scholarly journals Effects of Different Extraction Solvents on Oil Extracted from Jatropha Seeds and the Potential of Seed Residues as a Heat Provider

2020 ◽  
Author(s):  
Yadessa Gonfa Keneni ◽  
Legesse Adane Bahiru ◽  
Jorge Mario Marchetti
Keyword(s):  
Seed Oil ◽  
Acid Value ◽  
Biodiesel Production ◽  
Seed Collection ◽  
Average Value ◽  
Jatropha Seeds ◽  
Jatropha Seed ◽  
Mixed Oil ◽  
Seed Collections

Abstract The present study focuses on the determination of oil contents of thirteen different jatropha seed collections from Ethiopia. The oil was extracted with a Soxhlet extractor using n-hexane which was selected out of four different solvents: diethyl ether, ethanol, n-heptane, and n-hexane. Cotton and thimble were used as filter for the extractions. Some properties of the oil of Chali seed collection and a sample of mixed oils (a mixture of equal volume of oils from thirteen different seed collections) were determined. The energy contents of selected de-oiled jatropha seed residues were also estimated. In the extraction with cotton and thimble, the largest percentage of oil yield was obtained from Dana seed (48.29%) and Chali seed (45.79) collections, respectively. The acid value (1.32 mg KOH/g) and percentage of free fatty acids (%FFA) (0.66%) of Chali seed oil were lower than the acid value (2.12 mg KOH/g) and %FFA (1.06%) of the mixed oil, and thus, the former oil is more suitable for alkaline-catalyzed biodiesel production. The iodine values of both Chali seed oil (116.02 g/100 g) and mixed oil (109.24 g/100 g) did not exceed the maximum standard for biodiesel according to the European EN 14214 specification, and the oils could be used for biodiesel production. The gross calorific values of de-oiled jatropha seed residues after oil extraction were found to range from 18.57 to 24.03 MJ/kg, and with the average value of 19.64 MJ/kg. Thus, the de-oiled seed residues can be used as the source of heat.

scholarly journals Physicochemical Characterization of Jatropha podagrica Seed Oil for Potential Biodiesel Production and other Industrial Applications in Thailand

2021 ◽  
Vol 50 (1) ◽  
pp. 85-92
Author(s):  
Duangporn Premjet ◽  
Abraham Kusi Obeng ◽  
Hah Young Yoo ◽  
Seung Wook Kim ◽  
Siripong Premjet
Keyword(s):  
Fatty Acid ◽  
Oil Content ◽  
Seed Oil ◽  
Physicochemical Characterization ◽  
Acid Value ◽  
Industrial Applications ◽  
Physicochemical Analysis ◽  
Biodiesel Production ◽  
Seed Kernel ◽  
Jatropha Seed

Jatropha is considered as one of the most promising potential oil sources for biodiesel production and other industrial applications. However, research on the potential of Jatropha seed oil is mainly focused on Jatropha curcas, with other species receiving little attention. The physicochemical properties of J. podagrica seed oil was studied to determine its potential as feedstock for biodiesel production and other industrial applications in Thailand. The seed oil was extracted with n-hexane from milled kernels using the soxhlet extractor and subsequently characterised for free fatty acids, iodine value, viscosity, saponification value, density, and acid value. The fatty acid profile of the seed oil was also analysed using gas chromatography (GC). Analysis of the physical properties of the J. podagrica seed kernel showed lower average physical characteristics when compared to those of J. curcas seed kernel. J. podagrica seeds had high oil content comparable to J. curcas oil content. The main fatty acid components of the seed oil were oleic acid (15%) and linoleic acid (70%). Generally, the results of the physicochemical analysis indicated that J. podagrica seed oil would be very useful for the production of soap and shampoo in Thailand. To produce biodiesel from the seed oil, a two-step acid-catalysed transesterification process would be appropriate.

scholarly journals Influence of Physicochemical Characteristics of Neem Seeds (Azadirachta indica A. Juss) on Biodiesel Production

Biomolecules ◽  
2020 ◽  
Vol 10 (4) ◽  
pp. 616
Author(s):  
Bakari Hamadou ◽  
Djomdi ◽  
Ruben Zieba Falama ◽  
Cedric Delattre ◽  
Guillaume Pierre ◽  
...  
Keyword(s):  
Seed Oil ◽  
Fatty Acid Content ◽  
Calorific Value ◽  
Acid Value ◽  
Physicochemical Characteristics ◽  
Biodiesel Production ◽  
Major Drawback ◽  
Neem Seed Oil ◽  
The City

The aim of this work is to study the influence of the physicochemical characteristics of neem seeds, according to their mass and oil content, on the production of biodiesel. After the physical characterization of the seeds and extraction of the oil (triglycerides), biodiesel was produced from crude neem seed oil by transesterification with ethanol in the presence of sodium hydroxide. This study shows that the physicochemical characteristics of these seeds vary according to the origin of the samples. The seeds from Zidim, with a mass average of 200 seeds evaluated at 141.36 g and an almond content of 40.70%, have better characteristics compared to those collected in the city of Maroua, with average values evaluated at 128.00 g and 36.05%, respectively. Almonds have an average lipid content of 53.98 and 56.75% for the Maroua and Zidim samples, respectively. This study also reveals that neem oil, by its physicochemical characteristics, has a satisfactory quality for a valorization in the production of biodiesel. However, its relatively high free fatty acid content is a major drawback, which leads to a low yield of biodiesel, evaluated on average at 89.02%, and requires a desacidification operation to improve this yield. The analysis of biodiesel indicates physicochemical characteristics close and comparable to those of petrodiesel, particularly in terms of calorific value, density, kinematic viscosity, acid value, evaluated at 41.00 MJ/kg, 0.803, 4.42 cSt, and 0.130 mg/g, respectively.

Determination of β -Sitosterol with Chemical Course and Material Applications in Jatropha Seed Oil by High Performance Liquid Chromatography

2012 ◽  
Vol 577 ◽  
pp. 69-72 ◽  
Author(s):  
Shu Yu Liu ◽  
Anaerguli Maihemuti
Keyword(s):  
High Performance Liquid Chromatography ◽  
Liquid Chromatography ◽  
High Performance ◽  
Seed Oil ◽  
Reversed Phase ◽  
Analytical Recovery ◽  
Relative Standard ◽  
The Mean ◽  
Jatropha Seed

A simple and rapid high performance liquid chromatography (HPLC) assay was developed to identify and measure theβ-sitosterol with chemical course and material applications in jatropha seed oil. The stigmasterol was isolated with a good selectivity by HPLC employing reversed phase C18 columns. The components were separated by mobile phase of methanol-water (99/1, v/v) and detected at 205nm. The quantitation of the stigmasterol was reproducible and the method relative standard deviation is 1.1%. The mean analytical recovery was 96.2%.

An Assessment of in vitro Antioxidant Potential of Camelina sativa L. Seed Oil and Estimation of Tocopherol Content using HPTLC Method

2021 ◽  
Vol 13 (2) ◽  
pp. 589-600
Author(s):  
R. Pathak ◽  
M. Mohsin ◽  
S. P. S Mehta
Keyword(s):  
Physicochemical Properties ◽  
Seed Oil ◽  
Acid Value ◽  
Tocopherol Content ◽  
Camelina Sativa ◽  
Biodiesel Production ◽  
Biofuel Production ◽  
Antioxidant Potential ◽  
Camelina Seed

The present study was aimed to analyze the physicochemical properties of Camelina sativa L. seed oil in order to identify its utilization as a primary feedstock for biofuel production. Efforts were also made to identify and quantify the amount of α- tocopherols in Camelina seed oil and evaluated in vitro antioxidant potential of Camelina sativa seed oil and were compared with α–tocopherol standard. Physicochemical properties such as oil yield content (36.66 %), less acid value (5.39 mg KOH/g) make it a prominent feedstock for biodiesel production.  Saponification value (182.66 mg KOH/g) also makes this oil useful in soap and cosmetic industries. To check in vitro antioxidant potential of Camelina seed oil H2O2, DPPH and ABTS were used as free radical inducers. Oil showed remarkable inhibition potential of trapping these free radicals. Tocopherol content was analyzed through HPTLC. Camelina sativa seed oil was found to contain 59.34 mg/100 g of tocopherol content. It is evident from this study that Camelina oil has high antioxidant potential and there is no need to add other antioxidant substances in the products formed by using Camelina sativa seed oil.

scholarly journals Potential Feedstock of Rubber Seed Oil for Biodiesel Production

2019 ◽  
Vol 7 (4.14) ◽  
pp. 196
Author(s):  
N. Hamzah ◽  
S. Mohd Isa ◽  
N. Ahmad Tajuddin
Keyword(s):  
Fossil Fuels ◽  
Seed Oil ◽  
Methyl Esters ◽  
Acid Value ◽  
Environmental Benefits ◽  
Biodiesel Production ◽  
Optimum Conditions ◽  
Rubber Seed Oil ◽  
Rubber Seed ◽  
Animal Fats

Biodiesel can help to reduce the world‘s dependence on fossil fuels and which also has significant environmental benefits. Biodiesel is a mixture of fatty acid methyl esters (FAME) obtained via transesterification of vegetable oils or animal fats with an alcohol. The rubber seed oil (RSO) is chosen as a potential non-edible vegetable oil for the production of biodiesel. The oil was extracted from the seed by using pressurized liquid extraction (ASE). The percentage rubber seed oil extracted from 2.6 kilograms rubber seed was obtained 35%. The acid value of RSO has reduced from 52.3 mg KOH/g to 0.8 mg KOH/g while FFA% value has reduced from 35% to 1.18% after acid esterification was applied to RSO. The oil was proceed with base transesterification where the triglycerides from the oil were converted into FAME. The optimization of transesterification process was performed in order to determine the optimum conditions that give the highest FAME yield. Result shows that optimum conditions of the transesterification of rubber seed oil were 1:6 of oil to methanol mass ratio ,30 wt% KOH catalyst, 60 oC reaction temperature and 60 minutes reaction time, that offering the highest biodiesel yield of 96%.   

scholarly journals Physiochemical properties of biodiesel produced from ogbono (Irvingia gabonesis) seed oil

Bio-Research ◽  
2021 ◽  
Vol 19 (1) ◽  
pp. 1210-1216
Author(s):  
Iklima Ibrahim Bandi ◽  
Shamsuddeen Yahaya ◽  
Hafsatu Buhari Bature ◽  
Musa Usman Dabai ◽  
Samira Shehu Adamu ◽  
...  
Keyword(s):  
Potassium Hydroxide ◽  
Fossil Fuels ◽  
Seed Oil ◽  
Acid Value ◽  
Biodiesel Production ◽  
Promising Alternative ◽  
Physiochemical Properties ◽  
Saponification Value ◽  
Astm D6751 ◽  
Significant Attention

Biodiesel is a promising alternative fuel and has gained significant attention due to the predicted depletion of conventional fossil fuels and environmental concerns. This study aims to produce biodiesel from ogbono seed oil (using 98 ml methanol and 2g potassium hydroxide (KOH) as a catalyst) via transesterification process and to determine the physiochemical properties of the biodiesel produced. The physiochemical properties of the feedstock (extracted ogbono seed oil) were also determined before the transesterification process. The physiochemical properties of the produced biodiesel showed that it has a density of 0.5±0.00 g/cm3, pour point of 2.0±0, saponification value of 58.90±0.06 mg KOH/g, ester value of 98.0±0.5% (m/m), iodine value of 26.64±0.15gI2/100g, acid value of 0.28±0.05 mgKOH/g, moisture value of 0.0006 ±0.0% and trace amounts of ash content. The results of the physiochemical properties of the produced biodiesel agree with ASTM-D6751 and EN 14214 standard. Thus, it was concluded that ogbono seed oil is an excellent feedstock for biodiesel production via base catalyzed transesterification process

scholarly journals Jatropha curcas seed tolerance to desiccation and storage at low temperatures

2019 ◽  
pp. 396
Author(s):  
Alessandra Olmo Dardengo ◽  
Henrique Duarte Vieira ◽  
Bruno Borges Deminicis ◽  
Pedro Amorim Berbert ◽  
Márcia Terezinha Ramos de Oliveira
Keyword(s):  
Low Temperatures ◽  
Seed Quality ◽  
Biodiesel Production ◽  
Quality Analysis ◽  
Physic Nut ◽  
Randomized Design ◽  
Completely Randomized Design ◽  
Jatropha Seeds ◽  
Jatropha Seed ◽  
And Storage

Jatropha seeds were classified according to tolerance to desiccation and storage, as a way to subsidize future propagation programs, as jatropha seed shows to be a promising oilseed for biodiesel production. The objective of this work was to study the physiological classification regarding the tolerance of physic nut seeds to desiccation and storage at low temperatures and to verify if their behavior was closer to that of seeds classified as orthodox, recalcitrant or intermediate. The seeds were harvested in the morning and sent to the Laboratory, being processed and submitted to drying, storage and emergency assessment. For seed quality analysis, the germination test and the emergence speed index were used, using a completely randomized design, with four treatments (no drying, 12% humidity, 5% humidity and 12% humidity a -20ºC for 90 days) and five repetitions. After physiological classification, it was found that seeds of physic nut are orthodox, thus can be stored at low temperature (-20ºC) and with low water content (<5%), without compromising their viability.

scholarly journals Design of a Small Scale Pilot Biodiesel Production Plant and Determination of the Fuel Properties of Biodiesel Produced With This Plant

2014 ◽  
Vol 3 (2) ◽  
pp. 67
Author(s):  
Tanzer Eryılmaz ◽  
Muttalip Erkan
Keyword(s):  
Seed Oil ◽  
Calorific Value ◽  
Fuel Properties ◽  
Biodiesel Production ◽  
Small Scale ◽  
Mustard Seed ◽  
Production Plant ◽  
Copper Strip ◽  
Wild Mustard

A small scale pilot biodiesel production plant that has a volume of 65 liters/day has been designed, constructed and tested. The plant was performed using oil mixture (50% wild mustard seed oil + 50% refined canola oil) and methanol with sodium hydroxide (NaOH) catalyst. The fuel properties of biodiesel indicated as density at 15oC (889.64 kg/m3), kinematic viscosity at 40oC (6.975 mm2/s), flash point (170oC), copper strip corrosion (1a), water content (499.87 mg/kg), and calorific value (39.555 MJ/kg), respectively.

scholarly journals Pemurnian Gliserol dari Hasil Samping Produksi Biodiesel Minyak Kelapa Sawit (Purification of Glycerol from the By-Product of Palm Oil Biodiesel Production)

2014 ◽  
Vol 4 (1) ◽  
pp. 53-58
Author(s):  
Fahrizal Hazra ◽  
Irfan Septiawan
Keyword(s):  
Phosphoric Acid ◽  
Acid Concentration ◽  
Palm Oil ◽  
Crude Glycerol ◽  
Biodiesel Production ◽  
Average Value ◽  
Result Analysis ◽  
Phosphoric Acid Concentration ◽  
Palm Oil Biodiesel

The process of making biodiesel made of palm oil produced as a by-product of glycerol with low purity levels, liquids, viscous blackish brown with a very alkaline pH (pH >10). Glycerol is often referred to as crude glycerol. The process of refining glycerol that is by adding phosphoric acid concentration range. The average value of the levels of glycerol from glycerol purification results on the phosphoric acid concentration of 2.5%, 5% and 7.5% (v/v) i.e. 81.2205%, 83.4609% and 80.7595%. Determination of the levels of glycerol results showed samples of glycerol rough after the addition of phosphoric acid with different concentrations of already existing standards. The result analysis of glycerol after purification by the addition of phosphoric acid at concentrations of 5% is most suitable for the process of improving  the purity of glycerol.Keywords: crude glycerol, purification, phosphate acid, glycerol content

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