Fabrication of Porous Crystalline PLGA-PEG Induced by Swelling during the Recrystallization Annealing Process

Author(s):  
Jidong Dai ◽  
Xin Tan ◽  
Min Liang ◽  
Dandan Wei ◽  
Yinhua Tao ◽  
...  
2011 ◽  
Vol 181-182 ◽  
pp. 156-160
Author(s):  
Jin Ze Li ◽  
Hai Long Zhang ◽  
Zhi Hong Li

More detailed analysis of chemical compositions, cold plastic deformation and microstructure and properties change of 40Mn and 65Mn steel in recrystallization annealing process were made in the paper. How to get high plasticity and improve the performance of cold pressure processing technology as to cold-rolled 40Mn, 65Mn steel in recrystallization annealing technology, it was suggested that hardness was appropriately sacrificed to ensure the high plasticity. The paper analyzed concretely the reason of the influence of ball Fe3C to plasticity. Recrystallization annealing process and metallographic structure analysis were made. Basically set the process of 40Mn and 65Mn steel recrystallization annealing. Initially carry out the practical application, receive a better effect and have more potential applications foreground.


2013 ◽  
Vol 873 ◽  
pp. 42-47
Author(s):  
Zheng Bing Meng ◽  
Lang He ◽  
Guang Liang Wu ◽  
Xin Bin Liu ◽  
Chao Yang Zhou

The variation of microstructure of Ti-IF steel of extra deep drawing grade, which having a 83%cold-rolled deformation under simulated batch annealing process at temperature ranging from 480°C to 750°C, was studied by using optical microscopy, X-ray diffraction (XRD) and metallographic micro-hardness tester. The evolution of texture during the recrystallization process was analyzed by Orientation Density Function (ODF). The results show that, the recrystallization temperature of experimental steel is 620-630°C, and the recrystallization process can be accomplished within 1h at660°C. Four major textures after cold rolling are observed as follows,{001}<110>, {111}<110>, {111}<112> and {112}<110>, respectively. At the early stage of recrystallization annealing, texture evolves from {111} toγ-{111}, which is quite beneficial to achieve high deep drawing performance,the texture {001}<110> and {112}<110> change marginally. as the annealing temperature rises up to 720°C, texture {001}<110> and {112}<110> change into fiber textureγ-{111}. After annealing,{111}<112> and {111}<110> textures become the two main types.


2020 ◽  
Vol 4 (2) ◽  
pp. 48-55
Author(s):  
A. S. Jamaludin ◽  
M. N. M. Razali ◽  
N. Jasman ◽  
A. N. A. Ghafar ◽  
M. A. Hadi

The gripper is the most important part in an industrial robot. It is related with the environment around the robot. Today, the industrial robot grippers have to be tuned and custom made for each application by engineers, by searching to get the desired repeatability and behaviour. Vacuum suction is one of the grippers in Watch Case Press Production (WCPP) and a mechanism to improve the efficiency of the manufacturing procedure. Pick and place are the important process for the annealing process. Thus, by implementing vacuum suction gripper, the process of pick and place can be improved. The purpose of vacuum gripper other than design vacuum suction mechanism is to compare the effectiveness of vacuum suction gripper with the conventional pick and place gripper. Vacuum suction gripper is a mechanism to transport part and which later sequencing, eliminating and reducing the activities required to complete the process. Throughout this study, the process pick and place became more effective, the impact on the production of annealing process is faster. The vacuum suction gripper can pick all part at the production which will lower the loss of the productivity. In conclusion, vacuum suction gripper reduces the cycle time about 20%. Vacuum suction gripper can help lower the cycle time of a machine and allow more frequent process in order to increase the production flexibility.


2019 ◽  
Vol 85 (5) ◽  
pp. 28-32
Author(s):  
A. S. Kolyanova ◽  
Y. N. Yaltsev

A calculation method for obtaining the misorientation distribution function (MDF) for cubic crystals which can be used to estimate the presence or absence of special boundaries in the materials is presented. The calculation was carried out for two samples of Al-Mg-Si alloy subjected to various mechanical and thermal treatments: the first sample is subjected to rolling; the second sample is subjected to recrystallization annealing. MDF is calculated for each sample; the results are presented in the Euler space and in the angle-axis space. The novelty of the method consists in the possibility of gaining data on the grain boundaries from X-ray texture analysis without using electron microscopy. A calculation involving only mathematical operations on matrices was performed on the basis of the orientation distribution function restored from incomplete pole figures. It is shown that no special boundaries are observed in the deformed sample, whereas in the recrystallized alloy, special boundaries are detected at Ʃ = 23, 13, and 17. The shortcoming of the proposed method can be attributed to the lack of accurate data on grain boundaries, since all possible orientation in the polycrystal should be taken into account in MDF calculation.


2021 ◽  
Vol 64 (6) ◽  
Author(s):  
Zhiqiang Cao ◽  
Yiming Wei ◽  
Wenjing Chen ◽  
Shaohua Yan ◽  
Lin Lin ◽  
...  

Nanomaterials ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 131
Author(s):  
Tingting Xiao ◽  
Qi Yang ◽  
Jian Yu ◽  
Zhengwei Xiong ◽  
Weidong Wu

FePt nanoparticles (NPs) were embedded into a single-crystal MgO host by pulsed laser deposition (PLD). It was found that its phase, microstructures and physical properties were strongly dependent on annealing conditions. Annealing induced a remarkable morphology variation in order to decrease its total free energy. H2/Ar (95% Ar + 5% H2) significantly improved the L10 ordering of FePt NPs, making magnetic coercivity reach 37 KOe at room temperature. However, the samples annealing at H2/Ar, O2, and vacuum all showed the presence of iron oxide even with the coverage of MgO. MgO matrix could restrain the particles’ coalescence effectively but can hardly avoid the oxidation of Fe since it is extremely sensitive to oxygen under the high-temperature annealing process. This study demonstrated that it is essential to anneal FePt in a high-purity reducing or ultra-high vacuum atmosphere in order to eliminate the influence of oxygen.


Author(s):  
Tuan Van Nguyen ◽  
Kim Anh Huynh ◽  
Quyet Van Le ◽  
Hayeong Kim ◽  
Sang Hyun Ahn ◽  
...  

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Jeongpil Kim ◽  
Jeong-Hyun Eum ◽  
Junhyeok Kang ◽  
Ohchan Kwon ◽  
Hansung Kim ◽  
...  

AbstractHerein, we introduce a simple method to prepare hierarchical graphene with a tunable pore structure by activating graphene oxide (GO) with a two-step thermal annealing process. First, GO was treated at 600 °C by rapid thermal annealing in air, followed by subsequent thermal annealing in N2. The prepared graphene powder comprised abundant slit nanopores and micropores, showing a large specific surface area of 653.2 m2/g with a microporous surface area of 367.2 m2/g under optimized conditions. The pore structure was easily tunable by controlling the oxidation degree of GO and by the second annealing process. When the graphene powder was used as the supercapacitor electrode, a specific capacitance of 372.1 F/g was achieved at 0.5 A/g in 1 M H2SO4 electrolyte, which is a significantly enhanced value compared to that obtained using activated carbon and commercial reduced GO. The performance of the supercapacitor was highly stable, showing 103.8% retention of specific capacitance after 10,000 cycles at 10 A/g. The influence of pore structure on the supercapacitor performance was systematically investigated by varying the ratio of micro- and external surface areas of graphene.


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