 60% and 80%. The reference mix was the MCAS mix containing 50% reclaimed asphalt pavement (RAP) and virgin aggregate. Identical 0/31.5-mm continuously graded dolomite virgin aggregate was used in all mixes. 2.5% foamed bitumen (FB) and 2.0% CEM I 42.5R Portland cement (PC) were used to increase the cohesion of the mineral mix. Foamed bitumen was produced from 50/70 penetration paving bitumen. The behaviour of the recycled base course was tested in the range of cyclic sinusoidal strain with amplitude εo = 25–50 με. The tests were carried out in the (-7°C, 5°C, 13°C, 25°C, 40°C) temperature and (0.1 Hz, 0.3 Hz, 1 Hz, 3 Hz, 10 Hz, 20 Hz) loading time range. The complex modulus was tested in a direct tension-compression test on cylindrical samples (DTC-CY) in accordance with EN 12697-26. The results of the tests were used to assess the complex modulus (E*), phase angle (φ) and complex modulus components (E1) and (E2).Tests of the mixes indicate that recycled concrete aggregate can be used in recycled cold mixes in amounts of up to 80%. Increasing the amount of recycled concrete aggregate does not cause excessive stiffness of the recycled mix in comparison with the reference mix. The tests did not demonstrate a significant difference in terms of the phase angle (φ), which indicates a similar content of the viscous part and elastic part in the obtained complex modulus for the reference mix (RAP + MCAS) and the mix containing recycled concrete aggregate (RC + MCAS).

Effect of Temperature on Phase Angle and Dynamic Modulus of Asphalt Mixtures Using SPT

2020 ◽  
Vol 1007 ◽  
pp. 99-104
Author(s):  
Juraidah Ahmad ◽  
Mohd Rosli Hainin ◽  
Ekarizan Shaffie ◽  
Khairil Azman Masri ◽  
Mohd Amin Shaffi
Keyword(s):  
Phase Angle ◽  
Dynamic Modulus ◽  
Performance Test ◽  
Complex Modulus ◽  
Asphalt Binder ◽  
Asphalt Mixture ◽  
Load Resistance ◽  
Asphalt Mixtures ◽  
Effect Of Temperature ◽  
Low Viscosity

The Simple Performance Test (SPT) can be used to characterize the strength and load resistance of asphalt mixtures. The objectives of this study are to determine the effect of temperature on the phase angle and dynamic complex modulus of the asphalt mixtures tested at 30°C, 35°C, 40°C, 45°C and 50°C at 25Hz, 20Hz, 10Hz, 5Hz, 1Hz and 0.5Hz frequencies. The asphalt mixtures of NMAS 12.5mm are prepared using asphalt binder PEN 80/100 and PEN 60/70. The asphalt mixtures are designed using the Superpave system and compacted using the Superpave Gyratory Compactor (SGC). The dynamic modulus test results showed that at a higher temperature, the stiffness of the asphalt mixtures is affected. The dynamic modulus of the mixtures is highest at 30°C and gradually decrease at 35°C, 40°C, 45°C and 50°C respectively. The dynamic modulus values for asphalt mixtures with bitumen grade PEN 60/70 are also higher compared to the asphalt mixtures with bitumen grade PEN 80/100. Results also showed that the low phase angle values indicate low viscosity of the asphalt binder due to increase in temperature. The present study is meaningful in understanding the asphalt mixture behaviour at different temperature and loading frequencies.

Sign in / Sign up

Export Citation Format

Share Document