Impact of Machining and Phase Composition Change of Titanium Alloyed with Molybdenum

The titanium samples alloyed with molybdenum and aluminum are used to conduct full high-precision X-ray experiments enabling to determine the characteristic of the atomic interrelations - the unit cell dimension, and to establish the phase components of the doped single crystal. An orthorhombic phase is found, the volume of which increases after the deformation impact.

Oscillatory Changes in Structural Characteristics in Multicomponent Ceramics, YBCO

The structural characteristics of samples of a four-component superconducting material (YBCO) after exposure to X-ray irradiation during a long time are investigated. The effect of X-ray beam processing on angular positions (corresponding parameters of the crystal lattice) and the width of Bragg reflections is established. The phenomenon of oscillatory behavior in the unit cell dimension with long-time irradiation is found. The analysis of the profiles of reflection also demonstrates the presence of reversible changes phase composition with the exposure time. The observed phenomena reflect the presence of a nontrivial and specific process of compression and expansion of the unit cell due to the accumulation and then disengagement outside of ionized oxygen, which is formed under such irradiation exposure on the surface of the samples.

Multi-Band Polarization Insensitive Ultra-Thin THz Metamaterial Absorber for Imaging and EMI Shielding Applications

this article, a multi-band polarization-insensitive metamaterial absorber is designed for THz imaging and EMI shielding. A unique oval-shaped structure with three circular ring-shaped resonators is proposed with a unit cell dimension of36×36×19.6μm3. The absorbance of the proposed multiband MMA is 98.57%, 90%and 99.85% at 5.58, 7.98-8.84, 11.45THz frequency respectively. Return loss is nearly the same for the changing incident and polarization angle. Therefore, this metamaterial absorber with a wide range of polarization insensitivity is found and it is also suitable for quantum RADAR Imaging, energy harvesting, and optoelectronic devices.

Interdigital Coupled Compact FSS Reflector for UWB Antenna Gain Enhancement

A compact UWB FSS reflector is presented based on interdigital structure for gain enhancement of an UWB antenna. An equivalent circuit approach is proposed for the analysis of the FSS reflector. The reflector comprises a 6 × 6 array of unit cell dimension 6 mm × 6 mm and which is very compact. The reflector gives a linear phase response over UWB band. A UWB monopole antenna is designed with a half circular disc structure based on microstrip technology. A maximum of 5 dBi gain enhancement is achieved with this compact FSS reflector when placed at a distance below the antenna. The measured results closely follow the simulated ones which proves feasibility of this design.

A Compact Triple Band EBG Using Interdigital Coplanar Waveguide Structure for Antenna Gain Enhancement

A new triple band EBG unit cell with compact size has been designed, fabricated, and tested. The proposed EBG unit cell is based on a square mushroom-like EBG (M-EBG) structure with an interdigital coplanar waveguide (ICPW). With this technique, the size of the proposed ICPW-EBG structure has been reduced from λ/2 to λ/4 compared with the conventional M-EBG unit cell dimension, which is 18 × 18 mm2. The proposed unit cell was designed in order to respond for three frequency bands at 1.8 GHz, 2.45 GHz, and 3.7 GHz. An array of 10 × 10 unit cell was also designed as a reflector with an overall dimension of 181.8 × 181.8 mm2. The dipole antennas were implemented over the designed reflector with a short distance of λ/8 to radiate electromagnetic wave. The simulation results showed that the ICPW-EBG reflector can improve directivity of the dipole antenna to be 9.12 dB at 1.8 GHz, 9.02 dB at 2.45 GHz, and 8.40 dB at 3.7 GHz. The measurement directivities agreed well with simulation results including 8.72 dB at 1.8 GHz, 8.56 dB at 2.4 GHz, and 8.1 dB at 3.7 GHz. This is the first design of triple band EBG unit cell with 50% size reduction compared with the conventional structure at the same frequency. The designed ICPW-EBG reflector with dipole antenna results in the triple band operation, low-profile and high gain suitable for modern wireless communication systems.

Polarization independent bandstop frequency selective surface for X-band application

Purpose A novel low profile frequency selective surface (FSS) with a band-stop response at 10 GHz is demonstrated. The purpose of this designed FSS structure is to reject the X-band (8-12 GHz) for the application of shielding. The proposed FSS structure having the unit cell dimension of 8 × 8 mm2, the miniaturization of the FSS unit cell in terms of λ0 is 0.266 λ0 × 0.266 λ0, where λ0 is free space wavelength. The designed FSS provides 4 GHz bandwidth with insertion loss of 15 dB. The transverse electric (TE) and transverse magnetic (TM) modes of the proposed design are same because of polarization independent characteristics and hold the angularly stable frequency response for both TE and TM mode polarization. Both the simulation and measurement results are in good agreement to each other. Design/methodology/approach The proposed FSS design contains square-shaped PEC material, which is placed on the substrate and the shape of the circle and rectangle is etched over the PEC material. The PEC material of the patch dimension is 0.0175 mm. The substrate used for the proposed design is FR4 lossy with the thickness of 0.8 mm and permittivity εr = 4.3 having a loss tangent of 0.02. Findings To find a new design and miniaturized FSS structure is discussed. Originality/value 100%

An empirical assessment of two-dimensional (2D) Debye–Scherrer-type image-plate X-ray diffraction data collapsed into a 1D diffractogram

X-ray diffraction (XRD) has been routinely employed in the Earth sciences to characterize the crystallography of rocks and minerals. Routine characterization of samples too small for analysis by classic automated powder diffraction methods becomes challenging without access to single crystal or micro-diffraction equipment. Here, we show that a traditional Gandolfi camera lined with an image-plate (IP) as the detection medium can return a fully quantitative diffraction pattern from a sub-milligram single grain specimen in a simple and straightforward manner. Data pertaining to peak positions (d-spacings) were assessed using SRM640c Si powder, while intensity data were compared to the certified values for intensity standard SRM676a alumina powder. The refined unit-cell dimension of Si powder differed from the certified value of 5.4312 Å by no more than 0.0003 Å with a standard deviation (σ) of 0.0002 Å among the three experiments. For intensity, the σ and disparity from the certified values of three diffraction experiments on SRM676a were both <2%. The results of a comparative study of the crystallographic parameters determined for a naturally occurring garnet and clinopyroxene given through the refinement of their crystal structure by single-crystal XRD method are presented. These show through Rietveld refinement of X-ray data obtained by the Gandolfi–IP method outlined here that both accurate and precise XRD data can be produced in a timely and cost-effective manner using only an IP, Gandolfi camera, and software freely available on the internet.

Crystal structure and thermal expansion of Mn1−xFexGe

A series of temperature-dependent single-crystal and powder diffraction experiments has been carried out using synchrotron radiation in order to characterize the monogermanides of Mn, Fe and their solid solutions. The MnGe single crystal is found to be enantiopure and we report the absolute structure determination. The thermal expansion, parametrized with the Debye model, is discussed from the temperature-dependent powder diffraction measurements for Mn1−xFexGe (x= 0, 0.1, 0.2, 0.25, 0.3, 0.4, 0.5, 0.6, 0.7, 0.75, 0.8, 0.9). Whereas the unit-cell dimension and the Debye temperature follow a linear trend as a function of composition, the thermal expansion coefficient deviates from linear dependence with increasing Mn content. No structural phase transformations have been observed for any composition in the temperature range 80–500 K for both single-crystal and powder diffraction, indicating that the phase transition previously observed with neutron powder diffraction most probably has a magnetic origin.