Production of Cu-Sn-Zn Ternary Alloy Coating via Electroplating

2017 ◽  
Vol 888 ◽  
pp. 400-403
Author(s):  
Rozainita Rosley ◽  
Suzi Salwah Jikan ◽  
Nur Azam Badarulzaman
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Surface Morphology ◽  
Ternary Alloy ◽  
Phase Structure ◽  
Alloy Coating ◽  
Complexing Agents ◽  
Carbon Substrate ◽  
X Ray ◽  
Scanning Electron

This research deals with the interest in production of Cu-Sn-Zn ternary alloy coating via electroplating on carbon substrate by using less hazardous electrolyte. A detailed study was made on the effect of different concentration of reducing and complexing agents. The surface morphology and phase structure of the deposited layers were examined by scanning electron microscope (SEM) equipped with energy dispersive x-ray spectroscopy (EDS), respectively. The results confirmed that the layers of Cu-Sn-Zn was obtained with this less hazardous electrolyte.

Microstructure Characterization of Laser Clad TiVCrAlSi High Entropy Alloy Coating on Ti-6Al-4V Substrate

2010 ◽  
Vol 154-155 ◽  
pp. 621-625 ◽  
Author(s):  
Can Huang ◽  
Yong Zhong Zhang ◽  
Rui Vilar
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Alloy Coating ◽  
High Entropy Alloy ◽  
X Ray Diffraction ◽  
X Ray ◽  
High Entropy ◽  
Bcc Phase ◽  
Scanning Electron

Due to the promising properties of high entropy alloy, TiVCrAlSi high entropy alloy coating was prepared on Ti-6Al-4V alloy surface by laser cladding. The microstructure and phase analysis of as-cast TiVCrAlSi alloy and laser clad coating were characterized by scanning electron microscope and X-ray diffraction. The results indicate that as-cast TiVCrAlSi alloy is mainly composed of (Ti,V)5Si3 and bcc phase. The laser clad coating is metallurgically bonded to the substrate with few pores and cracks. Laser clad TiVCrAlSi coating is also composed of (Ti,V)5Si3 and bcc phases.

Photoluminescence and Structure of Chemically Etched Si

1991 ◽  
Vol 256 ◽  
Author(s):  
S. Shih ◽  
K. H. Jung ◽  
T. Y. Hsieh ◽  
J. Sarathy ◽  
C. Tsai ◽  
...  
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Surface Morphology ◽  
Chemical Etching ◽  
Room Temperature ◽  
Porous Si ◽  
X Ray Diffraction ◽  
X Ray ◽  
First Time ◽  
Scanning Electron

ABSTRACTWe demonstrate for the first time that chemical etching of Si in HF-HNO3-based solution without applying bias can produce a room temperature photoluminescent porous Si layer. Scanning electron microscope studies reveal a surface morphology similar to that of the conventionally anodized porous Si. The formation mechanism of the chemically etched (CE) film can be explained by a local anodization concept. X-ray diffraction studies on the luminescent CE porous Si show a broad amorphous peak.

Hypochlorous and Urea Modifications on Carbon Fiber Surface and Effects on Microorganism Immobilization

2011 ◽  
Vol 356-360 ◽  
pp. 106-109 ◽  
Author(s):  
Yan Ling Bao ◽  
Guang Ze Dai ◽  
Chuan Jiang
Keyword(s):  
Electron Microscope ◽  
Carbon Fiber ◽  
Scanning Electron Microscope ◽  
Surface Morphology ◽  
Photoelectron Spectroscopy ◽  
Fiber Surface ◽  
The Other ◽  
X Ray ◽  
Microorganism Immobilization ◽  
Scanning Electron

PAN-based carbon fiber (CF) was modified by hypochlorous and urea in current treatments. The CF surface morphology and natures were characterized by specific facilities, such as scanning electron microscope (SEM), X-ray photoelectron spectroscopy (XPS) and the degree of moisture. On the other hand, the biocompatibility nature was indicated by immobilization results of microorganisms on CF. The results show that the surface hydrophilicity and roughness of CF surface would contribute greatly to improve the immobilization ability of microorganisms on CF surface, and the produced oxygen on CF has more effect on microorganism immobilization than nitrogen.

X-ray micro tomography in the scanning electron microscope

1978 ◽  
Vol 36 (1) ◽  
pp. 106-107 ◽  
Author(s):  
W. Brünger
Keyword(s):  
Electron Beam ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Target Surface ◽  
The Body ◽  
X Rays ◽  
Cross Sectional ◽  
X Ray ◽  
Micro Tomography ◽  
Scanning Electron

Reconstructive tomography is a new technique in diagnostic radiology for imaging cross-sectional planes of the human body /1/. A collimated beam of X-rays is scanned through a thin slice of the body and the transmitted intensity is recorded by a detector giving a linear shadow graph or projection (see fig. 1). Many of these projections at different angles are used to reconstruct the body-layer, usually with the aid of a computer. The picture element size of present tomographic scanners is approximately 1.1 mm2.Micro tomography can be realized using the very fine X-ray source generated by the focused electron beam of a scanning electron microscope (see fig. 2). The translation of the X-ray source is done by a line scan of the electron beam on a polished target surface /2/. Projections at different angles are produced by rotating the object.During the registration of a single scan the electron beam is deflected in one direction only, while both deflections are operating in the display tube.

PHAX-SCAN: Functional integration of a Scanning Electron Microscope and an energy-dispersive x-ray analyser

1989 ◽  
Vol 47 ◽  
pp. 56-57
Author(s):  
Marc H. Peeters ◽  
Max T. Otten
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
High Speed ◽  
High Performance ◽  
Functional Integration ◽  
Energy Dispersive ◽  
X Rays ◽  
X Ray ◽  
High Speed Analysis ◽  
Scanning Electron

Over the past decades, the combination of energy-dispersive analysis of X-rays and scanning electron microscopy has proved to be a powerful tool for fast and reliable elemental characterization of a large variety of specimens. The technique has evolved rapidly from a purely qualitative characterization method to a reliable quantitative way of analysis. In the last 5 years, an increasing need for automation is observed, whereby energy-dispersive analysers control the beam and stage movement of the scanning electron microscope in order to collect digital X-ray images and perform unattended point analysis over multiple locations.The Philips High-speed Analysis of X-rays system (PHAX-Scan) makes use of the high performance dual-processor structure of the EDAX PV9900 analyser and the databus structure of the Philips series 500 scanning electron microscope to provide a highly automated, user-friendly and extremely fast microanalysis system. The software that runs on the hardware described above was specifically designed to provide the ultimate attainable speed on the system.

PENGGUNAAN TiO2 PARTIKEL NANO HASIL SINTESIS BERBASIS AIR MENGGUNAKAN METODA SOL-GEL PADA BAHAN KAPAS SEBAGAI APLIKASI UNTUK TEKSTIL ANTI UV

Arena Tekstil ◽  
2013 ◽  
Vol 28 (1) ◽  
Author(s):  
Maya Komalasari ◽  
Bambang Sunendar
Keyword(s):  
Fourier Transform ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Sol Gel ◽  
Crosslinking Agent ◽  
X Ray Diffraction ◽  
Nano Tio2 ◽  
X Ray ◽  
Infra Red ◽  
Scanning Electron

Partikel nano TiO2 berbasis air dengan pH basa telah berhasil disintesis dengan menggunakan metode sol-gel dan diimobilisasi pada kain kapas dengan menggunakan kitosan sebagai zat pengikat silang. Sintesis dilakukan  dengan prekursor TiCl4 pada konsentrasi 0,3 M, 0,5 M dan 1 M, dan menggunakan templat kanji dengan proses kalsinasi pada suhu 500˚C selama 2 jam. Partikel nano TiO2 diaplikasikan ke kain kapas dengan metoda pad-dry-cure dan menggunakan kitosan sebagai crosslinking agent. Berdasarkan hasil Scanning Electron Microscope (SEM),diketahui bahwa morfologi partikel TiO2 berbentuk spherical dengan ukuran nano (kurang dari 100 nm). Karakterisasi X-Ray Diffraction (XRD) menunjukkan adanya tiga tipe struktur kristal utama, yaitu (100), (101) dan (102) dengan fasa kristal yang terbentuk adalah anatase dan rutile. Pada karakterisasi menggunakan SEM terhadap serbuk dari TiO2 yang telah diaplikasikan ke permukaan kain kapas, terlihat adanya imobilisasi partikel nano TiO2 melalui ikatan hidrogen silang dengan kitosan pada kain kapas. Hasil analisa tersebut kemudian dikonfirmasi dengan FTIR (Fourier Transform Infra Red) yang hasilnya memperlihatkan puncak serapan pada bilangan gelombang 3495 cm-1, 2546 cm-1, dan 511 cm-1,  yang masing-masing diasumsikan sebagai adanya vibrasi gugus fungsi O-H, N-H dan Ti-O-Ti. Hasil SEM menunjukkan pula bahwa kristal nano yang terbentuk diantaranya adalah fasa rutile , yang berdasarkan literatur terbukti dapatberfungsi sebagai anti UV.

scholarly journals Influence of the Nb and V Addition on the Microstructure and Corrosion Resistance of the Fe-B-Co-Si Alloy

Materials ◽  
2021 ◽  
Vol 14 (14) ◽  
pp. 4045
Author(s):  
Rafał Mech ◽  
Jolanta Gąsiorek ◽  
Amadeusz Łaszcz ◽  
Bartosz Babiarczuk
Keyword(s):  
Corrosion Resistance ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Significant Influence ◽  
Corrosion Performance ◽  
X Ray ◽  
Final Performance ◽  
Differential Calorimeter ◽  
Comparison Of The Results ◽  
Scanning Electron

The paper presents a comparison of the results of the corrosion resistance for three Fe-B-Co-Si-based newly developed alloys with the addition of Nb and V. The corrosion performance differences and microstructure variations were systematically studied using scanning electron microscope, electric corrosion equipment, X-ray diffractometer, and differential calorimeter. It has been shown that each alloying addition increased the corrosion resistance. The highest corrosion resistance obtained by potentiodynamic polarization was found for the alloy with both Nb and V addons (Fe57Co10B20Si5Nb4V4) and lowest in the case of the basic four-element Fe62Co15B14Si9 material. This shows that the proper choice of additions is of significant influence on the final performance of the alloy and allows tailoring of the material for specific applications.

scholarly journals Characterizing Severely Plastically Deformed Materials Using Transmission Kikuchi Diffraction and Energy Dispersive X-ray Spectroscopy in the Scanning Electron Microscope

2013 ◽  
Vol 19 (S2) ◽  
pp. 692-693
Author(s):  
P. Trimby
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Energy Dispersive ◽  
X Ray ◽  
Scanning Electron

Extended abstract of a paper presented at Microscopy and Microanalysis 2013 in Indianapolis, Indiana, USA, August 4 – August 8, 2013.

Photoelectrochemical Properties of Anatase TiO2 Films Prepared by Improved Liquid Phase Deposition

2015 ◽  
Vol 1120-1121 ◽  
pp. 419-423
Author(s):  
Cai Xia Lei ◽  
X.L. Jiang ◽  
Y. Liu ◽  
X. Liu ◽  
Y.T. Ma ◽  
...  
Keyword(s):  
Electron Microscope ◽  
Liquid Phase ◽  
Scanning Electron Microscope ◽  
Reaction Temperature ◽  
White Light ◽  
Photoelectrochemical Properties ◽  
Liquid Phase Deposition ◽  
X Ray ◽  
Good Crystallinity ◽  
Scanning Electron

In this paper, the hydrothermal-assisted liquid phase deposition (HT-LPD) method has been developed to prepare TiO2 films. The crystalline structures and morphologies of as-prepared TiO2 films were analyzed using an X-ray diffractometer (XRD) and scanning electron microscope (SEM). It was found that the HT-LPD TiO2 film showed good crystallinity with preferrred orientation along c-axis. Moreover, the as-prepared TiO2 films consisted of two layers, with the tiny nanoparticles as the underlying layer and the flower-like clusters as the upper layer. The photoelectrochemical measurements revealed that, when illuminated by the white light, the HT-LPD TiO2 films exhibited a more negative photopotential value and an increased photocurrent value with elevated reaction temperature, excepting for the sample prerared at 150 °C. In summary, the TiO2 films prepared by the improved LPD method could be served as the promising photoanode for the photoelectrochemical applications.

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