Effect of Strain Rate on the Microstructure and β-Texture Evolutions in β-Processed Forging of a Near-β Titanium Alloy

2021 ◽  
Vol 1016 ◽  
pp. 882-887
Author(s):  
Ling Jian Meng ◽  
Tomonori Kitashima

The effect of strain rate on the β texture evolution during two-step hot forging of Ti-6246 alloy was investigated. The two-step forging consisted of 15% or 50% prior-β forging at 980°C and subsequent 60% or 25% forging at 870°C in the (α + β) dual-phase region. The total compression ratio was 75%, and the investigated strain rates were 0.01 and 1.0 s−1. The β forging texture showed typical {001} and {111} body-centered cubic textures. With increasing compression ratio in the (α + β) region and at a strain rate of 0.01 s−1, the amount of precipitated α phase increased. Dynamic recrystallization was rarely observed after forging in the (α + β) region at a strain rate of 0.01 s−1. Large amounts of α precipitates lowered the {001} β texture intensity through slip transmission between the α and β phases under the Burgers orientation relationship. However, in specimens forged at a strain rate of 1.0 s−1, as the compression ratio in the β single-phase region increased, the growth of dynamic-recrystallized β grains was promoted at the prior-β grain boundaries, where α-phase precipitation was not substantial. These effects resulted in a higher {001} texture intensity of the β phase in specimens forged at 1.0 s−1 compared with that of the β phase in specimens forged at 0.01 s−1.

2020 ◽  
Vol 321 ◽  
pp. 13003
Author(s):  
Zimin Lu ◽  
Jiao Luo ◽  
Miaoquan Li

Effect of strain rate on α-lath thickness of TC17 alloy with a basketweave microstructure was studied in the present work. For this purpose, this alloy was deformed in the β phase region and subsequently soluted and aged in α+β phase region. Moreover, optical micrograph (OM) and electron backscatter diffraction (EBSD) were applied to analyze the change of lath thickness at different strain rates. The result showed that α-lath thickness increased with increasing strain rate. This phenomenon was possibly attributed to the higher degree of variant selection (DVS) at higher strain rate (0.1 s-1). The higher DVS was beneficial for the formation of parallel α-lath colonies during cooling after deformation. And, these parallel α-lath colonies would more easily grow up and coarsen during subsequent heat treatment. Therefore, α-lath at higher strain rate is more thick.


Materials ◽  
2020 ◽  
Vol 13 (16) ◽  
pp. 3623 ◽  
Author(s):  
Danying Zhou ◽  
Hua Gao ◽  
Yanhua Guo ◽  
Ying Wang ◽  
Yuecheng Dong ◽  
...  

A self-designed Ti-35421 (Ti-3Al-5Mo-4Cr-2Zr-1Fe wt%) titanium alloy is a new type of low-cost high strength titanium alloy. In order to understand the hot deformation behavior of Ti-35421 alloy, isothermal compression tests were carried out under a deformation temperature range of 750–930 °C with a strain rate range of 0.01–10 s−1 in this study. Electron backscatter diffraction (EBSD) was used to characterize the microstructure prior to and post hot deformation. The results show that the stress–strain curves have obvious yielding behavior at a high strain rate (>0.1 s−1). As the deformation temperature increases and the strain rate decreases, the α phase content gradually decreases in the α + β phase region. Meanwhile, spheroidization and precipitation of α phase are prone to occur in the α + β phase region. From the EBSD analysis, the volume fraction of recrystallized grains was very low, so dynamic recovery (DRV) is the dominant deformation mechanism of Ti-35421 alloy. In addition to DRV, Ti-35421 alloy is more likely to occur in continuous dynamic recrystallization (CDRX) than discontinuous dynamic recrystallization (DDRX).


Metals ◽  
2018 ◽  
Vol 8 (8) ◽  
pp. 605 ◽  
Author(s):  
Yi Chen ◽  
Liang Cheng ◽  
Guang Yang ◽  
Yalin Lu ◽  
Fengbo Han

In this study, the deformation behavior of a Ti-40Al-10V (at.%) alloy within β single phase field was examined by means of isothermal compression at 1300 °C under strain rates of 2 s−1, 0.2 s−1, and 0.02 s−1, as well as its effect on the subsequent β→α transformation. The results showed that the alloy behaved steady-state flow with dislocation creep as the predominant rate-controlling process. Dynamic recrystallization (DRX) evidently occurred during deformation, and its volume fraction was dramatically increased so that at the lowest strain rate (0.02 s−1), a full-DRX β structure was obtained. The preferentially dynamic migration of grain boundaries with <100> orientation was demonstrated to be the major DRX mechanism. The texture was characterized by a <100> + <111> double-fiber at 2 s−1, but gradually transformed into a simple rotated cube orientationunder 0.02 s−1, accompanied by a decreasing texture intensity. During the subsequent β→α transformation, two types of α morphology wereproduced with evident variant selection, namely, the Widmannstatten colony and martensitic laths. Texture simulation revealed that the α texture was solely determined by parent β texture, despite of the variant selections.


2010 ◽  
Vol 638-642 ◽  
pp. 310-314
Author(s):  
Behrang Poorganji ◽  
Makoto Yamaguchi ◽  
Yoshio Itsumi ◽  
Katsushi Matsumoto ◽  
Tomofumi Tanaka ◽  
...  

In the present study, microstructure evolution of Ti-Fe alloys with different Fe content between 0.2-1.5mass% during hot deformation in (α+β) two-phase region is studied with focusing on effect of phase volume fraction at different deformation temperatures and strain rates. Hot deformation was conducted on the specimens quenched after β solutionizing at 1173K for 1.2ks at 1108, 1073 and 948K, by uniaxial compression by 50% at various strain rates ranged from 1 to 10-4 s-1. Initial structures are (α+β) lamellar structures of fine interlamellar spacing and colony sizes. Increase in Fe content results in increasing the fraction of the β phase at the given deformation temperature. Either colony size or interlamellar spacing is coarser at higher temperatures. At the higher deformation temperature where β phase fraction is larger, dynamic recovery of β phase is a major deformation mechanism while at a lower temperature, i.e., a higher α fraction, dynamic recrystallization of α phase occurs predominantly. It is concluded that critical strain needed for occurrence of dynamic recrystallization is decreased by increasing fraction of the α phase at the same deformation temperature, i.e., by decreasing Fe content. Furthermore, by increasing strain rate grain size of the recrystallized α is decreased.


2007 ◽  
Vol 539-543 ◽  
pp. 3607-3612 ◽  
Author(s):  
Jeoung Han Kim ◽  
Jong Taek Yeom ◽  
Nho Kwang Park ◽  
Chong Soo Lee

The high-temperature deformation behavior of the single-phase α (Ti-7.0Al-1.5V) and α + β (Ti-6Al-4V) alloy were determined and compared within the framework of self-consistent scheme at various temperature ranges. For this purpose, isothermal hot compression tests were conducted at temperatures between 650°C ~ 950°C to determine the effect of α/β phase volume fraction on average flow stress under hot-working condition. The flow behavior of α phase was estimated from the compression test results of single-phase α alloy whose chemical composition is close to that of α phase of Ti-6Al-4V alloy. On the other hand, the flow stress of β phase in Ti-6Al-4V was predicted by using self-consistent method. The flow stress of α phase was higher than that of β phase above 750°C, while the β phase revealed higher flow stress than α phase at 650°C. Also, at temperature above 750°C, the predicted strain rate of β phase was higher than that of α phase. It was found that the relative strength between α and β phase significantly varied with temperature.


Nanomaterials ◽  
2020 ◽  
Vol 10 (9) ◽  
pp. 1863
Author(s):  
Leonardo Bontempo ◽  
Sebastião G. dos Santos Filho ◽  
Luciana R. P. Kassab

In this study, we investigated the structural properties of TeO2-ZnO (TZ) and TeO2-ZnO-Au (TZA) thin films sputtered under different oxygen concentrations and either annealed or not annealed at 325 °C in air for 10 or 20 h. The lattice changes of the tellurium oxide were shown to be inherent in the polymorph properties of the α and β phases. The β phase was formed for null oxygen flow and the α phase was formed for different oxygen flows (0.5–7.0 sccm) during TZ and TZA sputtering. Au was encountered in its single phase or as AuTe2. The annealing had very little influence on the α and β phases for both TZ and TZA. It is worth noting that SiO2 and orthotellurate anions are both formed for not-null oxygen flow. An electrochemical mechanism was proposed to explain the SiO2 growth at the TZ/Si or TZA/Si interface, taking the orthotellurate anion as oxidizing agent into account.


2007 ◽  
Vol 26-28 ◽  
pp. 1279-1282 ◽  
Author(s):  
Koji Kato ◽  
Daisuke Hamatani ◽  
Kenji Matsuda ◽  
Tokimasa Kawabata ◽  
Yasuhiro Uetani ◽  
...  

It is known that the phase-decomposition process of 60/40 Cu-Zn alloy is so-called the bainitic transformation, and decomposition of α-phase from the β’-phase is as follow: β’ → α9R → αfcc. In this work,decomposition of α-phase from the β’ single phase of Cu-40.26at.%Zn alloy has been investigated by high-resolution transmission electron microscopy (HRTEM) to understand the phase transformation of this alloy. Especially, striations in the α-phase has been focused on the special feature for the change of the structure and hardening of this alloy during annealing. The result of a comparison between this alloy and the Si added alloy is also reported.


2015 ◽  
Vol 29 (10n11) ◽  
pp. 1540009
Author(s):  
Liang Cheng ◽  
Xiangyi Xue ◽  
Bin Tang ◽  
Hongchao Kou ◽  
Jinshan Li

In this paper, ingot breakdown process of a high Nb containing TiAl alloy with a chemical composition of Ti –42.63 Al –8.11 Nb –0.21 W –0.09 Y (at.%) has been investigated under conventional forging conditions. It was found that the present alloy possesses superior hot-workability that can be successfully forged by conventional upsetting route due to the appearance of large amount of β/B2 phase, though shear band was observed in the forged-pancake. Further studies revealed that hot-working performed in (α + β) phase region which can effectively impede the β → α transformation and thus significantly increase the volume fraction of β/B2 phase. In contrast, the amount of β/B2 phase was notably reduced by heat treatment at the same conditions. This stress-induced effect is considered to be responsible to the superior hot-workability of the present alloy and the mechanism has been discussed and reasonably clarified. It was also suggested that the stress-induced effect has practical significance that it allows the implementation of conventional multi-step forging process which can develop fine and uniform microstructures suitable for secondary processing.


2015 ◽  
Vol 641 ◽  
pp. 116-119 ◽  
Author(s):  
Janusz Krawczyk ◽  
Aneta Łukaszek-Sołek ◽  
Robert Dąbrowski

This work discusses the influence of the processing temperature, time and processing strain on the microstructure of the Ti6Al2Sn4Zr6Mo alloy. The Ti6Al2Sn4Zr6Mo alloy belongs to the two-phase (α+β) type of titanium alloys. The samples were compressed with the use of the Gleeble thermo-mechanical simulator at the temperatures of: 800, 900, 950, 1000 and 1100°C and at the strain rates of: 0.01; 0.1; 1; 10 and 100 s-1 to a total true strain of 1. The occurrence of the primary α phase in the Ti6Al2Sn4Zr6Mo alloy was investigated. The diagram showing the influence of the processing temperature and the strain rate on the dynamic recrystallization of the β phase was presented.The occurrence of the primary α phase precipitates blocks the grain growth. Therefore, the plastic deformation of this alloy should be carried out at a temperature at which the separation of the primary α phase occurs to finally obtain a material with a fine grain.


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