Mechanical and Corrosion Behavior of TiN Coatings Deposited on Nitrided AISI 420 Stainless Steel

2019 ◽  
Vol 813 ◽  
pp. 135-140
Author(s):  
Eugenia Laura Dalibon ◽  
Amado Cabo ◽  
Jorge Halabi ◽  
Ramiro D. Moreira ◽  
Kevin Silva ◽  
...  
Keyword(s):  
Stainless Steel ◽  
Wear Resistance ◽  
Corrosion Behavior ◽  
Nitrided Layer ◽  
Salt Spray ◽  
High Hardness ◽  
Wear Loss ◽  
Tin Coating ◽  
Tin Coatings ◽  
Pin On Disk

TiN coatings are widely used in different applications for extending the lifetime of components due to their high hardness and good wear resistance. However, it is not convenient to deposit them on soft stainless steels. In this work, the wear and corrosion behavior of commercial TiN coatings deposited by Arc-PVD on nitrided and non-nitrided martensitic stainless steel was studied. Two different nitriding conditions were used, one at high temperature (HTN) and the other at low temperature (LTN). Nanohardness and microhardness were measured. The microstructure was characterized by OM, SEM, XRD and XPS. Pin on disk and erosion tests were carried out in order to evaluate their wear resistance. The corrosion behavior was analyzed in salt spray fog and electrochemical tests in NaCl solution and the adhesion was measured in Scratch and Rockwell C Indentation tests.The coating thickness was about 1.5 µm and its hardness of 34 GPa. The nitrided layers were 13 µm and 17 µm thick for LTN and HTN, the hardness was approximately 12 GPa for both nitrided samples. The nitrided layer improved TiN coating adhesion in the Scratch tests. The wear loss volume was similar for both duplex and only coated samples in pin on disk tests. Nevertheless, wear resistance was not good for the LTN or HTN + TiN coating system in the erosion tests. Regarding corrosion behavior, the coatings showed poor corrosion resistance and this could be related to the presence of porous defects, which allow the solution to reach and attack the substrate, thus producing coating detachment around the pits.

Erosion Wear Resistance of TiAlCrN Coating on Stainless Steel Impacted by Solid Particles

2011 ◽  
Vol 675-677 ◽  
pp. 1271-1274
Author(s):  
Feng Fang Wu ◽  
Jian Xin Deng
Keyword(s):  
Stainless Steel ◽  
Wear Resistance ◽  
Average Diameter ◽  
Scratch Test ◽  
Solid Particles ◽  
Vacuum Arc ◽  
Wear Loss ◽  
Erosion Wear ◽  
Tin Coating ◽  
Unbalanced Magnetron

TiAlCrN coating was deposited on a stainless steel using unbalanced magnetron sputtering technique. The erosion wear resistance of the TiAlCrN coating was investigated by comparison with that of the TiN coating deposited by filtered vacuum arc deposition. SEM was used for observing the surface morphologies of coatings both the un-eroded and eroded. Scratch test was used to evaluate the adhesion of the coatings. The erosion wear was tested with a gas blast apparatus at room temperature. In the test, the coatings were impacted at an impingement angle of 90° by angular SiC solid particles with an average diameter of 124um. The maximum depth of the erosion scar measured by the optical profiler was used to evaluate the erosion wear loss of the coatings. TiAlCrN coating proved to have much lower erosion rate than TiN coating. Unlike TiN coating, the TiAlCrN coating behaved like semi-brittle material.

scholarly journals Effect of Rare Earth Oxides on Microstructure and Corrosion Behavior of Laser-Cladding Coating on 316L Stainless Steel

Coatings ◽  
2019 ◽  
Vol 9 (10) ◽  
pp. 636 ◽  
Author(s):  
Xu ◽  
Wang ◽  
Chen ◽  
Qiao ◽  
Zhang ◽  
...  
Keyword(s):  
Stainless Steel ◽  
Rare Earth ◽  
Corrosion Behavior ◽  
Laser Cladding ◽  
316L Stainless Steel ◽  
Electrochemical Impedance ◽  
Salt Spray ◽  
Rare Earth Oxides ◽  
X Ray Diffraction ◽  
X Ray

The effect of rare earth oxides on the microstructure and corrosion behavior of laser-cladding coating on 316L stainless steel was investigated using hardness measurements, a polarization curve, electrochemical impedance spectroscopy (EIS), a salt spray test, X-ray diffraction, optical microscopy, and scanning electron microscopy (SEM). The results showed that the modification of rare earth oxides on the laser-cladding layer caused minor changes to its composition but refined the grains, leading to an increase in hardness. Electrochemical and salt spray studies indicated that the corrosion resistance of the 316L stainless steel could be improved by laser cladding, especially when rare earth oxides (i.e., CeO2 and La2O3) were added as a modifier.

Laser Cladding of Ni60/WC/TiN Composite Coatings on 00Cr13Ni4Mo Hydro Turbine Blade Stainless Steel for Improvement of Wear Resistance

2012 ◽  
Vol 430-432 ◽  
pp. 101-105
Author(s):  
Kai Jin Huang ◽  
Hua Rui Jiang ◽  
Xin Lin
Keyword(s):  
Stainless Steel ◽  
Wear Resistance ◽  
Turbine Blade ◽  
Laser Cladding ◽  
Composite Coatings ◽  
High Hardness ◽  
Dry Sliding Wear ◽  
Wear Property ◽  
Hydro Turbine ◽  
Wear Condition

To improve the wear property of 00Cr13Ni4Mo hydro turbine blade stainless steel, Ni-based composite coatings were fabricated on 00Cr13Ni4Mo stainless steel by laser cladding using mixed powders of Ni60, WC and TiN. The microstructure of the coatings was characterized by XRD and SEM techniques. The wear resistance of the coatings was evaluated under dry sliding wear condition at room temperature. The results show that the coatings mainly consist of Ni-based solid solution, WC and TiN phases. The coatings exhibit excellent wear resistance due to its high hardness of WC and TiN phases. The main wear mechanisms of the coatings and the 00Cr13Ni4Mo sample are different, the former is abrasive wear and the latter is adhesive wear.

Possibilities of Preparing Tools Working in Conditions of Abrasion Wear with the Modification of the Tool Surfaces by Nitridation

2014 ◽  
Vol 635 ◽  
pp. 89-93
Author(s):  
Martin Orečný ◽  
Petra Lacková ◽  
Marián Buršák
Keyword(s):  
Wear Resistance ◽  
Nitrided Layer ◽  
High Hardness ◽  
Chromium Steel ◽  
Material Surface ◽  
Diffusion Annealing ◽  
Additional Increase ◽  
Abrasion Wear ◽  
Heat Treated

The proposed paper deals about the heat treatment of two types of chromium tool steels that are assigned to work in specific conditions of abrasion wear. The materials are heat treated to achieve high hardness for higher abrasion wear resistance. An additional increase of the materials abrasion wear resistance can be achieved by applying nitridation with diffusion annealing of the material surface. The paper deals about the influence of the material purity, his chemical composition on the process of diffusion, the quality of the nitrided layer of a vacuum smelted steel Bӧhler W400 VMR and a chromium steel X210Cr12.

The Effect of Processes Parameters on the Abrasive Wear Resistance of Boronized AISI 1050 Steel

2016 ◽  
Author(s):  
Mete Han Boztepe ◽  
Melih Bayramoglu
Keyword(s):  
Wear Resistance ◽  
Abrasive Wear ◽  
Mesh Size ◽  
High Hardness ◽  
High Strength ◽  
Constant Load ◽  
Abrasive Wear Resistance ◽  
Wear Testing ◽  
Wear Properties ◽  
Pin On Disk

Boronizing is one of the thermochemical surface treatment processes which is extensively used to obtain excellent mechanical properties such as high strength, very high hardness, good toughness and fracture toughness. In this study, AISI 1050 steel specimens have been subjected to pack boronizing process by using Ekabor 2 powder within the stainless steel seal container. The experiments were carried out at temperatures of 800 °C, 850 °C and 900 °C for 3, 6 and 9 hours to investigate the effect of these parameters on the wear resistance of boronized specimens. Pin-on-Disk wear testing is used to characterize wear properties of boronized specimens. Wear tests were performed at dry conditions under constant load of 30 N by using 220 mesh size Al2O3 abrasive paper. Different rotating speeds of the pin-on disk were selected as 300, 600, 900, 1200, 1500 revolutions for each of the test specimens. After the abrasive tests, weight losses of the specimens were measured to determine the abrasive wear resistance of boronized specimens. The results were also compared with unboronized and conventional hardened AISI 1050 steel specimens respectively.

scholarly journals Investigation of Mechanical Properties of AISI 316 Stainless Steel by Carbonitriding Process

2020 ◽  
Vol 184 ◽  
pp. 01018
Author(s):  
A Rohit Sai Krishna ◽  
B Vamshi Krishna ◽  
D Harshith ◽  
T Sashank ◽  
Ram Subbiah
Keyword(s):  
Stainless Steel ◽  
Wear Resistance ◽  
Wear Behavior ◽  
Wear Test ◽  
Salt Bath ◽  
Wear Loss ◽  
Case Hardening ◽  
Wide Range ◽  
Pin On Disc ◽  
Aisi 316 Stainless Steel

This project investigates on salt bath nitriding process in order to improve the wear behavior of the material. This process increases the hardness of the material. The specimens were nitrided at 580°c on three different timing hours such as 60 minutes, 90 minutes & 120 minutes. A pin on disc machine is used to conduct wear test, so that wear loss can be determined. The specimens are to be magnified by metallographic test like scanning electron microscope. The untreated specimen is used to compare with the nitrided specimen. The best specimen is chosen which determines the life of material & improves the better wear resistance. The hardness of untreated material and nitrided material are compared. The material AISI stainless steel has many unique properties but it lacks wear resistance and hardness because of which it has limited applications. By conducting heat treatment operation, the hardness of the material does not improve, but by conducting case hardening process the hardness of the outer case will be high compared to base metal. If the hardness and wear resistance of the material improves the material can be used in wide range of applications.

Microstructure and Corrosion Behavior of Arc Sprayed Stainless Steel Coatings

2000 ◽  
Author(s):  
T. Tajiri ◽  
Z. Zeng
Keyword(s):  
Stainless Steel ◽  
Corrosion Behavior ◽  
Salt Water ◽  
Steel Substrate ◽  
Salt Spray ◽  
Great Influence ◽  
Stainless Steel 316L ◽  
Metallographic Examination ◽  
Corrosion Behaviors ◽  
Corrosive Environments

Abstract The microstructure of arc sprayed stainless steel 316L coatings appears mainly in bright white matrix, deteriorated layers (grey), and black pores under optical microscopy. The black pores and the chromium-depleted areas in the deteriorated layers are known as the factors for decreasing the ability of protecting substrate under corrosive environments. Results of experiments in this paper suggests, in the condition of this study besides the factors mentioned above, Fe-Cr oxides should be another factor of dominating the corrosion resistance in the coatings. It also describes that the quantity and the distributions of such oxides are great influence on the corrosion behaviors. In this study, two kinds of coatings were used, one with thick deteriorated layers and another with thin deteriorated layers, which were sprayed on mild steel substrate by air atomization and nitrogen atomization respectively. Salt spray test and salt-water dip test were carried out to investigate corrosion behavior in macro and micro view. An effect of sealing treatment on the performance of the coatings was also examined. Results of metallographic examination and image processing analysis are well supported by a detailed investigation of corrosion behaviors of individual phases.

Effects of Substrate Bias Voltages on the Erosion Wear Resistance of TiN Coatings Deposited by Pulsed Filtered Vacuum Cathode Arc Deposition

2010 ◽  
Vol 443 ◽  
pp. 481-486 ◽  
Author(s):  
Feng Fang Wu ◽  
Jian Xin Deng ◽  
Pei Yan
Keyword(s):  
Wear Resistance ◽  
Erosion Rate ◽  
Average Diameter ◽  
Hard Metal ◽  
Solid Particles ◽  
Wear Loss ◽  
Erosion Wear ◽  
Tin Coatings ◽  
Cathode Arc ◽  
Arc Deposition

TiN coatings were produced on substrates of a hard metal at different bias by pulsed filtered vacuum cathode arc deposition assisted with ion bombardment. The erosion wear resistance of TiN coatings was investigated. The erosion wear was tested with a gas blast apparatus. In the test, TiN coatings were impacted at an impingement angle of 90° by angular SiC solid particles with an average diameter of 124um. The maximum depth of the erosion scar measured by the Veeco NT9300 optical profiler was used to evaluate the erosion wear loss of the coatings. The coatings proved to have lower erosion rate than the substrate material and consequently, the erosion rate increased significantly to the high level of the hard metal substrate after the coatings were penetrated. The results indicated that the TiN coating deposited at 150V bias had the lowest erosion wear rate and best wear resistance. The failure mechanism was revealed by examining the surface morphology of the coatings before and after the erosion test. The erosion wear of the TiN coatings behaved as typical brittle materials.

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