scholarly journals Enhancing the cement quality using polypropylene fiber

2019 ◽  
Vol 10 (3) ◽  
pp. 1097-1107 ◽  
Author(s):  
Salaheldin Elkatatny ◽  
Rahul Gajbhiye ◽  
Anas Ahmed ◽  
Ahmed Abdulhamid Mahmoud

AbstractDurability and long-term integrity of oil well cement are the most important parameters to be considered while designing the cement slurry, especially in the high-pressure and high-temperature (HPHT) environments. In this study, the effect of adding the polypropylene fiber (PPF) to Saudi Class G cement is evaluated under HPHT conditions. The effect of the PPF on the cement compressive and tensile strength, thickening time, density, free water, porosity, and permeability was studied. The effect of the PPF particles on the cement sheath microstructure was studied through powder X-ray diffraction (XRD) and scanning electron microscope. The results obtained showed that PPF did not affect the cement rheology, density, and free water. The addition of PPF considerably decreased the thickening time and improved the tensile and compressive strength of the cement. 0.75% by weight of cement (BWOC) of PPF reduced the thickening time by 75%, from 317 to 78 min. The compressive strength of the cement increased by 17.8% after adding 0.5% BWOC of PPF, while the tensile strength increased by 18% when 0.75% of PPF is used which is attributed to the formation of stable forms of calcium silicate hydrates because of the ability of PPF to accelerate cement hydration process as indicated by the XRD results. The ability of the PPF to decrease the cement thickening time along with its ability to improve the cement strength suggests the use of PPF as an alternative for silica floor in shallow wells where a reduction in thickening time will decrease the wait on cement time. Porosity and permeability of the base cement were also decreased by incorporating PPF because of the pores filling effect of PPF particles as indicated by the microstructure analysis.

2021 ◽  
pp. 147-156
Author(s):  
Ali M. Hadi ◽  
Ayad A. Al-Haleem

Cement is a major component in oil and gas drilling operations that is used to maintain the integrity of boreholes by preventing the movement of formation fluids through the annular space and outside the casing. In 2019, Iraq National Oil Company ordered all international oil and gas companies which are working in Iraq to use Iraqi cement (made in Iraq) in all Iraqi oil fields; however, the X-ray fluorescence (XRF) and compressive strength results in this study show that this cement is not matching with American Petroleum Institute (API) standards. During this study, barolift was used to improve the properties of Iraqi cement used in oil wells at high pressure and high temperature (HPHT). Barolift (1 g) was added to cement admixture to evaluate its influence on improving the performance of cement, mainly related to the property of toughness.  Primarily, the quality and quantity of cement contents were determined using X-ray fluorescence. Experiments were conducted to examine the characteristics of the base cement and the cement system containing 1g of barolift, such as thickening time, free water, compressive strength, and porosity. X-ray diffraction (XRD), scanning electron microscope (SEM), and energy dispersive X-ray spectroscopy (EDS) were conducted for analyzing the microstructure of cement powder. The experimental results showed that barolift acted as a retarder and improved the thickening time, slightly increased the free water, enhanced the mechanical properties, reduced the porosity, and aided in scheming new cement slurry to withstand the HPHT conditions. Microstructure analysis showed that barolift particles blocked the capillaries by filling cement spaces and, thus, a denser and stricter cement network was achieved.


2019 ◽  
Vol 11 (23) ◽  
pp. 6776 ◽  
Author(s):  
Abdulmalek Ahmed ◽  
Ahmed Abdulhamid Mahmoud ◽  
Salaheldin Elkatatny ◽  
Weiqing Chen

In deep hydrocarbon development wells, cement slurry with high density is required to effectively balance the high-pressure formations. The increase in the slurry density could be achieved by adding different heavy materials. In this study, the effect of the weighting materials (barite, hematite, and ilmenite) on the properties of Saudi Class G cement matrix of vertical homogeneity, compressive strength, porosity, and permeability was evaluated. Three cement slurries were weighted with barite, hematite, and ilmenite, and cured at 294 °F and 3000 psi for 24 h. All slurries have the same concentration of the different additives except the weighting material. The amount of weighting material used in every slurry was determined based on the targeted density of 18 lbm/gal. The results of this study revealed that the most vertically homogenous cement matrix was the ilmenite-weighted sample with a vertical variation of 17.6% compared to 20.2 and 24.8% for hematite- and barite-weighted cement, respectively. This is attributed to the small particle size of the ilmenite. The medical computerized tomography (CT) scan confirmed that the ilmenite-weighted sample is the most homogeneous, with a narrow range of density variation vertically along the sample. Hematite-weighted cement showed the highest compressive strength of 55.3 MPa, and the barite- and ilmenite-weighted cement compressive strengths are each 18.4 and 36.7% less than the compressive strength of the hematite-weighted cement, respectively. Barite-weighted cement has the lowest porosity and permeability of 6.1% and 18.9 mD, respectively. The maximum particle size of ilmenite used in this study is less than 42 μm to ensure no abrasion effect on the drilling system, and it minimized the solids segregation while maintaining a compressive strength that is higher than the minimum acceptable strength, which is the recommended weighting material for Saudi Class G cement.


2019 ◽  
Vol 10 (2) ◽  
pp. 319-325
Author(s):  
Ghulam Abbas ◽  
Sonny Irawan ◽  
Khalil Rehman Memon ◽  
Javed Khan

AbstractCellulose-based polymers have been successfully used in many areas of petroleum engineering especially in enhanced oil recovery drilling fluid, fracturing and cementing. This paper presents the application of cellulose-based polymer in oil well cementing. These polymers work as multifunctional additive in cement slurry that reduce the quantity of additives and lessen the operational cost of cementing operation. The viscosity of cellulose polymers such as hydroxyethyl cellulose (HEC), carboxymethylcellulose (CMC) and hydroxypropyl methylcellulose (HPMC) has been determined at various temperatures to evaluate the thermal degradation. Moreover, polymers are incorporated in cement slurry to evaluate the properties and affect in cement slurry at 90 °C. The API properties like rheology, free water separation, fluid loss and compressive strength of slurries with and without polymer have been determined at 90 °C. The experimental results showed that the viscosity of HPMC polymer was enhanced at 90 °C than other cellulose-based polymers. The comparative and experimental analyses showed that the implementation of cellulose-based polymers improves the API properties of cement slurry at 90 °C. The increased viscosity of these polymers showed high rheology that was adjusted by adding dispersant which optimizes the rheology of slurry. Further, improved API properties, i.e., zero free water separation, none sedimentation, less than 50 ml/30 min fluid loss and high compressive strength, were obtained through HEC, CMC and HPMC polymer. It is concluded that cellulose-based polymers are efficient and effective in cement slurry that work as multifunctional additive and improve API properties and cement durability. The cellulose-based polymers work as multifunctional additive that reduces the quantity of other additives in cement slurry and ultimately reduces the operational cost of cementing operation. The comparative analysis of this study opens the window for petroleum industry for proper selection of cellulose-based polymer in designing of cement slurry.


2021 ◽  
Vol 11 (2) ◽  
pp. 30-48
Author(s):  
Amel Habeeb Assi ◽  
Faleh H. M. Almahdawi ◽  
Qasim Abdulridha Khalti

The reinforced fiberglass in cement slurry reflects the effect on its properties compared to usual additives. Fiberglass is typically used in cement slurry design for one or another of the following goals: (Earth earthquake, bearing storage, and with differential stresses, to enhance cement durability and increase its compressive strength). The main goal is to use glass fiber and ground fiberglass to improve the tensile strength and moderate compressive strength significantly. On the other hand, the use of glass fibers led to a slight increase in the value of thickening time, which is a desirable effect. Eleven glass fiber samples and milled glass fiber were used to show these materials' effect on Iraqi cement with (0.125, 0.25, 0.5, 0.75, 1, and 2) % of cement weight. Those tests used to study cement slurry‟s following properties were compressive strength, thickening time, rheology properties of free water, filtering, and density. These evaluations showed that slurries with less than 1% fiber content gave a higher compressive strength than a sample containing more than 1% glass fiber. However, the slurry mixed with equal or less than 1% milled glass fiber is higher compressive than the sample mixed with more than 1% milled glass fiber. So the optimal concentration for glass fiber is less than 1% by weight of cement (BWOC); either for milled glass fiber, it is less or equal to 1% BWOC. Both materials contributed to increasing the compressive strength of the cement. However, attention must be paid to the idealThis work is licensed under a Creative Commons Attribution 4.0 International License. concentration that should be added during the cement slurry preparation because if we use these two materials carelessly for the ideal concentration, this leads to the collapse and bombardment of the resistance of the cement rock. In other words, the collapse of cement resistance and causing problems during the cementing process.


2011 ◽  
Vol 477 ◽  
pp. 274-279 ◽  
Author(s):  
Yi Xu ◽  
Lin Hua Jiang ◽  
Hong Qiang Chu ◽  
Lei Chen

In this study, the effects of fiber types on the mechanical properties of lightweight aggregate concretes were investigated. Three types of fibers, namely, polypropylene fiber, steel fiber and water hyacinth (Eichhornia crassipes) fiber, and two types of lightweight aggregates, namely, expanded polystyrene and ceramsite were used. The compressive strength and splitting tensile strength of concretes were tested. The results show that both the compressive strength and the splitting tensile strength were improved by adding a reasonable volume of steel fiber and polypropylene fiber into LWAC. The addition of water hyacinth fiber had little effect on the compressive strength of LWAC, while a little increase was observed in the splitting tensile strength.


2014 ◽  
Vol 692 ◽  
pp. 433-438 ◽  
Author(s):  
Jing Fu Zhang ◽  
Jin Long Yang ◽  
Kai Liu ◽  
Bo Wang ◽  
Rui Xue Hou

Carbon dioxide CO2could corrode the oil well cement paste matrix under agreeable moisture and pressure condition in deep oil wells, which could decrease the compressive strength and damage the annular seal reliability of cement paste matrix. The problem of oil well cement paste matrix corrosion by CO2was researched in the paper for obtain the feasible corrosion prevention technical measures. The microstructure and compressive strength of corroded cement paste matrix were examined by scanning electron microscopeSEMand strength test instrument etc. under different corrosion conditions. The mechanism and effect law of corrosion on oil well cement paste matrix by CO2were analyzed. And the suitable method to protect CO2corrosion in deep oil wells was explored. The results show that the corrosion mechanism of cement paste matrix by CO2was that the wetting phase CO2could generate chemical reaction with original hydration products produced from cement hydration, which CaCO3were developed and the original composition and microstructure of cement paste matrix were destroyed. The compressive strength of corrosion cement paste matrix always was lower than that of un-corrosion cement paste matrix. The compressive strength of corrosion cement paste matrix decreased with increase of curing temperature and differential pressure. The corroded degree of cement paste matrix was intimately related with the compositions of cement slurry. Developing and design anti-corrosive cement slurry should base on effectively improving the compact degree and original strength of cement paste matrix. The compounding additive R designed in the paper could effectively improve the anti-corrosive ability of cement slurry.


Author(s):  
Moein Khoshroo ◽  
Ali Akbar Shirzadi Javid ◽  
Nima Rajabi Bakhshandeh ◽  
Mohamad Shalchiyan

In this study, the effect of using crumb rubber and recycled aggregates on the mechanical properties of concrete has been evaluated as areplacement of fine and coarse aggregates In order to add the admixtures and evaluate their combined effect, 20 different types of concrete mixture ratio were prepared. The results indicated that in those samples containing crumb rubber and recycled aggregates the compressive strength is reduced and adding fiber up to 0.1%. to these concrete samples can improve the compressive strength Also, the tensile strength of the samples mixed with crumb rubber and recycled aggregates were decreased, and with the addition of propylene fiber up to 0.4%. the tensile strength slightly increased Moreover by adding the crumb rubber to the samples the elasticity modulus was reduced but by adding fiber to samples about 0.1% and 0.2.% the modulus of elasticity of concrete in all samples were increased. According to the results, it can be said that using the combination of 5% of crumb rubber as a replacement of fine aggregate, and the combination of 35% of recycled aggregates as a replacement of coarse aggregate, and also by adding 0.1% polypropylene fiber in volumetric percentage of concrete along with adding 7% of micro silica as a replacement of cement led to the best effect on the mechanical properties of concrete.


2010 ◽  
Vol 168-170 ◽  
pp. 1325-1329
Author(s):  
Ye Ran Zhu ◽  
Jun Cai ◽  
Dong Wang ◽  
Guo Hong Huang

This paper investigates the mechanical properties (compressive strength, splitting tensile strength and flexural toughness) of polypropylene fiber reinforced self-compacting concrete (PFRSCC). The effect of the incorporation of polypropylene fiber on the mechanical properties of PFRSCC is determined. Four point bending tests on beam specimens were performed to evaluate the flexural properties of PFRSCC. Test results indicate that flexural toughness and ductility are remarkably improved by the addition of polypropylene fiber.


2016 ◽  
Vol 677 ◽  
pp. 246-253
Author(s):  
Artur Koper

The article analysed the results of comparative sampling of selected properties of concretes with addition of aggregates from sanitary ceramic wastes. For the need of the analyses there were created concretes of various w/c coefficients (0,35, 0,50, 0,75) and with diverse percentage participation of ceramic wastes aggregates (exchange of 50% and 100% coarse aggregates into ceramic). The range of performed samples and analyses included sampling of mechanical and physical properties of concretes and the aggregates used. What was under analysis: for aggregates – sampling of bulk density, absorbency, resistance to crushing; for concretes from ceramic wastes – sampling of density, absorbency, compressive strength, tensile strength and compressive strength after roasting. Roasting was performed according to defined temperature cycles: cycle I - from 0 to 150OC (vaporisation of free water), cycle II - from 150 to 550OC (separation of chemically combined water), cycle III - beyond 550OC (change of hydraulic combination into ceramic, sintering).


2012 ◽  
Vol 730-732 ◽  
pp. 307-312 ◽  
Author(s):  
Ana Cecilia Vieira da Nóbrega ◽  
Antonio Eduardo Martinelli ◽  
Dulce Maria de Araújo Melo ◽  
Marcus Antonio de Freitas Melo ◽  
Julio Cezar de Oliveira Freitas ◽  
...  

Mud acid attack of 14 lbm/gal Portland cement composites with 15 % of nonionic aqueous polyurethane was investigated. Plain Portland hardened cement slurries showed the loss of weight around 23 %. The addition of aqueous polyurethane resulted in longer durability, with reduction around 87 % on the loss of weight without influence on the compressive strength or fratographic. The mechanism is related with the decreased porosity and permeability due to the polymeric net formation on the bulk and minor quantities of Ca+2, preferentially leached to the acidic solution. In this way, Portland-aqueous polyurethane composites are possible solutions to oil well cementing submitted to steam injection and mud acid acidizing operations.


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