Plasma Chemical Synthesis of Aluminum Nitride Nanopowder

2019 ◽  
Vol 822 ◽  
pp. 628-633 ◽  
Author(s):  
Pavel Alexandrovich Novikov ◽  
Artem Eduardovich Kim ◽  
Nikolay Evgenievich Ozerskoi ◽  
Qing Sheng Wang ◽  
Anatoly Anatolyevich Popovich

We studied in detail the process of producing nanosized aluminum nitride using inductively coupled nitrogen plasma from micron powder of pure aluminum. The phase and granulometric composition of the obtained nanopowders, as well as their morphology, was studied. The influence of various parameters (initial components, gas flow rates, feed rate of the initial powder, etc.) on the synthesis result is determined. Received nanodispersed Al-AlN powder with particle sizes up to 300 nm and aluminum nitride content from 11.6 to 48.8%.

1999 ◽  
Vol 23 (1) ◽  
pp. 38-39
Author(s):  
N. Bellakhal ◽  
K. Draou ◽  
J. L. Brisset

Exposure of a 304 stainless steel sample to an inductively coupled low pressure radio frequency (RF) nitrogen plasma leads to the formation of a nitriding layer. The protective properties of this layer are investigated by electrochemical methods. The corrosion potential of the steel in an aqueous solution depends on the working parameters of the plasma such as the time exposure and the distance between the steel sample and the high voltage (HV) coil of the treatment reactor.


2011 ◽  
Vol 39 (6) ◽  
pp. 1103-1110 ◽  
Author(s):  
J. E. Ritchie ◽  
A. B. Williams ◽  
C. Gerard ◽  
H. Hockey

In this study, we evaluated the performance of a humidified nasal high-flow system (Optiflow™, Fisher and Paykel Healthcare) by measuring delivered FiO2 and airway pressures. Oxygraphy, capnography and measurement of airway pressures were performed through a hypopharyngeal catheter in healthy volunteers receiving Optiflow™ humidified nasal high flow therapy at rest and with exercise. The study was conducted in a non-clinical experimental setting. Ten healthy volunteers completed the study after giving informed written consent. Participants received a delivered oxygen fraction of 0.60 with gas flow rates of 10, 20, 30, 40 and 50 l/minute in random order. FiO2, FEO2, FECO2 and airway pressures were measured. Calculation of FiO2 from FEO2 and FECO2 was later performed. Calculated FiO2 approached 0.60 as gas flow rates increased above 30 l/minute during nose breathing at rest. High peak inspiratory flow rates with exercise were associated with increased air entrainment. Hypopharyngeal pressure increased with increasing delivered gas flow rate. At 50 l/minute the system delivered a mean airway pressure of up to 7.1 cmH2O. We believe that the high gas flow rates delivered by this system enable an accurate inspired oxygen fraction to be delivered. The positive mean airway pressure created by the high flow increases the efficacy of this system and may serve as a bridge to formal positive pressure systems.


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