Cementitious Sealing Material: 3D Digital Image Based Characterization of Pore Size Distribution and Modeling of Transport Properties

2013 ◽  
Author(s):  
Neven Ukrainczyk ◽  
Eduardus A. B. Koenders ◽  
Klaas van Breugel
Keyword(s):  
Pore Size ◽  
Transport Properties ◽  
Digital Image ◽  
Oil And Gas ◽  
Transport Model ◽  
Medial Axis ◽  
Three Dimensional ◽  
Cementitious Materials ◽  
Pore Size Distributions

Exhausted oil and gas reservoirs are one of the most potential storage facilities to sequestrate the worlds CO2. These reservoirs are sealed with cementitious materials, that should have a long time performance. Therefore, this paper emphasizes the characterization of the evolving capillary pore network and transport properties of the cementitious microstructure used to seal the wellbore. The Hymostruc numerical model is employed to simulate the development of an evolving virtual microstructure of cementitious materials. The simulated 3D microstructures were then digitized to form a matrix of cubic voxels. The pore-size distributions of the obtained virtual microstructures were calculated using a combination of three-dimensional digital image processing algorithms: 1) distance transform and 2) medial axis thinning algorithm to obtain a 3D skeleton of the pore structure. Transport properties of the simulated microstructures are analyzed employing a finite difference 3D transport model. The modeling results are compared with available literature results.

Numerical Algorithm for Pore Size Distribution Characterization of Materials from 3D Images

2013 ◽  
Vol 699 ◽  
pp. 584-589 ◽  
Author(s):  
Neven Ukrainczyk ◽  
Eduard Koenders ◽  
Klaas van Breugel
Keyword(s):  
Pore Structure ◽  
Pore Size Distribution ◽  
Pore Size ◽  
Size Distribution ◽  
Numerical Algorithm ◽  
Digital Image ◽  
Medial Axis ◽  
Characterization Of Materials ◽  
2D And 3D

This paper presents an image based numerical method proposed to obtain information regarding pore structure and organization of pores within materials based on 3D digital image input. The output of the numerical algorithm is a pore size distribution of materials. The algorithm is based on the combination of the two digital image processing algorithms: 1) a medial axis thinning algorithm to obtain 3D skeleton of the pore structure, and 2) the distance transform of an image. The method is tested on simple 2D and 3D microstructures of packed spheres, demonstrating the performance of the proposed method.

CHARACTERIZATION OF PORE SIZE DISTRIBUTIONS USING NON-NEWTONIAN FLUIDS

2020 ◽  
Author(s):  
Scott C. Hauswirth ◽  
◽  
Majdi Abou Najm ◽  
Christelle Basset
Keyword(s):  
Pore Size ◽  
Newtonian Fluids ◽  
Size Distributions ◽  
Pore Size Distributions

scholarly journals Experimental investigation on pore size distribution and drying kinetics during lyophilization of sugar solutions

2018 ◽  
Author(s):  
Petra Foerst ◽  
M. Lechner ◽  
N. Vorhauer ◽  
H. Schuchmann ◽  
E. Tsotsas
Keyword(s):  
Pore Structure ◽  
Pore Size Distribution ◽  
Pore Size ◽  
Size Distribution ◽  
Freeze Drying ◽  
Three Dimensional ◽  
Drying Kinetics ◽  
Process Efficiency ◽  
Freeze Dried ◽  
Pore Size Distributions

The pore structure is a decisive factor for the process efficiency and product quality of freeze dried products. In this work the two-dimensional ice crystal structure was investigated for maltodextrin solutions with different concentrations by a freeze drying microscope. The resulting drying kinetics was investigated for different pore structures. Additionally the three-dimensional pore structure of the freeze dried samples was measured by µ-computed tomography and the pore size distribution was quantified by image analysis techniques. The two- and three-dimensional pore size distributions were compared and linked to the drying kinetics.Keywords: pore size distribution; freeze drying; maltodextrin solution; freeze drying microscope   

Three-Dimensional Strain-Based Model for the Severity Characterization of Dented Pipelines

2018 ◽  
Vol 1 (3) ◽  
Author(s):  
Chike Okoloekwe ◽  
Muntaseer Kainat ◽  
Doug Langer ◽  
Sherif Hassanien ◽  
J.J. Roger Cheng ◽  
...  
Keyword(s):  
Oil And Gas ◽  
Numerical Models ◽  
Three Dimensional ◽  
Strain Analysis ◽  
Computation Time ◽  
Order Continuity ◽  
Element Analysis ◽  
The Mathematical Model ◽  
Derivatives Of

Oil and gas pipelines traverse long distances and are often subjected to mechanical forces that result in permanent distortion of its geometric cross section in the form of dents. In order to prioritize the repair of dents in pipelines, dents need to be ranked in order of severity. Numerical modeling via finite element analysis (FEA) to rank the dents based on the accumulated localized strain is one approach that is considered to be computationally demanding. In order to reduce the computation time with minimal effect to the completeness of the strain analysis, an approach to the analytical evaluation of strains in dented pipes based on the geometry of the deformed pipe is presented in this study. This procedure employs the use of B-spline functions, which are equipped with second-order continuity to generate displacement functions, which define the surface of the dent. The strains associated with the deformation can be determined by evaluating the derivatives of the displacement functions. The proposed technique will allow pipeline operators to rapidly determine the severity of a dent with flexibility in the choice of strain measure. The strain distribution predicted using the mathematical model proposed is benchmarked against the strains predicted by nonlinear FEA. A good correlation is observed in the strain contours predicted by the analytical and numerical models in terms of magnitude and location. A direct implication of the observed agreement is the possibility of performing concise strain analysis on dented pipes with algorithms relatively easy to implement and not as computationally demanding as FEA.

scholarly journals Ink-bottle Effect and Pore Size Distribution of Cementitious Materials Identified by Pressurization–Depressurization Cycling Mercury Intrusion Porosimetry

Materials ◽  
2019 ◽  
Vol 12 (9) ◽  
pp. 1454 ◽  
Author(s):  
Yong Zhang ◽  
Bin Yang ◽  
Zhengxian Yang ◽  
Guang Ye
Keyword(s):  
Pore Structure ◽  
Pore Size Distribution ◽  
Pore Size ◽  
Size Distribution ◽  
Mercury Intrusion Porosimetry ◽  
Cementitious Materials ◽  
Limestone Powder ◽  
Accurate Estimation ◽  
Mercury Intrusion ◽  
Pore Size Distributions

Capturing the long-term performance of concrete must be underpinned by a detailed understanding of the pore structure. Mercury intrusion porosimetry (MIP) is a widely used technique for pore structure characterization. However, it has been proven inappropriate to measure the pore size distribution of cementitious materials due to the ink-bottle effect. MIP with cyclic pressurization–depressurization can overcome the ink-bottle effect and enables a distinction between large (ink-bottle) pores and small (throat) pores. In this paper, pressurization–depressurization cycling mercury intrusion porosimetry (PDC-MIP) is adopted to characterize the pore structure in a range of cementitious pastes cured from 28 to 370 days. The results indicate that PDC-MIP provides a more accurate estimation of the pore size distribution in cementitious pastes than the standard MIP. Bimodal pore size distributions can be obtained by performing PDC-MIP measurements on cementitious pastes, regardless of the age. Water–binder ratio, fly ash and limestone powder have considerable influences on the formation of capillary pores ranging from 0.01 to 0.5 µm.

A Direct and Quantitative Three-Dimensional Reconstruction of the Internal Structure of Disordered Mesoporous Carbon with Tailored Pore Size

2013 ◽  
Vol 19 (3) ◽  
pp. 745-750 ◽  
Author(s):  
Juan Balach ◽  
Flavio Soldera ◽  
Diego F. Acevedo ◽  
Frank Mücklich ◽  
César A. Barbero
Keyword(s):  
Pore Size ◽  
Focused Ion Beam ◽  
Ion Beam ◽  
Three Dimensional ◽  
Quantitative Characterization ◽  
Resorcinol Formaldehyde ◽  
Dual Beam ◽  
Dimensional Reconstruction ◽  
A New Technique

AbstractA new technique that allows direct three-dimensional (3D) investigations of mesopores in carbon materials and quantitative characterization of their physical properties is reported. Focused ion beam nanotomography (FIB-nt) is performed by a serial sectioning procedure with a dual beam FIB-scanning electron microscopy instrument. Mesoporous carbons (MPCs) with tailored mesopore size are produced by carbonization of resorcinol-formaldehyde gels in the presence of a cationic surfactant as a pore stabilizer. A visual 3D morphology representation of disordered porous carbon is shown. Pore size distribution of MPCs is determined by the FIB-nt technique and nitrogen sorption isotherm methods to compare both results. The obtained MPCs exhibit pore sizes of 4.7, 7.2, and 18.3 nm, and a specific surface area of ca. 560 m2/g.

scholarly journals Morphological Characterization of Nanofibers: Methods and Application in Practice

2012 ◽  
Vol 2012 ◽  
pp. 1-14 ◽  
Author(s):  
Jakub Širc ◽  
Radka Hobzová ◽  
Nina Kostina ◽  
Marcela Munzarová ◽  
Martina Juklíčková ◽  
...  
Keyword(s):  
Specific Surface ◽  
Mercury Porosimetry ◽  
Three Dimensional ◽  
Nitrogen Adsorption ◽  
Morphological Characterization ◽  
Biologically Active ◽  
Porous Scaffolds ◽  
Electrospinning Technique ◽  
Pore Size Distributions

Biomedical applications such as wound dressing for skin regeneration, stem cell transplantation, or drug delivery require special demands on the three-dimensional porous scaffolds. Besides the biocompatibility and mechanical properties, the morphology is the most important attribute of the scaffold. Specific surface area, volume, and size of the pores have considerable effect on cell adhesion, growth, and proliferation. In the case of incorporated biologically active substances, their release is also influenced by the internal structure of nanofibers. Although many scientific papers are focused on the preparation of nanofibers and evaluation of biological tests, the morphological characterization was described just briefly as service methods. The aim of this paper is to summarize the methods applicable for morphological characterization of nanofibers and supplement it by the results of our research. Needleless electrospinning technique was used to prepare nanofibers from polylactide, poly(ε-caprolactone), gelatin, and polyamide. Scanning electron microscopy was used to evaluate the fiber diameters and to reveal eventual artifacts in the nanofibrous structure. Nitrogen adsorption/desorption measurements were employed to measure the specific surface areas. Mercury porosimetry was used to determine total porosities and compare pore size distributions of the prepared samples.

Fabrication and Characterization of Diatomite Functionalized Cellulose Acetate Nanofibers

2019 ◽  
Vol 6 (3) ◽  
pp. 28-36
Author(s):  
Çiğdem Akduman
Keyword(s):  
Pore Size ◽  
Cellulose Acetate ◽  
High Specific Surface Area ◽  
High Porosity ◽  
Size Distributions ◽  
Mean Flow ◽  
Water Contact ◽  
Pore Size Distributions ◽  
Nanofiber Membranes

Cellulose acetate (CA) nanofiber membranes incorporated with diatomite (DE) were prepared by electrospinning to produce electrospun nanofiber membranes with high specific surface area and high porosity with fine pores. When the DE percentage increased from 0 to 30%, the water contact angle (WCA) of the membranes increased from 86.21° to 118.44°, indicating that neat CA nanofibers were more hydrophilic than CA/DE nanofibers and had a better wetting tendency. CA, CA-10DE, and CA-20DE nanofiber membranes showed a mean flow pore size (MFP) of 2.941, 2.681, and 2.408 μm, respectively, with narrow pore size distributions. However, the CA-30DE nanofiber membrane showed a smaller MFP size of 0.5014 μm. CA nanofibers were produced in the range of 206.31 to 281.13 nm. The dye removal ability of these membranes was tested using an aqueous solution of C.I. Reactive Red 141.

scholarly journals Three-dimensional characterization of a fractured granite and transport properties

2000 ◽  
Vol 105 (B9) ◽  
pp. 21387-21401 ◽  
Author(s):  
R. Gonzalez-Garcia ◽  
O. Huseby ◽  
J.-F. Thovert ◽  
B. Ledésert ◽  
P. M. Adler
Keyword(s):  
Transport Properties ◽  
Three Dimensional ◽  
Fractured Granite
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