scholarly journals Effect of frequency, temperature, and time of sonication on xanton content of mangosteen (Garcinia mangostana L.) peel extract through ultrasound assisted extraction

2019 ◽  
Vol 125 ◽  
pp. 25006 ◽  
Author(s):  
Suryono Suryono ◽  
Hadiyanto Hadiyanto ◽  
Moh. Yasin ◽  
Retno Widyowati ◽  
Muflihatul Muniroh ◽  
...  
Keyword(s):  
Extraction Process ◽  
Extraction Yield ◽  
Sonication Time ◽  
Ultrasound Assisted Extraction ◽  
Garcinia Mangostana ◽  
Mangosteen Peel ◽  
Assisted Extraction ◽  
Ultrasound Assisted ◽  
Conventional Methods ◽  
Frequency Temperature

Ultrasound Assisted Extraction (UAE) has been used for the extraction of mangosteen peel (Garcinia mangostana L.) in producing xanton. Mangosteen peel extraction with UAE has been carried out to determine the effect of frequency, temperature, and time of sonication on the xanton content. The parameters controlled are frequency (20 - 40 kHz), temperature (25 - 35oC), and sonication time (20 - 40 minutes). The solvent used in the extraction was methanol with a ratio of mangosteen peel: solvent = 1: 10 and analysis of xanton content in the extraction. Extraction results showed that the content of xanthones from the extraction results of mangosteen (Gracinia mangostana L.) peel with UAE had optimum values at a frequency of 40 kHz, temperature of 35oC, and sonication time of 30 minutes. At the same frequency, temperature, and time, conventionally showed xanthones content of mangosteen rind extract of 93 ppm. The results show that the extraction yield using UAE is greater than that of conventional methods. From the results of this experiment, it can be concluded that the use of the UAE in the xanthones extraction process of mangosteen peel (Gracinia mangostana L.) is more optimal when compared to conventional methods.

scholarly journals Optimization of ultrasound-assisted extraction of total polyphenolic compounds from Juglans nigra L. leaves

2018 ◽  
Vol 83 (11) ◽  
pp. 1273-1284 ◽  
Author(s):  
Marijana Gavrilovic ◽  
Katarina Rajkovic ◽  
Valentina Simic ◽  
Sanja Jeremic ◽  
Snjezana Mirkovic ◽  
...  
Keyword(s):  
Extraction Process ◽  
Relative Difference ◽  
Extraction Yield ◽  
Ethanol Solution ◽  
Juglans Nigra ◽  
Total Phenolic ◽  
Ultrasound Assisted Extraction ◽  
Commercial Preparation ◽  
Assisted Extraction ◽  
Ultrasound Assisted

The ultrasound-assisted extraction of Juglans nigra L. leaves was optimized with respect to total phenolic content (TP) of the extracts by varying the concentration of aqueous ethanol solution (E) and different solvent-to-solid ratio (S). The influence and optimum of the operating parameters (E and S) was examined using response surface methodology (RSM). The statistical criteria indicated the adequacy, reliability and precision of the developed RSM model. RSM showed that maximum extraction yield of TP 28.59 mg g-1 of draw plant was achieved at the optimal values of 50% E and 20 kg kg-1 S. Using the modelled optimized conditions, the detected relative difference between the predicted and the experimental yield was ?2.3 %. The determined TP content in the extracts varied from 12.54 to 29.26 mg GAE g-1 of dry plant indicated that J. nigra is a valuable source of phenolic substances. The extracts of J. nigra leaves obtained under optimal conditions showed good antioxidant activity (IC50 = 18.91?0.03 ?g cm-3) which was determined by the scavenging effect on 2,2-diphenyl-1-picrylhydrazyl radical. The optimization of the TP extraction process is the important step in improving techno-economics of the potential commercial preparation of J. nigra extracts, as natural source of antioxidants.

scholarly journals Optimization of Ficus deltoidea Using Ultrasound-Assisted Extraction by Box-Behnken Statistical Design

2016 ◽  
Vol 02 ◽  
pp. 71 ◽  
Author(s):  
L. J. Ong ◽  
Awang Soh Mamat ◽  
Muhammad Shahzad Aslam ◽  
Muhammad Syarhabil Ahmad ◽  
◽  
...  
Keyword(s):  
Ethanol Concentration ◽  
Statistical Design ◽  
Extraction Yield ◽  
Total Phenolic ◽  
Sonication Time ◽  
Ultrasound Assisted Extraction ◽  
Ficus Deltoidea ◽  
Assisted Extraction ◽  
Ultrasound Assisted ◽  
Sample Ratio

In this study, the effect of extraction parameters (ethanol concentration, sonication time, and solvent-to-sample ratio) onFicus deltoidealeaves was investigated using ultrasound-assisted extraction by response surface methodology (RSM). Total phenolic content (TPC) ofF. deltoideaextracts was identified using Folin-Ciocalteu method and expressed in gallic acid equivalent (GAE) per g. Box-Behnken statistical design (BBD) was the tool used to find the optimal conditions for maximum TPC. Besides, the extraction yield was measured and stated in percentage. The optimized TPC attained was 455.78 mg GAE/g at 64% ethanol concentration, 10 minutes sonication time, and 20 mL/g solvent-to-sample ratio whereas the greatest extraction yield was 33% with ethanol concentration of 70%, sonication time of 40 minutes, and solvent-to-material ratio at 40 mL/g. The determination coefficient,R2, for TPC indicates that 99.5% capriciousness in the response could be clarified by the ANOVA model and the value of 0.9681 of predictedR2is in equitable agreement with the 0.9890 of adjustedR2. The present study shows that ethanol water as solvent, a short time of 10 minutes, and adequate solvent-to-sample ratio (20 mL/g) are the best conditions for extraction.

scholarly journals Effect of Ultrasound-Assisted Extraction Parameters on Total Polyphenols and Its Antioxidant Activity from Mango Residues (Mangifera indica L. var. Manililla)

Separations ◽  
2021 ◽  
Vol 8 (7) ◽  
pp. 94
Author(s):  
Anahí J. Borrás-Enríquez ◽  
Elizabeth Reyes-Ventura ◽  
Socorro J. Villanueva-Rodríguez ◽  
Lorena Moreno-Vilet
Keyword(s):  
Antioxidant Activity ◽  
Mangifera Indica ◽  
Central Point ◽  
Added Value ◽  
Sonication Time ◽  
Ultrasound Assisted Extraction ◽  
Extraction Technology ◽  
Total Polyphenols ◽  
Assisted Extraction ◽  
Ultrasound Assisted

Manililla is a mango variety whose residues contain bioactive compounds such as polyphenols and flavonoids, with high added value. The use of environmentally friendly extraction technology would be of great relevance; hence, this study aimed to evaluate the effect of solvent relation, sonication time and amplitude on the ultrasound-assisted extraction of total polyphenols in Manililla mango residues (peel, endocarp and kernel) and antioxidant activity. An experimental design 23 with a central point was used to evaluate the curvature behavior of the process variables. Conventional maceration was used as a control. The better conditions were obtained at the central point using 50% ethanol in water, 60% amplitude and 20 min of sonication time. We obtained values of up to 1814 mg GAE/100 g, 469 mg GAE/100 g and 672 mg GAE/100 g of total polyphenols and 1228 mg QE/100 g, 653 mg QE/100 g and 880 mg QE/100 g of total flavonoids for peel, endocarp and kernel, respectively. Mangiferin was quantified in ultrasound-assisted extraction at 150 mg/g in peel and 0.025 mg/g in the kernel, but it was not detectable in maceration. An antioxidant capacity of 87%, 14% and 83% inhibition for peel, endocarp and kernel, respectively, were obtained. Peel and kernel were the residues with higher potential as extraction material, while endocarp was not.

scholarly journals Mathematical Modelling of Ultrasound-Assisted Extraction Kinetics of Bioactive Compounds from Artichoke By-Products

Foods ◽  
2021 ◽  
Vol 10 (5) ◽  
pp. 931
Author(s):  
Cristina Reche ◽  
Carmen Rosselló ◽  
Mónica M. Umaña ◽  
Valeria Eim ◽  
Susana Simal
Keyword(s):  
Power Density ◽  
Bioactive Compounds ◽  
Extraction Yield ◽  
Total Phenolic ◽  
Model Parameters ◽  
Ultrasound Assisted Extraction ◽  
Yield Curves ◽  
Assisted Extraction ◽  
Ultrasound Assisted ◽  
Ultrasound Power

Valorization of an artichoke by-product, rich in bioactive compounds, by ultrasound-assisted extraction, is proposed. The extraction yield curves of total phenolic content (TPC) and chlorogenic acid content (CAC) in 20% ethanol (v/v) with agitation (100 rpm) and ultrasound (200 and 335 W/L) were determined at 25, 40, and 60 °C. A mathematical model considering simultaneous diffusion and convection is proposed to simulate the extraction curves and to quantify both temperature and ultrasound power density effects in terms of the model parameters variation. The effective diffusion coefficient exhibited temperature dependence (72% increase for TPC from 25 °C to 60 °C), whereas the external mass transfer coefficient and the equilibrium extraction yield depended on both temperature (72% and 90% increases for TPC from 25 to 60 °C) and ultrasound power density (26 and 51% increases for TPC from 0 (agitation) to 335 W/L). The model allowed the accurate curves simulation, the average mean relative error being 5.3 ± 2.6%. Thus, the need of considering two resistances in series to satisfactorily simulate the extraction yield curves could be related to the diffusion of the bioactive compound from inside the vegetable cells toward the intercellular volume and from there, to the liquid phase.

Research on Detecting Tris-(2,3-dibromopropyl)-Phosphate in Textiles with the HPLC/DAD Method

2012 ◽  
Vol 441 ◽  
pp. 640-644
Author(s):  
Ke Jie Fu ◽  
Li Sheng Yang ◽  
Chang Sheng Feng ◽  
Liang Chen
Keyword(s):  
Limit Of Detection ◽  
Extraction Process ◽  
Ultrasound Assisted Extraction ◽  
Routine Testing ◽  
Assisted Extraction ◽  
Ultrasound Assisted ◽  
Pre Treatment ◽  
Finishing Agent ◽  
Detecting Method ◽  
Precision Test

A detecting method for toxic flame retardant finishing agent tris-(2,3-dibromopropyl) -phosphate (TRIS for short) in textiles was studied. In the method, an acetonitrile ultrasound-assisted extraction process was included in sample pre-treatment, and HPLC/DAD was used in the separation and identification of extractives. After that, the conditions of pre-treatment and chromatograph were optimized. The results showed that the limit of detection (LOD) by this method (S/N10) is 1.0 mg/kg, its recovery ranged from 78.1% to 98.4%, and RSD of the precision test is 3.2%, of which all met the requirements for routine testing.

scholarly journals Antioxidant Capacity and Antigenotoxic Effect of Hibiscus sabdariffa L. Extracts Obtained with Ultrasound-Assisted Extraction Process

2020 ◽  
Vol 10 (2) ◽  
pp. 560
Author(s):  
Gregorio Iván Peredo Pozos ◽  
Mario Alberto Ruiz-López ◽  
Juan Francisco Zamora Nátera ◽  
Carlos Álvarez Moya ◽  
Lucia Barrientos Ramírez ◽  
...  
Keyword(s):  
Antioxidant Activity ◽  
Human Lymphocytes ◽  
Dry Weight ◽  
Extraction Process ◽  
Hibiscus Sabdariffa ◽  
Ultrasound Assisted Extraction ◽  
Solid Ratio ◽  
Assisted Extraction ◽  
Ultrasound Assisted ◽  
Antigenotoxic Effect

Hibiscus sabdariffa (Roselle) is in high demand worldwide due to its beneficial health properties owing to the polyphenols content, mainly in the flower calyx. The objective of this study was to find the best conditions (time and liquid: solid ratio) to extract polyphenols from Roselle using Ultrasound-Assisted Extraction (UAE) (40 kHz, 180 W), with ethanol how solvent; as well as determine the yield of phenols, anthocyanin, flavonoids, tannins, antioxidant activity (DPPH) and antigenotoxic effect (comet assay). A traditional solid-liquid extraction was applied as a reference. Extraction times of 40 and 60 min resulted in the highest polyphenols (13.019 mg GAE/g dry weight (dw)), flavonoids (4.981 CE/g dw), anthocyanins (1.855 mg Cya3GE/g dw), and tannins (0.745 CE/g dw) recoveries and an antioxidant activity (DPPH) of 74.58%. Extracts from white calyces contained similar amounts of phenols and flavonoids, but very little condensed tannins (0.049 CE/g dw) and practically no anthocyanins. Extracts from red and white calyces, showed antigenotoxic activity and repaired capacity of damage caused by mutagens in human lymphocytes.

scholarly journals Bioactive Compounds in Bael Fruit Pulp Waste: Ultrasound-Assisted Extraction, Characterization, Modeling, and Optimization Approaches

2020 ◽  
Vol 11 (2) ◽  
pp. 9318-9334
Keyword(s):  
Bioactive Compounds ◽  
Food Additives ◽  
Extraction Process ◽  
Coefficient Of Determination ◽  
Fruit Pulp ◽  
Ultrasound Assisted Extraction ◽  
Modeling And Optimization ◽  
Assisted Extraction ◽  
Pharmaceutical Industries ◽  
Ultrasound Assisted

Bael fruit is an abundant source of bioactive compounds that have importance in the food and pharmaceutical industries. The process of extraction of the bael fruit juice produced a higher percentage of bael fruit pulp waste (BFPW) (37.33 %), which was recycled for the extraction of bioactive compounds. Thus the bioactive compounds like polyphenols, flavonoids, and carotenoids were extracted from BFPW by using the ultrasound-assisted extraction (UAE) technique. The modeling and optimization of the extraction process were carried out by using the experimental design of response surface methodology (RSM). The ethanol concentration of 51.22 %, ultrasound amplitude of 51.45 %, and ultrasound treatment time of 6.11 minutes were obtained to be an RSM optimized values of extraction process variables. The lower values of root mean squared error (RMSE) and mean absolute error (MAE) and higher values of coefficient of determination (R2) indicated admissibility and acceptability of RSM. This extraction process of bioactive compounds has the potential to implement it on an industrial scale for the formulation of food additives and medicines.

scholarly journals Modelling and Optimization of Ultrasound Assisted Extraction of Polyphenols Using Response Surface Methodology

2020 ◽  
Vol 5 (9) ◽  
pp. 1004-1012
Author(s):  
Junior Franck Ekorong Akouan Anta ◽  
Biloa Dorothée Marcelle ◽  
Bruno Fabrice Siewe ◽  
Raghavarao K. S. M. S.
Keyword(s):  
Response Surface Methodology ◽  
Response Surface ◽  
Reducing Power ◽  
Extraction Yield ◽  
Operating Conditions ◽  
Extraction Time ◽  
Ultrasound Assisted Extraction ◽  
Stirring Rate ◽  
Assisted Extraction ◽  
Ultrasound Assisted

Mango seed kernels are by-products of the consumption and transformation of mango fruits (Mangifera indica L.). Many ways of valorisation have been proposed, and among them, their phenolic compounds extraction. To increase the extraction yield, ultrasound-assisted extraction was modelled and optimized. The 4 factors Central Composite design associated with the Response Surface Methodology (RSM) were used to achieve that goal. The effect of extraction time, temperature, stirring rate and the Ultrasound Amplitude, on the total phenolic compound extraction yield and the total reducing power of the extract, were studied and modelled. The modelling allows us to do a multi-response optimization to identify the best-operating conditions to achieve at the same time the highest extraction yield and antioxidant capacity. The optimal operating conditions achieved were 41.82 min of extraction time, 54.75⁰C as extraction time, under 266.67 rpm as stirring rate, and 100% ultrasound amplitude. With an expected extraction yield of 71.35 mg GA/g, and 123.058 mg AA/g of total reducing power. 2 extraction cycles, under these conditions, are enough to extract a maximum of the phenolic content, under the described conditions.

scholarly journals Ziziphus lotus (L.) Lam. plant treatment by ultrasounds and microwaves to improve antioxidants yield and quality: An overview

2021 ◽  
Vol 5 (12) ◽  
pp. 53-68
Author(s):  
Farida Berkani ◽  
Maria Luísa Serralheiro ◽  
Farid Dahmoune ◽  
Malik Mahdjoub ◽  
Nabil Kadri ◽  
...  
Keyword(s):  
Antioxidant Activity ◽  
Extraction Yield ◽  
Point Of View ◽  
Microwave Assisted Extraction ◽  
Ultrasound Assisted Extraction ◽  
Microwave Assisted ◽  
Yield And Quality ◽  
Assisted Extraction ◽  
Industrialization Process ◽  
Ultrasound Assisted

The purpose of this review is to compile the literature published about different aspects of microwave-assisted extraction (MAE) use and ultrasound-assisted extraction (UAE) applied on jujube worldwide and to compare the results on the antioxidant activity obtained for each extraction method. As a result of the increased consumers demand for natural products, as well as for those of agro-food, nutraceutical, cosmetic industries, and green extraction techniques are nowadays trending to be potential alternatives that can improve antioxidant yield and its quality from an economical and environmental point of view by reducing time, energy, and solvent consumption. Ultrasounds and microwaves are widely used methods in the extraction of active principles due to their cavitation and dipolar rotation effect, respectively. These two techniques provide efficiency of extraction while minimizing the time and preserving the quality of the food matrix, overcoming the disadvantages of conventional techniques characterized by their consumption of large quantities of solvents and providing a sparse quantity of extraction. Jujube, a shrub with a high antioxidant potential, which can be affected by various extraction conditions can be the target of UAE and MAE to increase the antioxidant extraction yield. Exploiting the beneficial properties such as the antioxidant activity can lead to an industrialization process, replacing therefor synthetic antioxidants with natural compounds. These can also help in the development of new nutraceuticals and can be used, for instance, in agro-food industries as preservatives. Keywords : Microwave-assisted extraction (MAE), ultrasound-assisted extraction (UAE), antioxidants, Ziziphus lotus (L.) Lam plant.

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