Investigation of Ni/Al/Ti Ohmic Contact on N-Type 4H-SiC

2021 ◽  
Vol 1045 ◽  
pp. 186-193
Author(s):  
Meng Qian Xue ◽  
Cai Ping Wan ◽  
Nian Nian Ge ◽  
Heng Yu Xu
Keyword(s):  
Surface Morphology ◽  
Ohmic Contact ◽  
Ohmic Contacts ◽  
Alloy System ◽  
Ohmic Resistance ◽  
Annealing Conditions ◽  
Atomic Force ◽  
Metal Composition ◽  
Specific Contact ◽  
P Type

In order to understand the contribution of various metals in the formation of ohmic contacts, Ni/Al/Ti ohmic contacts on n-type 4H-SiC in terms of a different annealing temperature and Ti composition are investigated, which is more difficult to form than p-type ohmic contact. The formation of the Ni/Al/Ti metal alloy system is much more sensitive to metal composition than annealing conditions. With the increase of metal composition, the contact with a high Ti content yields a lower specific contact resistivity compared with the low Ti contact. The annealed surface morphology and phase resultants were examined by scanning electron microscopy (SEM) and atomic force microscope (AFM), respectively. With the increase of Ti components, the surface morphology of the samples becomes more uniform and smoother, while the surface roughness remains unchanged. It implies that Ti metal can not only reduce the ohmic resistance, but also protect the surface of the sample and maintain the roughness.

Effects of Different Post-Implantation Annealing Conditions on the Electrical Properties of Interfaces to p-Type Implanted 4H-SiC

2012 ◽  
Vol 717-720 ◽  
pp. 825-828
Author(s):  
Alessia Frazzetto ◽  
Fabrizio Roccaforte ◽  
Filippo Giannazzo ◽  
R. Lo Nigro ◽  
M. Saggio ◽  
...  
Keyword(s):  
Electrical Properties ◽  
Ohmic Contacts ◽  
Specific Contact Resistance ◽  
Electrical Parameters ◽  
Capping Layer ◽  
Annealing Conditions ◽  
Specific Contact ◽  
Activation Annealing ◽  
P Type ◽  
Post Implantation

This paper reports on the effects of different post-implantation annealings on the electrical properties of interfaces to p-type implanted 4H-SiC. The morphology of p-type implanted 4H-SiC was controlled using a capping layer during post-implantation activation annealing of the dopant. Indeed, the surface roughness of Al-implanted regions strongly depends on the use of the protective capping layer during the annealing. However, while the different morphological conditions do not affect the macroscopical electrical properties of the implanted SiC (such as the sheet resistance), they led to an improvement of the morphology and of the specific contact resistance of Ti/Al Ohmic contacts formed on the implanted regions. These electrical and morphologic improvements were associated with a lowering of Schottky barrier height. Preliminary results showed that the different activation annealing conditions of p-type implanted SiC can affect also the electrical parameters (like threshold voltage and mobility) of lateral MOSFETs.

Effects of Surface and Interlayer Processing Conditions on Selected Ohmic Contact Metallizations for p-type Silicon Carbide

2000 ◽  
Vol 640 ◽  
Author(s):  
L. M. Porter ◽  
T. Jang ◽  
T. Worren ◽  
K. C. Chang ◽  
N. A. Papanicolaou ◽  
...  
Keyword(s):  
Silicon Carbide ◽  
Surface Morphology ◽  
Ohmic Contact ◽  
Deposition Temperature ◽  
Doping Concentration ◽  
Processing Conditions ◽  
Dopant Incorporation ◽  
Specific Contact ◽  
Specific Contact Resistivity ◽  
P Type

ABSTRACTA comparative study of Pt and Pt/Si contacts to p-type 6H-SiC in terms of various processing conditions and interlayer specifications was performed. Deposition temperature, the thickness of the Si layer, and B-dopant incorporation in the Si were found to significantly affect the specific contact resistivity (SCR) values. In addition, pre-etching of the SiC surface in SF6 + Ar was found to consistently reduce the SCR's. The lowest average SCR values were 3 × 10−5 Ωcm2 for Pt/Si/SiC contacts deposited on pre-etched SiC surfaces (7.0 × 1018 cm−3 doping concentration) and annealed at 1100 °C for 5 min.Aluminum-titanium contacts also showed dependence on the thicknesses of the Al and Ti layers and on the locations of the layers. Differences in both the SCRs and surface morphology are presented.

A Comparative Optimization of Electrical Properties and Surface Morphology of Ti/Al/Ta/Au Ohmic Contacts in AlGaN/GaN HEMTs on Si(111), Sapphire, 4H-SiC Substrates

2012 ◽  
Vol 538-541 ◽  
pp. 2207-2210
Author(s):  
Sung Jin Cho ◽  
Cong Wang ◽  
Nam Young Kim
Keyword(s):  
Surface Morphology ◽  
Sapphire Substrate ◽  
Ohmic Contact ◽  
Annealing Time ◽  
Ohmic Contacts ◽  
Annealing Temperature ◽  
Contact Process ◽  
Annealing Temperatures ◽  
Ohmic Resistance ◽  
Gan Hemts

In the process of characterizing AlGaN/GaN HEMTs on Si (111), Sapphire, 4H-SiC substrates, various Rapid Thermal Annealing (RTA) conditions for the Ti/Al/Ta/Au ohmic contact process and the resulting surface analysis have been investigated. In order to achieve a low ohmic contact resistance (RC) and a high quality surface morphology, we tested seven steps (800 °C to 920 °C) annealing temperatures and two steps (15, 30 sec) annealing times. According to these annealing temperatures and times, the optimal ohmic resistance of 3.62 × 10-6 Ohm • cm2 on Si(111) substrate, 9.44 × 10-6 Ohm • cm2 on Sapphire substrate and 1.24 × 10-6 Ohm • cm2 on 4H-SiC substrate are obtained at an annealing temperature of 850 °C and an annealing time of 30 sec, 800 °C and an annealing time of 30 sec and 900 °C and an annealing time of 30 sec, respectively. The surface morphologies of the ohmic contact metallization at different annealing temperatures are measured using an Atomic Force Microscope (AFM). AFM morphology Root Mean Square (RMS) level determines the relationship of the annealing temperature and the annealing time for all of the samples. According to these annealing temperatures and times, the optimal ohmic surface RMS roughness of 13.4 nm on Si(111) substrate, 3.8 nm on Sapphire substrate and 2.9 nm on 4H-SiC substrate are obtained at an annealing temperature of 850 °C and an annealing time of 30 sec, 800 °C and an annealing time of 30 sec and 900 °C and an annealing time of 30 sec, respectively.

Formation of Ni/Pt/Au Ohmic Contacts to p-GaN

1997 ◽  
Vol 482 ◽  
Author(s):  
Ja-Soon Jang ◽  
Hyo-Gun Kim ◽  
Kyung-Hyun Park ◽  
Chang-Sub Um ◽  
Il-Ki Han ◽  
...  
Keyword(s):  
Contact Resistance ◽  
Ohmic Contact ◽  
Ohmic Contacts ◽  
Chemical Vapor ◽  
Electron Beam Evaporation ◽  
Specific Contact Resistance ◽  
Metal Thin Films ◽  
Linear Behavior ◽  
Specific Contact ◽  
P Type

AbstractWe report a new Ni/Pt/Au (20/30/80 nm) metallization scheme to achieve a low ohmic contacts to p-type GaN with a carrier concentration of 9.4 × 1016 cm-3. A Mg-doped GaN layer (0.5 μm) was grown on (0001) sapphire substrate by metalorganic chemical vapor deposition (MOCVD). All metal thin films were deposited on the p-GaN layer in an electron-beam evaporation system. Samples were annealed by a rapid thermal annealing (RTA) process at a range of temperatures from 300 °C to 850 °C under a flowing Ar atmosphere. A circulartransmission line model (c-TLM) was employed to calculate the specific contact resistance, and current-voltage (I-V) data were measured with HP4155A. The Ni/Pt/Au contacts without the annealing process showed nearly rectifying characteristics. The ohmic contacts were formed on the samples annealed at 500 °C for 30 sec and the I-V data showed a linear behavior. The specific contact resistance was 2.1 × 10-2 Ωcm2. However with increasing the annealing temperature above 600 °C, ohmic contacts were again degraded. Auger electron spectroscopy (AES) depth profiles were used to investigate the interfacial reactions between the trilayer and GaN. AES results suggested that Pt plays a significant role in forming ohmic contact as an acceptor at the interface. Atomic force microscope (AFM) also showed that the samples with good ohmic contact have very smooth surface.

Investigation on Ag/Ti Ohmic Contacts to Si-Doped n-Type Al0.27Ga0.73N and the Effect of Post Annealing Treatments

2006 ◽  
Vol 517 ◽  
pp. 281-286
Author(s):  
Surina Othman ◽  
F.K. Yam ◽  
Abu Hassan Haslan ◽  
Hassan Zainuriah
Keyword(s):  
Surface Morphology ◽  
Ohmic Contacts ◽  
Cryogenic Cooling ◽  
Force Microscopy ◽  
Ohmic Behavior ◽  
Atomic Force ◽  
Transmission Line Method ◽  
Specific Contact ◽  
Different Temperatures ◽  
Si Doped

In this study, we investigated the contact characteristics of bi-layer thin films, Ag (200nm)/Ti (100nm) on Si-doped n-type Al0.27Ga0.73N film grown on sapphire substrate. The contacts were annealed at different temperatures (400°C-800°C) for 10 min in N2 ambient. The effects of cryogenic cooling immediately after heat treatment for improving ohmic behavior (I-V linearity) of the samples were reported. Specific contact resistivity, ρc, was determined using transmission line method (TLM) via current-voltage (I-V) measurements. Scanning electron microscopy (SEM) measurements were carried out on the as-deposited, annealed (N), and annealed-and-cryogenically (N+C) treated contacts where the surface morphology of each of these conditions were compared. In addition, measurement of the samples by atomic force microscopy (AFM) was taken in order to characterize the surface morphology.

scholarly journals Thermally Stable Ohmic Contact to p-Type 4H-SiC Based on Ti3SiC2 Phase

2016 ◽  
Vol 858 ◽  
pp. 553-556 ◽  
Author(s):  
Tony Abi-Tannous ◽  
Maher Soueidan ◽  
Gabriel Ferro ◽  
Mihai Lazar ◽  
Christophe Raynaud ◽  
...  
Keyword(s):  
Thin Films ◽  
Electrical Properties ◽  
Magnetron Sputtering ◽  
Ohmic Contact ◽  
Room Temperature ◽  
Ohmic Contacts ◽  
Specific Contact Resistance ◽  
Specific Contact ◽  
Thermionic Field Emission ◽  
P Type

In this study, the electrical properties of Ti3SiC2 based ohmic contacts formed on p-type 4H-SiC(0001) 4°-off substrates were studied. The Ti3SiC2 thin films were grown by thermal annealing (from 900°C to 1200°C) of Ti50Al50 layer deposited by magnetron sputtering. XRD analyzes were performed on the samples to further investigate the compounds formed after annealing. Using TLM structures, the Specific Contact Resistance (SCR) at room temperature of all contacts was measured. The temperature dependence (up to 600°C) of the SCR was studied to understand the current mechanisms at the interface and to determine the barrier height value by fitting the experimental results using the thermionic field emission theory. Aging tests showed that Ti3SiC2 based contacts were stable up to 200h at 600°C under Ar.

Improvement of the Specific Contact Resistance on P-Type 4H-SiC by Using a Highly P-Typed Doped 4H-SiC Layer Selectively Grown by VLS Transport

2014 ◽  
Vol 806 ◽  
pp. 57-60
Author(s):  
Nicolas Thierry-Jebali ◽  
Arthur Vo-Ha ◽  
Davy Carole ◽  
Mihai Lazar ◽  
Gabriel Ferro ◽  
...  
Keyword(s):  
Contact Resistance ◽  
Ohmic Contacts ◽  
Schottky Barrier Height ◽  
Annealing Temperature ◽  
Process Condition ◽  
Specific Contact Resistance ◽  
High Doping Level ◽  
Annealing Temperatures ◽  
Specific Contact ◽  
P Type

This work reports on the improvement of ohmic contacts made on heavily p-type doped 4H-SiC epitaxial layer selectively grown by Vapor-Liquid-Solid (VLS) transport. Even before any annealing process, the contact is ohmic. This behavior can be explained by the high doping level of the VLS layer (Al concentration > 1020 cm-3) as characterized by SIMS profiling. Upon variation of annealing temperatures, a minimum value of the Specific Contact Resistance (SCR) down to 1.3x10-6 Ω.cm2 has been obtained for both 500 °C and 800 °C annealing temperature. However, a large variation of the SCR was observed for a same process condition. This variation is mainly attributed to a variation of the Schottky Barrier Height.

Si+ Implantation and Activation in GaN Comparison of GaN on Sapphire and GaN on Silicon

2012 ◽  
Vol 711 ◽  
pp. 213-217 ◽  
Author(s):  
Anne Elisabeth Bazin ◽  
Frédéric Cayrel ◽  
Mohamed Lamhamdi ◽  
Arnaud Yvon ◽  
Jean Christophe Houdbert ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Ohmic Contacts ◽  
Silicon Oxide ◽  
Electrical Activation ◽  
Specific Contact Resistance ◽  
Force Microscopy ◽  
Atomic Force ◽  
Specific Contact ◽  
Good Behaviour ◽  
Scanning Electron

In this paper, we evaluated gallium nitride heteroepitaxially grown on sapphire (GaN/Sa) and grown on silicon (GaN/Si) faced to implantation doping. Si+ was implanted on low doped n-type epilayers in order to create a plateau around 1020at.cm-3. All the samples were capped with a silicon oxide and annealed between 1000°C and 1150°C. The surface quality was evaluated in terms of roughness, pit density and maximum pit diameter using Atomic Force Microscopy (AFM) and Scanning Electron Microscopy (SEM). Finally, the dopant electrical activation was studied with Ti-Al contacts using the circular Transfert Length Method (c-TLM). This study shows that low Specific Contact Resistance (SCR) values of 8x10-5Ω.cm2 and 6x10-6Ω.cm2 are respectively obtained on GaN/Sa sample annealed at 1150°C-2min and on GaN/Si sample annealed at 1150°C-30s, proving that good ohmic contacts are obtained on both materials. Nevertheless, a compromise has to be done between the low SCR values obtained and the GaN surface degradation, observed by AFM and SEM after the different annealing treatments and which could affect the good behaviour of the GaN devices.

The Microstructure and Electrical Properties of Directly Deposited TiN Ohmic Contacts to Gallium Nitride.

1999 ◽  
Vol 595 ◽  
Author(s):  
P. Ruterana ◽  
G. Nouet ◽  
Th. Kehagias ◽  
Ph. Komninou ◽  
Th. Karakostas ◽  
...  
Keyword(s):  
Gallium Nitride ◽  
Electrical Properties ◽  
Film Thickness ◽  
Ohmic Contact ◽  
Ohmic Contacts ◽  
Epitaxial Relationship ◽  
Si Doped ◽  
P Type ◽  
20 Nm

AbstractWhen the stoichiometric TiN was deposited directly on GaN, we obtained columnar TiN grains of 5-20 nm section which cross the whole film thickness and are rotated mostly around the [111] axis. The conventional epitaxial relationship is obtained and no amorphous patches are observed at the interface. The deposition of TiN on Si doped GaN layers lead to the formation of an ohmic contact, whereas we obtain a rectifying contact on p type layers.

Ohmic Contacts to p-Type InGaAs/InP with a Graded Bandgap Heterobarrier

1993 ◽  
Vol 318 ◽  
Author(s):  
Patrick W. Leech ◽  
Geoffrey K. Reeves
Keyword(s):  
Contact Resistance ◽  
Ohmic Contacts ◽  
Rutherford Backscattering Spectrometry ◽  
Specific Contact Resistance ◽  
Superlattice Structure ◽  
Specific Contact ◽  
P Type ◽  
Metal Layers ◽  
Anneal Temperature ◽  
Graded Bandgap

ABSTRACTOhmic contacts to p-type InP with an In0.47Ga0.53As buffer layer and an interposed superlattice of 50 Å In0.47Ga0.53As/ 50 Å InP have been investigated. Initial studies of contacts to In0.47Ga0.53As/ InP without the superlattice structure have shown that Pd/Zn/Pd/Au metallization produced a lower specific contact resistance (pc = 1.1 × 10−4 Ω cm2) than Pd/Ge/Au, and over a wider range of anneal temperature than Au/Zn/Au. The incorporation of the superlattice in the p-In0.47Ga0.53As/ InP structure resulted in Pd/Zn/Pd/Au contacts with pc of 3.2 × 10−5 Ω cm2 as-deposited and 7.5 × 10−6 Ω.cm2 after a 500 °C anneal. The presence of Pd/Zn in the metallization was shown as important in reducing pc. Significant intermixing of the metal layers and In0.47Ga0.53As occured at ≥ 350 °C, as revealed by Rutherford backscattering spectrometry.

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