Analysis of the moisture evaporation process during vacuum freeze-drying of koumiss and shubat

2016 ◽  
Vol 53 (5) ◽  
pp. 1571-1578 ◽  
Author(s):  
Azret Utebaevich Shingisov ◽  
Ravshanbek Sultanbekovich Alibekov
Keyword(s):  
Freeze Drying ◽  
Evaporation Process ◽  
Moisture Evaporation

scholarly journals Coal Moisture Variations in Response to Rainfall Events in Mine and Coal-Fired Power Plant Stockpiles—Part 2: Evaporation

Minerals ◽  
2021 ◽  
Vol 11 (12) ◽  
pp. 1366
Author(s):  
Quentin Peter Campbell ◽  
Marco le Roux ◽  
Fardis Nakhaei
Keyword(s):  
Laboratory Experiments ◽  
Evaporation Process ◽  
Ambient Conditions ◽  
Moisture Evaporation ◽  
Rainfall Events ◽  
Heating Value ◽  
Surface Evaporation ◽  
Fine Coal ◽  
Coal Beds ◽  
Rate Of Evaporation

Additional moisture added in coal stockpiles due to rain and other climatic processes causes a significant problem worldwide, which leads to not only decrease in the heating value of the coal but also creates an extra efficiency penalty. Therefore, it is important to make some predictions for control of coal moisture within stockpiles after the rainfall. When the rain falls on the stockpile, it either runs off the surface or infiltrates the stockpile. The infiltrated water may evaporate from the surface, drain or stay within the stockpile. The aims of this study (parts 1 and 2) are to describe and compare the changes in coal moisture content following rainfall events. The mechanisms of runoff, infiltration and drainage after rainfall were described in the first paper of this series. In part 2 the influence of coal particle size and ambient conditions on the rate and depth of moisture evaporation within the stockpile is investigated. The laboratory experiments showed cyclic events of adsorbing moisture overnight and desorbing this moisture during the day as part of the coal surface evaporation process. The rate of evaporation from the surface of the fine coal stockpile was faster than the coarse stockpile; however, the coarse stockpile experienced a more efficient evaporation process because of its porous structure. Fine coal beds experienced evaporation only near the surface, while the maximum influencing layer of evaporation is a depth of 0.4 cm below the surface in coarse coal beds.

scholarly journals Effect Carrier Agent Formulation in Drying Rate and Antioxidant Activity of Roselle Extract

2018 ◽  
Vol 156 ◽  
pp. 02010
Author(s):  
Febiani Dwi Utari ◽  
Mohammad Djaeni ◽  
Wahyu Zuli Pratiwi ◽  
Muhammad Alver Syahputra ◽  
Uma Fadzilia Arifin
Keyword(s):  
Antioxidant Activity ◽  
Moisture Content ◽  
Nutritional Value ◽  
Drying Rate ◽  
Evaporation Process ◽  
Drying Process ◽  
Moisture Evaporation ◽  
Drying Temperature ◽  
Natural Colorant ◽  
Speed Up

Roselle (Hibiscus sabdarifa L) contains anthocyanins as the natural colorant and antioxidant. Drying the roselle extract was aims to produce the dry product that easy consumption as antioxidant. The carrier agent was added in roselle extract to improve the drying rate and maintain the nutritional value. This research studied the effect of carrier agent in drying rate and antioxidant activity. The method consists of two step involving roselle extraction using ultrasonic and the drying process. The roselle extraction by ultrasonic use the water as the solvent. The carrier agent (0%,5%,10% of maltodextrin) was added in roselle extract. The mixture was then dried in tray dryer dehumidification using zeolite in drying temperature 50,60, and 70⁰C. As the response, the moisture content was observed by gravimetry every 15 minutes for 150 minutes. The result showed that Page model was fitted to determine the constant of drying rate. Higher concentration of carrier agent enhanced the moisture evaporation process. Based on the DPPH analysis, the degradation of antioxidant activity in temperature 70⁰C was 2.14 times higher than in temperature 50⁰C. As the conclusion, addition of maltodextrin can speed up the drying process and retain the antioxidant activity of.

scholarly journals Experimental study of moisture evaporation process with different soil characteristics

2019 ◽  
Vol 7 (2) ◽  
pp. 78-83
Author(s):  
Ni An ◽  
Chao-Sheng Tang ◽  
Shi-Kang Xu ◽  
Xue-Peng Gong ◽  
Bin Shi ◽  
...  
Keyword(s):  
Experimental Study ◽  
Soil Characteristics ◽  
Evaporation Process ◽  
Moisture Evaporation

Ca-Histochemistry in slime mold plasmodia

1978 ◽  
Vol 36 (2) ◽  
pp. 130-131
Author(s):  
Ulrich Dierkes
Keyword(s):  
Physarum Polycephalum ◽  
Carbon Coating ◽  
Freeze Drying ◽  
Freeze Fracture ◽  
Freeze Substitution ◽  
Uranyl Acetate ◽  
Slime Mold ◽  
Staining Procedure ◽  
Protoplasmic Streaming ◽  
Intracellular Ca

Calcium is supposed to play an important role in the control of protoplasmic streaming in slime mold plasmodia. The motive force for protoplasmic streaming is generated by the interaction of actin and myosin. This contraction is supposed to be controlled by intracellular Ca-fluxes similar to the triggering system in skeleton muscle. The histochemical localisation of calcium however is problematic because of the possible diffusion artifacts especially in aquous media.To evaluate this problem calcium localisation was studied in small pieces of shock frozen (liquid propane at -189°C) plasmodial strands of Physarum polycephalum, which were further processed with 3 different methods: 1) freeze substitution in ethanol at -75°C, staining in 100% ethanol with 1% uranyl acetate, and embedding in styrene-methacrylate. For comparison the staining procedure was omitted in some preparations. 2)Freeze drying at about -95°C, followed by immersion with 100% ethanol containing 1% uranyl acetate, and embedding. 3) Freeze fracture, carbon coating and SEM investigation at temperatures below -100° C.

The Critical Point Drying Method Applied to Scanning Electron Microscopy of L-929 Cells

1970 ◽  
Vol 28 ◽  
pp. 278-279
Author(s):  
Charles TurnbiLL ◽  
Delbert E. Philpott
Keyword(s):  
Electron Microscopy ◽  
Carbon Dioxide ◽  
Surface Tension ◽  
Critical Point ◽  
Freeze Drying ◽  
Attractive Alternative ◽  
Crystal Formation ◽  
Critical Point Drying ◽  
Time Required ◽  
Scanning Electron

The advent of the scanning electron microscope (SCEM) has renewed interest in preparing specimens by avoiding the forces of surface tension. The present method of freeze drying by Boyde and Barger (1969) and Small and Marszalek (1969) does prevent surface tension but ice crystal formation and time required for pumping out the specimen to dryness has discouraged us. We believe an attractive alternative to freeze drying is the critical point method originated by Anderson (1951; for electron microscopy. He avoided surface tension effects during drying by first exchanging the specimen water with alcohol, amy L acetate and then with carbon dioxide. He then selected a specific temperature (36.5°C) and pressure (72 Atm.) at which carbon dioxide would pass from the liquid to the gaseous phase without the effect of surface tension This combination of temperature and, pressure is known as the "critical point" of the Liquid.

Preservation of Plant Cell Surfaces For Scanning Electron Microscopy

1973 ◽  
Vol 31 ◽  
pp. 472-473
Author(s):  
Linda M. Sicko ◽  
Thomas E. Jensen
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Critical Point ◽  
Filter Paper ◽  
Freeze Drying ◽  
Cell Surfaces ◽  
Air Drying ◽  
Popular Method ◽  
Critical Point Drying ◽  
Scanning Electron

The use of critical point drying is rapidly becoming a popular method of preparing biological samples for scanning electron microscopy. The procedure is rapid, and produces consistent results with a variety of samples. The preservation of surface details is much greater than that of air drying, and the procedure is less complicated than that of freeze drying. This paper will present results comparing conventional air-drying of plant specimens to critical point drying, both of fixed and unfixed material. The preservation of delicate structures which are easily damaged in processing and the use of filter paper as a vehicle for drying will be discussed.

Scanning Electron Microscopy-cuticular Lesions on the Roundworm Ascaris Suum

1970 ◽  
Vol 28 ◽  
pp. 114-115
Author(s):  
P. A. Madden ◽  
W. R. Anderson
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Freeze Drying ◽  
Room Temperature ◽  
Secondary Electron ◽  
Distilled Water ◽  
Freeze Dried ◽  
Silver Paint ◽  
To Come ◽  
Scanning Electron

The intestinal roundworm of swine is pinkish in color and about the diameter of a lead pencil. Adult worms, taken from parasitized swine, frequently were observed with macroscopic lesions on their cuticule. Those possessing such lesions were rinsed in distilled water, and cylindrical segments of the affected areas were removed. Some of the segments were fixed in buffered formalin before freeze-drying; others were freeze-dried immediately. Initially, specimens were quenched in liquid freon followed by immersion in liquid nitrogen. They were then placed in ampuoles in a freezer at −45C and sublimated by vacuum until dry. After the specimens appeared dry, the freezer was allowed to come to room temperature slowly while the vacuum was maintained. The dried specimens were attached to metal pegs with conductive silver paint and placed in a vacuum evaporator on a rotating tilting stage. They were then coated by evaporating an alloy of 20% palladium and 80% gold to a thickness of approximately 300 A°. The specimens were examined by secondary electron emmission in a scanning electron microscope.

Video real-time imaging of artificial membranes during freeze-drying by cryo-electron microscopy

1988 ◽  
Vol 46 ◽  
pp. 16-17
Author(s):  
Alan S. Rudolph ◽  
Ronald R. Price
Keyword(s):  
Real Time ◽  
Self Assembly ◽  
Freeze Drying ◽  
Video Capture ◽  
Drying Process ◽  
Artificial Membranes ◽  
The Past ◽  
Cryo Electron Microscopy ◽  
Spherical Structures ◽  
Capture Techniques

We have employed cryoelectron microscopy to visualize events that occur during the freeze-drying of artificial membranes by employing real time video capture techniques. Artificial membranes or liposomes which are spherical structures within internal aqueous space are stabilized by water which provides the driving force for spontaneous self-assembly of these structures. Previous assays of damage to these structures which are induced by freeze drying reveal that the two principal deleterious events that occur are 1) fusion of liposomes and 2) leakage of contents trapped within the liposome [1]. In the past the only way to access these events was to examine the liposomes following the dehydration event. This technique allows the event to be monitored in real time as the liposomes destabilize and as water is sublimed at cryo temperatures in the vacuum of the microscope. The method by which liposomes are compromised by freeze-drying are largely unknown. This technique has shown that cryo-protectants such as glycerol and carbohydrates are able to maintain liposomal structure throughout the drying process.

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