Intermetallic Phases Identification and Diffusion Simulation in Twin-Roll Cast Al-Fe Clad Sheet

Aluminium steel clad materials have high potential for industrial applications. Their mechanical properties are governed by an intermetallic layer, which forms upon heat treatment at the Al-Fe interface. Transmission electron microscopy was employed to identify the phases present at the interface by selective area electron diffraction and energy dispersive spectroscopy. Three phases were identified: orthorhombic Al5Fe2, monoclinic Al13Fe4 and cubic Al19Fe4MnSi2. An effective interdiffusion coefficient dependent on concentration was determined according to the Boltzmann–Matano method. The highest value of the interdiffusion coefficient was reached at the composition of the intermetallic phases. Afterwards, the process of diffusion considering the evaluated interdiffusion coefficient was simulated using the finite element method. Results of the simulations revealed that growth of the intermetallic phases proceeds preferentially in the direction of aluminium.

Experimental and numerical investigations of springback and residual stresses in bending of a three-ply clad sheet

In the present work, springback behaviour of a three-ply clad sheet metal, comprising of layers of SS430 and SS304 sandwiched with a layer of AA1050 is investigated in V-bending by using analytical, experimental and simulation techniques. The developed analytical model is based on theory of bending using Hill’s anisotropic yield criterion. The tensile properties of the clad sheet and individual layers oriented at three different directions w.r.t. the rolling direction are characterized. The tensile properties of the individual layers are used in the material model of analytical and numerical predictions of the springback. It is observed that the samples of the clad sheet which are transverse to the rolling direction, exhibit highest springback values due to higher tensile strength of the sheet when compared with the results acquired for other two orientations w.r.t. the rolling direction. These results are endorsed by the springback results obtained from analytical and simulation methods. The effect of sheet setting on the die during bending is also investigated using different techniques. The resulting longitudinal stresses before and after springback are analysed on inner and outer layers of the tested samples using experimental and numerical simulation procedures. In both the cases of sheet settings, the results of residual stress after springback predicted by simulations agree with the experimental results except a few cases.

Formation of Heterogeneous Microstructure in AA1050/AA5052/AA6061/AA1050 Layered Sheet Processed by Cold Roll-Bonding and Subsequent Annealing

A cold roll-bonding process was applied to fabricate an AA1050/AA6061/AA5052/AA1050 four-layer clad sheet and subsequently annealed. Three types of aluminum alloy sheets such as AA1050, AA6061 and AA5052 with 2 mm thickness, 40 mm width and 300 mm length were stacked up each other after such surface treatment as degreasing and wire brushing, then reduced to a thickness of 2 mm by multi-pass cold rolling. The rolling was performed at ambient temperature without lubricant using a 2-high mill with a roll diameter of 400 mm at rolling speed of 6.0 m/sec. The roll bonded AA1050/AA6061/AA5052/AA1050 clad sheet was then annealed for 0.5 h at 200~400 °C. Microstructures of the as-roll bonded and subsequently annealed aluminum sheets are investigated by electron back scatter diffraction (EBSD) measurement. After rolling, the roll-bonded AA1050/AA5052/AA6061/AA1050 sheet showed a typical deformation structure that the grains are largely elongated to the rolling direction. However, after annealing, it exhibits a very heterogeneous structure consisting of both deformation structure and recrystallization structure containing nanometer order grains. The formation of this heterogeneous structure and texture with annealing is investigated in detail through EBSD analysis.

Effects of Annealing and Deformation on Sagging Resistance of a Hot-Rolled, Four-Layered Al Alloy Clad Sheet

Multilayer brazeable aluminum alloy sheet is prone to collapse during high-temperature brazing process. The sagging resistance of the aluminum composite sheet needs to be further improved for quality control. Effects of annealing and rate of reduction on sagging resistance, microstructure, and Si diffusion of a hot-rolled, four-layered Al clad sheet (4343/3003/6111/3003) were investigated by means of a sagging device, OM, SEM, and TEM. Results showed that once annealed at 360°C, the sagging distance was increased from 3 to 15.7 mm as the reduction rate changed from 10% to 40%. By increasing annealing temperature to 410°C, those were changed from 3.1 to 20.8 mm accordingly. At 360°C/40% and 410°C/40%, specimens exhibited weak sagging resistance, whereas fine recrystallized grains were formed in the core promoting Si penetration along grain boundaries. While the specimens were treated at 360°C/10% and 410°C/10%, better sagging resistance was observed due to the formation of coarse recrystallized grains that can suppress erosion of Si. At the same reduction rate, the sagging resistance was higher for the sample annealed at a lower temperature as more precipitates appeared in the core (at 360°C), thus leading to an increase in strength.

Effects of Post Heat Treatment on the Mechanical Properties of Cold-Rolled Ti/Cu Clad Sheet

Titanium and titanium alloys have excellent corrosion and heat resistance, but weak electric and thermal conductivity. The weak conductivity of titanium can be overcome by cladding with copper, which has high conductivity. Although titanium is expensive, it is selected as a material suitable for applications requiring corrosion resistance such as in heat exchangers. This study was to investigate the effect of post heat treatment on the mechanical properties of the Ti/Cu cold-rolled clad plate by using the interfacial diffusion bonding. A titanium clad by cold rolling should be heat-treated after the rolling process to improve the bonding properties through the diffusion of metals and removal of residual stress due to work hardening, despite the easy formation of intermetallic compounds of Ti and Cu. As a result post-treatment, the elongation was improved by more than two times from 21% to max. 53% by the Ti-Cu interface diffusion phenomenon and the average tensile strength of the 450 °C heat-treated specimens was 353 MPa. By securing high elongation while maintaining excellent tensile and yield strength through post-treatment, the formability of Ti-Cu clad plate can be greatly improved.

Experimental study on bending behaviour of aluminium-copper clad sheets in V-bending process

The bimetallic sheets are used in the industrial sheet metal products to meet the demands of multi-functionality. The bending behaviour of bimetallic sheet is contributed by individual layers of the sheet and it is entirely different from the monolithic material. In this study, V-bending experiments are carried out to understand the springback, bend force and thickness change of Al-Cu clad sheets. The effect of different parameters such as sheet thickness, sheet setting condition, die angle, die opening and punch radius have been investigated. The results indicated that springback is more for smaller die angle, wider die opening and larger punch radius. Increase in die angle, increase in die opening or decrease in punch radius decreases the bend force. The clad sheet thickens at Al/Cu setting condition whereas it thins at Cu/Al setting condition. This thinning or thickening of the sheet influences the springback and bend force.