Effects of Microstructural Anisotropy on Fracture Behavior of Heat-Pressed Glass-Ceramics and Glass-Infiltrated Alumina Composites for Dental Restorations

2009 ◽  
pp. 77-88
Author(s):  
Humberto N. Yoshimura ◽  
Carla C. Gonzaga ◽  
Paulo F. Cesar ◽  
Walter G. Miranda
Keyword(s):  
Fracture Behavior ◽  
Glass Ceramics ◽  
Dental Restorations ◽  
Alumina Composites ◽  
Microstructural Anisotropy

scholarly journals Mechanical Properties of CaO–Al2O3–SiO2 Glass-Ceramics Precipitating Hexagonal CaAl2Si2O8 Crystals

Crystals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 393
Author(s):  
Kei Maeda ◽  
Kosho Akatsuka ◽  
Gaku Okuma ◽  
Atsuo Yasumori
Keyword(s):  
Fracture Toughness ◽  
Liquidus Temperature ◽  
Fracture Behavior ◽  
Glass Ceramics ◽  
High Fracture Toughness ◽  
Flexural Test ◽  
Toughening Mechanism ◽  
High Fracture ◽  
X Ray ◽  
Microcrack Toughening

Fracture behavior via a flexural test for a newly found CaO–Al2O3–SiO2 (CAS) glass-ceramic (GC) was compared with that of enstatite GC and mica GC, which are well-known GCs with high-fracture toughness and machinability, respectively. By focusing on the nonelastic load–displacement curves, CAS GC was characterized as a less brittle material similar to machinable mica GC, compared with enstatite GC, which showed higher fracture toughness, KIC. The microcrack toughening mechanism in CAS GC was supported by the nondestructive observation of microcracks around the Vickers indentation using the X-ray microcomputed tomography technique. The CAS GC also showed higher transparency than mica GC due to its low crystallinity. Moreover, the precursor glass had easy formability due to its low-liquidus temperature.

Novel Glass-Ceramics for Dental Application by Sol Gel Technique

2008 ◽  
Vol 396-398 ◽  
pp. 153-156 ◽  
Author(s):  
Xanthippi Chatzistavrou ◽  
E. Hatzistavrou ◽  
Nikolaos Kantiranis ◽  
Lambrini Papadopoulou ◽  
Eleana Kontonasaki ◽  
...  
Keyword(s):  
Glass Ceramic ◽  
Preparation Method ◽  
Sol Gel ◽  
Glass Ceramics ◽  
Dental Restorations ◽  
Gel Technique ◽  
Gel Preparation ◽  
Dental Applications ◽  
Potential Use

The aim of this study was the fabrication using a sol-gel technique of a new glass-ceramic with potential use in dental applications. The characterization of the composition and microstructural properties of the produced material confirmed the similarity between the new sol-gel derived glass-ceramic and a commercial leucite based fluorapatite dental glass-ceramic. The produced material has potential application in dental restorations and it is expected to exhibit better control of composition, microstructure and properties due to the intrinsic advantages of the sol-gel preparation method.

Effect of crystal size on the tribological properties of lithium disilicate glass-ceramics sliding against alumina and tungsten carbide spheres

2020 ◽  
Vol 72 (9) ◽  
pp. 1109-1116
Author(s):  
Crislaine da Cruz ◽  
Ivan Mathias ◽  
Mariza Veiga Senk ◽  
Gelson Biscaia de Souza ◽  
Francisco Carlos Serbena
Keyword(s):  
Wear Rate ◽  
Coefficient Of Friction ◽  
Glass Ceramic ◽  
Crystal Size ◽  
Glass Ceramics ◽  
Stationary Regime ◽  
Content Type ◽  
Dental Restorations ◽  
The Coefficient Of Friction ◽  
Dental Prosthetics

Purpose Lithium disilicate glass-ceramics (LS2 GC) are widely used as dental prosthetics and dental restorations. Based LS2 GC have hardness and translucency similar to that of natural teeth. This study aims to investigate the tribological features of LS2 GC with crystalline volume fraction of 64% and different crystal sizes from 8 µm to 34 µm for different counterparts. Design/methodology/approach The tribological behavior was investigated using a pin-on-disc tribometer with alumina and tungsten carbide (WC) spheres, applied load of 5 N and sliding speed of 5 cm/s at normal conditions. The coefficient of friction was measured continuously up to 10,000 sliding cycles. The specific wear rate was calculated from tribological and profile measurements. The wear mechanism was investigated by surface morphology analysis. Findings The coefficient of friction during running-in varied from 0.8 to 1.0 for the alumina counterpart, because of severe wear. Afterwards, it reduced and reached a stationary regime, characterized by a mild wear regime and the formation of a tribolayer formed by the debris. For the WC counterpart, the coefficient of friction curves increased initially with sliding cycles up to a stationary regime. The samples tested against WC presented the lowest specific wear rate (k), and no variation of wear rate with crystal size was observed. For samples tested against the alumina, crystallization and crystal size increased the wear resistance. Originality/value This study evaluated the effect of different counterfaces on the tribological properties of the LS2 GC, an important glass-ceramic base for many dental prosthetics and dental restorations, discussing results in light of the contact mechanics. Different specific wear rates, wear regimes and dependence on the glass-ceramic microstructure were observed depending on the counterpart. Peer review The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-08-2019-0352/

Zirconia Dental Implant Materials

2017 ◽  
Vol 907 ◽  
pp. 99-103
Author(s):  
Sergiu Ciprian Focșăneanu ◽  
Petrică Vizureanu ◽  
Andrei Victor Sandu ◽  
Mădălina Simona Bălţatu
Keyword(s):  
Mechanical Properties ◽  
Mechanical Strength ◽  
Dental Implants ◽  
Clinical Studies ◽  
Glass Ceramics ◽  
Ceramic Materials ◽  
Medical Applications ◽  
Dental Restorations ◽  
Esthetic Dentistry ◽  
Titanium Dental Implants

Ceramic materials are used for the fabrication of dental restorations respectively esthetic dentistry. The main ceramic materials are glass ceramics, spinel, alumina and zirconia. Zirconia was introduced into dentistry domain in the 1990s used like frameworks, implants, dowels, abutments and orthodontic brackets. Recently, zirconia materials are getting much attention for dental implants because of its toothlike color, mechanical properties, good corrosion and biocompatibility. This article presents an review of zirconia dental implants osseointegration and mechanical strength compared with other dental implants. Clinical studies published indicate that zirconia dental implants have the potential to become alternative of titanium dental implants used in medical applications.

scholarly journals Machinability of Zirconia Toughened Mica Glass Ceramics for Dental Restorations

2020 ◽  
Vol 24 (1) ◽  
Author(s):  
Sivaranjani Gali ◽  
Suresh Chiru
Keyword(s):  
Surface Roughness ◽  
Tool Wear ◽  
Feed Rate ◽  
Cutting Forces ◽  
Glass Ceramics ◽  
Spindle Speed ◽  
Depth Of Cut ◽  
Dental Ceramics ◽  
Edge Chipping ◽  
Dental Restorations

Objective: For a dental material to be machinable for CAD/CAM technology, it must offer convenient machining, under a given set of cutting conditions. Quantitative evaluation of machinability has been assessed in literature through various parameters such as tool wear, penetration rates, surface roughness, cutting force and power. A machinable ceramic will typically demonstrate a higher tool penetration rate with signs of reduced diamond tool wear and edge chipping. The purpose of this in vitro study was to evaluate the feasibility of machining an experimental ceramic, 20 wt.% zirconia reinforced mica glass ceramics (G20Z) for indirect dental restorations and compare the tool penetration rates of G20Z to commercially available dental ceramics, Presintered Zirconia (PSZ) and IPS emax CAD. Material and Methods:  Precursors of base glass (SiO2 -Al2O3 -K2O -MgO-B2O3 -F) were melted at 15000C for 2 h in a platinum crucible and quenched in deionised water. The glass frit was ball milled with 20 wt. % YSZ (G20Z) and subject to two stage heat treatment in a muffle furnace. Specimens of G20Z (12 X 2 mm) were evaluated for their feasibility of machining under varying spindle speed, depth of cut, and feed rates. Influence of depth of cut, spindle speed and feed rate (vc=8000-16000 rpm, d=0.4-0.8 mm, f=0.1- 0.3 mm/tooth) on cutting forces, material response, surface roughness and tool wear were investigated. Tool penetration rates, tool wear and margin chipping were also evaluated and compared with Pre-sintered Zirconia (PSZ)  and e.max CAD in a custom dental milling surveyor at 30,000 rpm with a load of 0.98 N under water lubrication for 6 min. Tool penetration rates were calculated as the ratio of length of cut and milling time with a measuring microscope and scanning electron microscope was used for tool wear and edge chipping. ANOVA and Tukey Kramer tests were used for statistically comparing the means of each group. Results: Spindle speed and feed rate play a significant role in influencing surface roughness, thrust force, cutting forces and tool wear. Penetration rates of G20Z (0.32 ±0.12 mm/min) was significantly greater than PSZ (0.26 ±0.06 mm/min) and IPS e.max CAD (0.21 ±0.05 mm/min). SEM observations reveal tool abrasion and edge chipping regardless of the ceramic type. Conclusion: High spindle speeds delivers low cutting forces with an average surface roughness of 1.61 µm, with abrasive wear of the tool insert and brittle fracture of zirconia mica glass ceramic composites. G20Z with its machinable nature demonstrates greater tool penetration rates than PSZ and IPS e.max CAD. Tool wear and edge chipping is seen in all the investigated ceramics.   Keywords Machinability, Dental Ceramics, Mica Glass-Ceramics, Dental Zirconia, Tool penetration rates.  

Study of Machinable Dental Glass Ceramics

2009 ◽  
Vol 620-622 ◽  
pp. 575-578 ◽  
Author(s):  
Xin Pei Ma ◽  
Guang Xin Li ◽  
Zhi Hao Jin ◽  
Ji Hua Chen ◽  
Mao Ju Yang ◽  
...  
Keyword(s):  
Glass Ceramics ◽  
Orthogonal Experimental Design ◽  
Computer Assisted ◽  
X Ray Diffraction ◽  
X Ray ◽  
Dental Restorations ◽  
Computer Assisted Design ◽  
All Ceramic ◽  
Cad Cam ◽  
Good Biocompatibility

Glass-ceramics are especially useful for the dental restorations because of their good biocompatibility, chemical stability, aesthetic, mechanical strength and wear resistance. The aim of this work was to obtain one mica glass-ceramic, which can be easily used for rapid machining into all-ceramic tooth with computer assisted design/computer assisted manufacture (CAD/CAM) devices. In the study, on the base of low melting machinable fluorosilicic mica glass ceramics, the effects of CeO2 and Fe2O3 in SiO2-B2O3-K2O-Na2O-Li2O-Al2O3-MgO-F system on color were studied. By orthogonal experimental design, the effects of crystallized parameters on the color, three point flexural strength and machinability of the glass ceramics were obtained, and the samples were analyzed by differential thermal analysis(DTA), X-ray diffraction (XRD) and scanning electron microscopy(SEM), respectively. Experimental results showed that the glass-ceramics with color close to the tooth can be obtained by adjusting the percentage of CeO2 and Fe2O3, and the glass-ceramics crystallized at 680°C for 2h have excellent mechanical properties and machinability.

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