A facile one-step route for production of CuO, NiO, and CuO–NiO nanoparticles and comparison of their catalytic activity for ammonium perchlorate decomposition

RSC Advances ◽  
2015 ◽  
Vol 5 (117) ◽  
pp. 96777-96784 ◽  
Author(s):  
Seyed Ghorban Hosseini ◽  
Reza Abazari

This study demonstrates a straightforward, inexpensive, high-yield, and ecofriendly route for synthesis of sphere-like CuO, NiO, and CuO–NiO (with different molar ratios) nanoparticles (NPs) through emulsion route.

2005 ◽  
Vol 437 (1-2) ◽  
pp. 106-109 ◽  
Author(s):  
Yanping Wang ◽  
Junwu Zhu ◽  
Xujie Yang ◽  
Lude Lu ◽  
Xin Wang

2011 ◽  
Vol 236-238 ◽  
pp. 1665-1669
Author(s):  
Min Zheng ◽  
Zuo Shan Wang ◽  
Qing Wang

Nitrogen-doped zinc oxide (N-doped ZnO) nanocrystallites were synthesized via improved one-step combustion technique by using citric acid as additive. Scan electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS) were used to determine the grain size, shape, degree of nitrogen incorporation and nature of the resultant oxynitride chemical bonding. The catalytic performance of N-doped ZnO on the thermal decomposition of ammonium perchlorate (AP) was investigated by DSC-TG technique. The results show that the as-synthesized N-doped ZnO has uniform crystallite size about 20-30nm in diameter and 1.25%wt nitrogen incorporation, which forms into NO bonding region in ZnO crystal lattice. The nitrogen doping is accountable for the significant increase in catalytic activity on the thermal decomposition of AP versus the commercial nanometer ZnO and the thermal decomposition peak shifts 133°C downward when the content of N-doped ZnO in AP is 3%wt.


2021 ◽  
Vol 50 (16) ◽  
pp. 5632-5643
Author(s):  
Suman Adhikari ◽  
Tirtha Bhattacharjee ◽  
Sharmila Bhattacharjee ◽  
Constantin Gabriel Daniliuc ◽  
Antonio Frontera ◽  
...  

To ascertain the influence of binary ligand systems on the coordination modes of the Ni(ii) metal center and resulting supramolecular architectures, three Ni(ii) thiolate complexes have been synthesized in high yield in one step in water and structurally characterized.


2020 ◽  
Vol 17 (8) ◽  
pp. 628-630
Author(s):  
Vu Binh Duong ◽  
Pham Van Hien ◽  
Tran Thai Ngoc ◽  
Phan Dinh Chau ◽  
Tran Khac Vu

A simple and practical method for the synthesis on a large scale of altretamine (1), a wellknown antitumor drug, has been successfully developed. The synthesis method involves the conversion of cyanuric chloride (2) into altretamine (1) by dimethylamination of 2 with an aqueous solution of 40% dimethylamine and potassium hydroxide in 1, -dioxan 4in one step to give altretamine (1) in high yield.


Author(s):  
Francisco G. Cirujano ◽  
Nuria Martin ◽  
Neyvis Almora-Barrios ◽  
Carlos Martí-Gastaldo

Room temperature one-step synthesis of the peptide-based porous material with a periodic distribution of pockets decorated with lysine side chain active sites behaves as a heterogeneous organocatalyst. The pockets are...


Molecules ◽  
2021 ◽  
Vol 26 (6) ◽  
pp. 1502
Author(s):  
Johannes M. Parikka ◽  
Karolina Sokołowska ◽  
Nemanja Markešević ◽  
J. Jussi Toppari

The predictable nature of deoxyribonucleic acid (DNA) interactions enables assembly of DNA into almost any arbitrary shape with programmable features of nanometer precision. The recent progress of DNA nanotechnology has allowed production of an even wider gamut of possible shapes with high-yield and error-free assembly processes. Most of these structures are, however, limited in size to a nanometer scale. To overcome this limitation, a plethora of studies has been carried out to form larger structures using DNA assemblies as building blocks or tiles. Therefore, DNA tiles have become one of the most widely used building blocks for engineering large, intricate structures with nanometer precision. To create even larger assemblies with highly organized patterns, scientists have developed a variety of structural design principles and assembly methods. This review first summarizes currently available DNA tile toolboxes and the basic principles of lattice formation and hierarchical self-assembly using DNA tiles. Special emphasis is given to the forces involved in the assembly process in liquid-liquid and at solid-liquid interfaces, and how to master them to reach the optimum balance between the involved interactions for successful self-assembly. In addition, we focus on the recent approaches that have shown great potential for the controlled immobilization and positioning of DNA nanostructures on different surfaces. The ability to position DNA objects in a controllable manner on technologically relevant surfaces is one step forward towards the integration of DNA-based materials into nanoelectronic and sensor devices.


2014 ◽  
Vol 2 (36) ◽  
pp. 7477-7481 ◽  
Author(s):  
Xinwei Dong ◽  
Yanjie Su ◽  
Huijuan Geng ◽  
Zhongli Li ◽  
Chao Yang ◽  
...  

N-doped CDs can be obtained directly with high yield by pyrolyzing ethanolamine in air within just 7 minutes with the assistance of hydrogen peroxide.


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