sensor response
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Author(s):  
Fabiola Bravo-Hualpa ◽  
Jorge Nelson Trevejo-Pinedo ◽  
Karinna Visurraga ◽  
Angela Pinedo ◽  
Kevin Acuna-Condori ◽  
...  

Abstract There is great interest in the development of a simple system that could identify adulteration or counterfeiting of Peruvian Pisco (a grape-based alcoholic drink). In this study, sensors based on SnO2-TiO2 and SnO2-MoO3 composites with different weight composition ratios were synthesized and characterized. These sensors were tested with aqueous solutions of EtOH/MetOH and Pisco samples of Italia and Quebranta varieties in order to explore their capacity to identify variations in these beverages. The response profile of the most sensitive sensors showed an enhanced response to alcoholic samples with greater content of ethanol up to a concentration of 45%v/v, while the increased content of methanol in the range of 0.1 to 0.3 % v/v diminished the intensity of the sensor response. Differences in the composition of methanol and ethanol in the Pisco varieties studied (Italia and Quebranta) were correlated to the capacity of the composite-based sensors to differentiate them with greater performance. Sensors based on SnO2-TiO2-1/2 composites showed greater reproducibility of their response profile over time in comparison to SnO2-TiO2-1/1 and SnO2-MoO3 composites. The PCA showed that composite sensors were able to differentiate Pisco samples according to their variety.


Chemosensors ◽  
2021 ◽  
Vol 10 (1) ◽  
pp. 11
Author(s):  
Azhar Ali Haidry ◽  
Qawareer Fatima ◽  
Ahmar Mehmood ◽  
Asim Shahzad ◽  
Yinwen Ji ◽  
...  

Metal oxides are excellent candidates for the detection of various gases; however, the issues such as the limited operating temperature and selectivity are the most important ones requiring the comprehensive understanding of gas adsorption kinetics on the sensing layer surfaces. To this context, the present study focuses mainly on the fabrication of a Pt/Cr-TiO2/Pt type sensor structure that is highly suitable in reducing the operating temperature (from 400 to 200 °C), extending the lower limit NO2 gas concentration (below 10 ppm) with fast response (37 s) and recovery (24 s) times. This illustrates that the sensor performance is not only solely dependent on the nature of sensing material, but also, it is significantly enhanced by using such a new kind of electrode geometry. Moreover, Cr doping into TiO2 culminates in altering the sensor response from n- to p-type and thus contributes to sensor performance enhancement by detecting low NO2 concentrations selectively at reduced operating temperatures. In addition, the NO2 surface adsorption kinetics are studied by fitting the obtained sensor response curves with Elovich, inter-particle diffusion, and pseudo first-order and pseudo second-order adsorption models. It is found that a pseudo first-order reaction model describes the best NO2 adsorption kinetics toward 7–170 ppm NO2 gas at 200 °C. Finally, the sensing mechanism is discussed on the basis of the obtained results.


Micromachines ◽  
2021 ◽  
Vol 13 (1) ◽  
pp. 26
Author(s):  
Pawan Pathak ◽  
Hyoung Jin Cho

A layer of self-assembled 1-octadecanethiol was used to fabricate a palladium (Pd)/zinc oxide (ZnO) nanoparticle-based flexible hydrogen sensor with enhanced response and high selectivity at room temperature. A palladium film was first deposited using DC sputtering technique and later annealed to form palladium nanoparticles. The formation of uniform, surfactant-free palladium nanoparticles contributed to improved sensor response towards hydrogen gas at room temperature. The obtained sensor response was higher than for previously reported room temperature Pd/ZnO sensors. Furthermore, the use of the polymer membrane suppressed the sensor’s response to methane, moisture, ethanol, and acetone, resulting in the selective detection of hydrogen in the presence of the common interfering species. This study shows a viable low-cost fabrication pathway for highly selective room temperature flexible hydrogen sensors for hydrogen-powered vehicles and other clean energy applications.


Sensor Review ◽  
2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Marta Dmitrzak ◽  
Pawel Kalinowski ◽  
Piotr Jasinski ◽  
Grzegorz Jasinski

Purpose Amperometric gas sensors are commonly used in air quality monitoring in long-term measurements. Baseline shift of sensor responses and power failure may occur over time, which is an obstacle for reliable operation of the entire system. The purpose of this study is to check the possibility of using PCA method to detect defected samples, identify faulty sensor and correct the responses of the sensor identified as faulty. Design/methodology/approach In this work, the authors present the results obtained with six amperometric sensors. An array of sensors was exposed to sulfur dioxide at the following concentrations: 0 ppm (synthetic air), 50 ppb, 100 ppb, 250 ppb, 500 ppb and 1000 ppb. The damage simulation consisted in adding to the sensor response a value of 0.05 and 0.1 µA and replacing the responses of one of sensors with a constant value of 0 and 0.15 µA. Sensor validity index was used to identify a damaged sensor in the matrix, and its responses were corrected via iteration method. Findings The results show that the methods used in this work can be potentially applied to detect faulty sensor responses. In the case of simulation of damage by baseline shift, it was possible to achieve 100% accuracy in damage detection and identification of the damaged sensor. The method was not very successful in simulating faults by replacing the sensor response with a value of 0 µA, due to the fact that the sensors mostly gave responses close to 0 µA, as long as they did not detect SO2 concentrations below 250 ppb and the failure was treated as a correct response. Originality/value This work was inspired by methods of simulating the most common failures that occurs in amperometric gas sensors. For this purpose, simulations of the baseline shift and faults related to a power failure or a decrease in sensitivity were performed.


Nanomaterials ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 3151
Author(s):  
Aninamol Ani ◽  
P. Poornesh ◽  
Albin Antony ◽  
K. K. Nagaraja ◽  
Ashok Rao ◽  
...  

In the present investigation, electron beam-influenced modifications on the CO gas sensing properties of indium doped ZnO (IZO) thin films were reported. Dose rates of 5, 10, and 15 kGy were irradiated to the IZO nano films while maintaining the In doping concentration to be 15 wt%. The wurtzite structure of IZO films is observed from XRD studies post electron beam irradiation, confirming structural stability, even in the intense radiation environment. The surface morphological studies by SEM confirms the granular structure with distinct and sharp grain boundaries for 5 kGy and 10 kGy irradiated films whereas the IZO film irradiated at 15 kGy shows the deterioration of defined grains. The presence of defects viz oxygen vacancies, interstitials are recorded from room temperature photoluminescence (RTPL) studies. The CO gas sensing estimations were executed at an optimized operating temperature of 300 °C for 1 ppm, 2 ppm, 3 ppm, 4 ppm, and 5 ppm. The 10 kGy treated IZO film displayed an enhanced sensor response of 2.61 towards low concentrations of 1 ppm and 4.35 towards 5 ppm. The enhancement in sensor response after irradiation is assigned to the growth in oxygen vacancies and well-defined grain boundaries since the former and latter act as vital adsorption locations for the CO gas.


2021 ◽  
Vol 2021 (29) ◽  
pp. 111-117
Author(s):  
Peter Morovič ◽  
Ján Morovič

It is well known that color formation acts as a noise-reducing lossy compression mechanism that results in ambiguity, known as metamerism. Surfaces that match under one set of conditions-an illuminant and observer or capture device-can mismatch under others. The phenomenon has been studied extensively in the past, leading to important results like metamer mismatch volumes, color correction, reflectance estimation and the computation of metamer sets-sets of all possible reflectances that could result in a given sensor response. However, most of these approaches have three limitations: first, they simplify the problem and make assumptions about what reflectances can look like (i.e., being smooth, natural, residing in a subspace based on some measured data), second, they deal with strict mathematical metamerism and overlook noise or precision, and third, only isolated responses are considered without taking the context of a response into account. In this paper we address these limitations by outlining an approach that allows for the robust computation of approximate unconstrained metamer sets and exact unconstrained paramer sets. The notion of spatial or relational paramer sets that take neighboring responses into account, and applications to illuminant estimation and color constancy are also briefly discussed.


2021 ◽  
Vol 11 (20) ◽  
pp. 9676
Author(s):  
Raju Sapkota ◽  
Pengjun Duan ◽  
Tanay Kumar ◽  
Anusha Venkataraman ◽  
Chris Papadopoulos

Planetary ball-milled zinc oxide (ZnO) nanoparticle suspensions (nanoinks) were used to produce thin film chemiresistive gas sensors that operate at room temperature. By varying milling or grinding parameters (speed, time, and solvent) different thin film gas sensors with tunable particle sizes and porosity were fabricated and tested with dry air/oxygen against hydrogen, argon, and methane target species, in addition to relative humidity, under ambient light conditions. Grinding speeds of up to 1000 rpm produced particle sizes and RMS thin film roughness below 100 nm, as measured by atomic force and scanning electron microscopy. Raman spectroscopy, photoluminescence, and X-ray analysis confirmed the purity and structure of the resulting ZnO nanoparticles. Gas sensor response at room temperature was found to peak for nanoinks milled at 400 rpm and for 30 min in ethylene glycol and deionized water, which could be correlated to an increased film porosity and enhanced variation in electron concentration resulting from adsorption/desorption of oxygen ions on the surfaces of ZnO nanoparticles. Sensor response and dynamic behavior was found to improve as the temperature was increased, peaking between 100 and 150 °C. This work demonstrates the use of low-cost PBM nanoinks as the active materials for solution-processed thin film gas/humidity sensors for use in environmental, medical, food packaging, laboratory, and industrial applications.


Nanomaterials ◽  
2021 ◽  
Vol 11 (10) ◽  
pp. 2598
Author(s):  
Dana Miu ◽  
Izabela Constantinoiu ◽  
Cornelia Enache ◽  
Cristian Viespe

Laser deposition was used to obtain Pd/ZnO bilayers, which were used as sensing layers in surface acoustic wave (SAW) sensors. The effect of laser deposition parameters such as deposition pressure, laser energy per pulse, laser wavelength or pulse duration on the porosity of the Pd and ZnO films used in the sensors was studied. The effect of the morphology of the Pd and ZnO components on the sensor response to hydrogen was assessed. Deposition conditions producing more porous films lead to a larger sensor response. The morphology of the ZnO component of the bilayer is decisive and has an influence on the sensor properties in the same order of magnitude as the use of a bilayer instead of a single Pd or ZnO layer. The effect of the Pd film morphology is considerably smaller than that of ZnO, probably due to its smaller thickness. This has implications in other bilayer material combinations used in such sensors and for other types of analytes.


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