Characteristics of Powder-Rolled and Sintered Sheets Made from HDH Ti Powders

2012 ◽  
Vol 520 ◽  
pp. 281-288 ◽  
Author(s):  
Nho Kwang Park ◽  
C.H. Lee ◽  
Jeoung Han Kim ◽  
Jae Keun Hong

In this study, direct powder rolling was applied to make thin sheets from HDH (hydrogenation and dehydrogenation) powders. Effects of materials and process parameters on tensile properties of sintered sheets are investigated. In the direct powder rolling with two-horizontal counter-rotating rollers, materials parameters including powder size and process parameters such as roll gap, roll speed, and packing height are controlled. With -100mesh Ti powders, CP titanium sheets of a thickness up to 1.5mm and a width up to 300mm were obtained without any rolling defects. Sintering of the rolled strips was performed between 1000°C and 1250°C at 50°C intervals for 1hour to 4 hours. The relative density of the sintered strips was found to be around 85 to 90 percent. After sintering, the complete densification was made by cold rolling, and microstructures and tensile properties were evaluated after annealing treatment at 750°C for 2 hours.

2007 ◽  
Vol 26-28 ◽  
pp. 367-371
Author(s):  
Hong Zhen Guo ◽  
Zhang Long Zhao ◽  
Bin Wang ◽  
Ze Kun Yao ◽  
Ying Ying Liu

In this paper the effect of isothermal forging process parameters on the microstructure and the mechanical properties of TA15 titanium alloy was researched. The results of the tests indicate that, in the range of temperature of 850 °C~980 °C and deformation degree of 20%~60%, with the increase of temperature or deformation, as the reinforcement of deformation recrystallization, the primary α-phase tends to the spherical shape and secondary α-phase transforms from the acicular shape to fine and spherical shape with disperse distribution, which enhance the tensile properties at room and high temperature. With the increment of forging times, the spheroidization of primary α-phase aggrandizes and secondary α-phase transforms from spherical and acicular shape to wide strip shape, which decrease the tensile properties at room and high temperature. The preferable isothermal forging process parameters are temperature of 980 °C, deformation degree of 60%, and few forging times.


Materials ◽  
2019 ◽  
Vol 12 (6) ◽  
pp. 930 ◽  
Author(s):  
Martin Malý ◽  
Christian Höller ◽  
Mateusz Skalon ◽  
Benjamin Meier ◽  
Daniel Koutný ◽  
...  

The aim of this study is to observe the effect of process parameters on residual stresses and relative density of Ti6Al4V samples produced by Selective Laser Melting. The investigated parameters were hatch laser power, hatch laser velocity, border laser velocity, high-temperature preheating and time delay. Residual stresses were evaluated by the bridge curvature method and relative density by the optical method. The effect of the observed process parameters was estimated by the design of experiment and surface response methods. It was found that for an effective residual stress reduction, the high preheating temperature was the most significant parameter. High preheating temperature also increased the relative density but caused changes in the chemical composition of Ti6Al4V unmelted powder. Chemical analysis proved that after one build job with high preheating temperature, oxygen and hydrogen content exceeded the ASTM B348 limits for Grade 5 titanium.


2014 ◽  
Vol 59 (4) ◽  
pp. 1533-1538
Author(s):  
A. Kawałek ◽  
H. Dyja ◽  
M. Knapinski ◽  
G. Banaszek ◽  
M. Kwapisz

Abstract In order to enhance the quality of plates, various solutions are being implemented, including normalizing rolling, the process of rolling followed by accelerated cooling, as well as new roll gap control systems. The hydraulic positioning of rolls and the working roll bending system can be mentioned here. The implementation of those systems results in increased loads of the rolling stands and working tools, that is the rolls. Another solution aimed at enhancing the cross-sectional and longitudinal shape of rolled plate is the introduction of asymmetric rolling, which consists in the intentional change of the stress and strain state in the roll gap. Asymmetric rolling systems have been successfully implemented in strip cold rolling mills, as well as in sheet hot rolling mills. The paper present results of studies on the effect of roll rotational speed asymmetry and other rolling process parameters on the change in the shape of rolled strip and the change of rolls separating force for the conditions of normalizing rolling of plates in the finishing stand. The variable process parameters were: the roll rotational speed asymmetry factor, av; the strip shape factor, h0/D; and the relative rolling reduction, ε. Working rolls of the diameter equal to 1000 mm and a constant lower working roll rotational speed of n = 50 rpm were assumed for the tests. The asymmetric rolling process was run by varying the rotational speed of the upper roll, which was lower than that of the lower roll. The range of variation of the roll rotational speed factor, av =vd/vg, was 1.01÷1.15. A strip shape factor of h0/D = 0.05÷0.014 was assumed. The range of rolling reductions applied was ε = 0.08÷0.50. The material used for tests was steel of the S355J2G3 grade. For the simulation of the three-dimensional plastic flow of metal in the roll gap during the asymmetric hot rolling of plates, the mathematical model of the FORGE 2008 ® program was used. For the mathematical description of the effect of rolling parameters on the strip curvature and rolls separating force the special multivariable polynomial interpolation was used. This method of tensor interpolation in Borland Builder programming environment was implemented. On the basis of the carried out analysis can be state, that by using the appropriate relative rolling reduction and working roll peripheral speed asymmetry factor for a given feedstock thickness (strip shape ratio) it is possible to completely eliminate the unfavorable phenomenon of strip bending on exit from the roll gap, or to obtain the permissible strip curvature which does not obstructs the free feed of the strip to the next pass or transferring the plate to the accelerated plate cooling stations. Additionally by introducing the asymmetric plate rolling process through differentiating working roll peripheral speeds, depending on the asymmetry factor used, the magnitude of the total roll separating force can be reduced and, at the same time, a smaller elastic deflection of rolling stand elements can be achieved. As a result smaller elastic deflection of the working rolls, smaller dimensional deviations across its width and length finished plate can be obtained.


2010 ◽  
Vol 17 (02) ◽  
pp. 229-234 ◽  
Author(s):  
JAE-KEUN HONG ◽  
CHAE-HUN LEE ◽  
JEOUNG-HAN KIM ◽  
JONG-TAEK YEOM ◽  
NHO-KWANG PARK

In the present study, the characteristics of the Ti powders fabricated by Hydride–Dehydride (HDH) were analyzed in terms of particle shape, size and size distribution. Ti powders were subjected to roll compaction and their microstructure and green densities were evaluated in terms of particle size, powder morphology, roll gap and rolling speed. Effects of blending elements having different powder sizes on densification properties were analyzed. The strip thickness was proportional to the roll gap up to 0.9 mm and the density of titanium strip was decreased with the increase in roll gap. As the roll speed increased, the strip density and thickness were decreased by using -200 mesh Ti powder. However, the effect of rolling speed for -400 mesh Ti powder was not greater than that of -200 mesh powder. The highest density by 93% was achieved by using -400 mesh Ti powder at 0.1 mm roll gap, however edge cracks and alligator cracks were occurred.


Metals ◽  
2018 ◽  
Vol 8 (2) ◽  
pp. 109 ◽  
Author(s):  
Antti Järvenpää ◽  
Matias Jaskari ◽  
Leo Karjalainen

Materials ◽  
2021 ◽  
Vol 14 (20) ◽  
pp. 5975
Author(s):  
Jae-Hwan Kim ◽  
Jong-Min Jung ◽  
Hyunbo Shim

The tensile properties and damping capacity of cold-rolled Fe–20Mn–12Cr–3Ni–3Si alloys were investigated. The martensitic transformation was identified, including surface relief with a specific orientation and partial intersection. Besides, as the cold rolling degree increased, the volume fraction of ε-martensite increased, whereas α’-martensite started to form at the cold rolling degree of 15% and slightly increased to 6% at the maximum cold rolling degree. This difference may be caused by high austenite stability by adding alloying elements (Mn and Ni). As the cold rolling degree increased, the tensile strength linearly increased, and the elongation decreased due to the fractional increment in the volume of martensite. However, the damping capacity increased until a 30% cold rolling degree was approached, and then decreased. The irregular tendency of the damping capacity was confirmed, depicting that it increased to a specific degree and then decreased as the tensile strength and elongation increased. Concerning the relationship between the tensile properties and the damping capacity, the damping capacity increased and culminated, and then decreased as the tensile properties and elongation increased. The damping capacity in the high-strength area tended to decrease because it is difficult to dissipate vibration energy into thermal energy in alloys with high strength. In the low-strength area, on the other hand, the damping capacity increased as the strength increased since the increased volume fraction of ε-martensite is attributed to the increase in the damping source.


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