EXPERIMENTAL STUDY ON STEADY DYNAMIC FRICTION OF MWCNTs MIXED LUBRICANTS

2019 ◽  
Vol 27 (07) ◽  
pp. 1950172
Author(s):  
SHRADDHA GONDANE ◽  
ARUN K. SINGH ◽  
NITISH SINHA ◽  
R. P. VIJAYAKUMAR
Keyword(s):  
Critical Velocity ◽  
Scaling Laws ◽  
Dynamic Stress ◽  
Curve Surface ◽  
Surface Damage ◽  
Stribeck Curve ◽  
Frictional Stress ◽  
Multiwalled Carbon ◽  
Direct Shear Tests ◽  
Metal Metal

This paper investigates the steady sliding behavior of multiwalled carbon nanotubes (MWCNTs) mixed lubricants at the metal–metal interface in direct shear tests. Slide-free-slide (SFS) experiments were performed to understand dynamic frictional stress of the sliding surfaces above the critical velocity. The experimental observations show that the dynamic stress decreases with increase in sliding velocity, but the same increases with normal stress. Further, in the case of change in concentration of the MWCNTs in the lubricant, the dynamic stress increases initially and then decreases to a minimum value and then further increases with addition of more nanoparticles in the lubricant. Dynamic stress and corresponding critical velocity are found to be minimum about 1.6% (wt./vol.) of MWCNTs concentration. Magnitude of cohesion as well as the coefficient of friction were also determined experimentally with the Coulomb friction law. The friction results are discussed in terms of the scaling laws in three regimes, namely viscous, rolling and sliding. These laws are justified on the basis of the mixed lubrication regime of Stribeck curve. Surface morphology of the test specimens before and after the experiment was also examined using SEM and EDS tests. No evidence of surface damage owing to motion of the nanoparticles was observed.

scholarly journals Permeability Experiment of Fractured Rock with Rough Surfaces under Different Stress Conditions

Geofluids ◽  
2020 ◽  
Vol 2020 ◽  
pp. 1-15 ◽  
Author(s):  
Zilong Zhou ◽  
Jing Zhang ◽  
Xin Cai ◽  
Shanyong Wang ◽  
Xueming Du ◽  
...  
Keyword(s):  
Fracture Surface ◽  
Dynamic Stress ◽  
Rough Surfaces ◽  
Fractured Rock ◽  
Great Influence ◽  
Surface Damage ◽  
Testing System ◽  
Material Transport ◽  
Fracture Surfaces ◽  
Before And After

To investigate the permeability changes and the mechanisms of fractured rock under dynamic and static stresses produced by earthquakes, permeability experiments on fractured rock with rough surfaces under axial dynamic and static stresses were conducted on the MTS815 Rock Mechanics Testing System. Surface asperity was investigated by scanning the specimen surfaces before and after testing. The results show that the roughness of fracture surface has a great influence on the permeability when the axial displacement is not enough to cause the fracture rock to slip. Moreover, the rougher fracture surface leads to severer surface damage as indicated by the more gouge productions. The accumulation of gouge materials on larger roughness fracture surfaces causes a slow drop in permeability. The fracture surfaces experience larger degradations, but it has small weights of gouge materials on fracture surface after testing under axial dynamic stress. The reason is that the gouge material transport and mobilization tend to occur in process of dynamic loading. Therefore, the permeability drops of axial dynamic stress are larger than those of axial static stress.

Fillers and Dissolvent in Porous Self-Generating Fine Super-Hard Abrasive Tool

2010 ◽  
Vol 135 ◽  
pp. 398-403 ◽  
Author(s):  
Hong Wei Fan ◽  
Bing Hai Lv ◽  
Ju Long Yuan ◽  
Q.F. Deng ◽  
W.F. Yao
Keyword(s):  
Metal Oxide ◽  
Surface Damage ◽  
Ceramic Materials ◽  
Precision Machining ◽  
Machining Efficiency ◽  
Metallic Oxide ◽  
Advanced Ceramics ◽  
Key Technology ◽  
Fecl3 Solution ◽  
Metal Metal

In order to obtain low surface damage and high machining efficiency for advanced ceramics, overcome clogging and dressing difficulties of traditional metal bonded super-hard abrasive, a novel fine super-hard abrasive with porous self-generating ability is proposed in this paper. And the matching of filler and dissolvent in abrasive are studied. Soluble filler is a key technology of porous self-generating fine super-hard abrasive. In this paper, metal, metal oxide and non-metallic oxide are respectively used as soluble fillers. Results of the experimental shows: In metal bonded super-hard abrasive, metal, metal oxide and non-metallic oxide as soluble filler are feasible, correspondingly, FeCl3 solution, aqueous solution and weak alkaline solution are used as dressing dissolvent, respectively. It can be met the requirement of high precision machining for advanced ceramic materials, hard and brittle machining materials.

Siphon Flows in Stratified Coronal Loops

1994 ◽  
Vol 144 ◽  
pp. 185-187
Author(s):  
S. Orlando ◽  
G. Peres ◽  
S. Serio
Keyword(s):  
Heat Flux ◽  
Scaling Laws ◽  
Flow Model ◽  
Supersonic Flows ◽  
Coronal Loops ◽  
Characteristic Parameters

AbstractWe have developed a detailed siphon flow model for coronal loops. We find scaling laws relating the characteristic parameters of the loop, explore systematically the space of solutions and show that supersonic flows are impossible for realistic values of heat flux at the base of the upflowing leg.

Surface Structure in Microtomed Sections Caused by Glass and Diamond Knives

1971 ◽  
Vol 29 ◽  
pp. 456-457
Author(s):  
J. Temple Black ◽  
William G. Boldosser
Keyword(s):  
Plastic Deformation ◽  
Epoxy Resin ◽  
Carbon Coating ◽  
Surface Damage ◽  
Body Angle ◽  
Normal Manner ◽  
Bottom Side ◽  
Cutting Direction ◽  
Made In ◽  
Diamond Knife

Ultramicrotomy produces plastic deformation in the surfaces of microtomed TEM specimens which can not generally be observed unless special preparations are made. In this study, a typical biological composite of tissue (infundibular thoracic attachment) infiltrated in the normal manner with an embedding epoxy resin (Epon 812 in a 60/40 mixture) was microtomed with glass and diamond knives, both with 45 degree body angle. Sectioning was done in Portor Blum Mt-2 and Mt-1 microtomes. Sections were collected on formvar coated grids so that both the top side and the bottom side of the sections could be examined. Sections were then placed in a vacuum evaporator and self-shadowed with carbon. Some were chromium shadowed at a 30 degree angle. The sections were then examined in a Phillips 300 TEM at 60kv.Carbon coating (C) or carbon coating with chrom shadowing (C-Ch) makes in effect, single stage replicas of the surfaces of the sections and thus allows the damage in the surfaces to be observable in the TEM. Figure 1 (see key to figures) shows the bottom side of a diamond knife section, carbon self-shadowed and chrom shadowed perpendicular to the cutting direction. Very fine knife marks and surface damage can be observed.

Quasiperiodic interfaces: HREM observations of grain and phase boundaries

1990 ◽  
Vol 48 (4) ◽  
pp. 332-333
Author(s):  
K. L. Merkle
Keyword(s):  
Atomic Structure ◽  
Direct Determination ◽  
Lattice Parameter ◽  
Atomic Scale ◽  
Misfit Dislocations ◽  
Oxide Systems ◽  
Atomic Structures ◽  
Periodic Arrays ◽  
Parameter Ratio ◽  
Metal Metal

The atomic structures of internal interfaces have recently received considerable attention, not only because of their importance in determining many materials properties, but also because the atomic structure of many interfaces has become accessible to direct atomic-scale observation by modem HREM instruments. In this communication, several interface structures are examined by HREM in terms of their structural periodicities along the interface.It is well known that heterophase boundaries are generally formed by two low-index planes. Often, as is the case in many fcc metal/metal and metal/metal-oxide systems, low energy boundaries form in the cube-on-cube orientation on (111). Since the lattice parameter ratio between the two materials generally is not a rational number, such boundaries are incommensurate. Therefore, even though periodic arrays of misfit dislocations have been observed by TEM techniques for numerous heterophase systems, such interfaces are quasiperiodic on an atomic scale. Interfaces with misfit dislocations are semicoherent, where atomically well-matched regions alternate with regions of misfit. When the misfit is large, misfit localization is often difficult to detect, and direct determination of the atomic structure of the interface from HREM alone, may not be possible.

Characterization of interfaces in CVD-coated nicalon fiber-reinforced SiC

1989 ◽  
Vol 47 ◽  
pp. 556-557
Author(s):  
K.L. More ◽  
R.A. Lowden
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Chemical Vapor ◽  
Chemical Vapor Infiltration ◽  
Frictional Stress ◽  
Fiber Reinforced ◽  
Pull Out ◽  
Carbon Coated ◽  
Fiber Matrix

The mechanical properties of fiber-reinforced composites are directly related to the nature of the fiber-matrix bond. Fracture toughness is improved when debonding, crack deflection, and fiber pull-out occur which in turn depend on a weak interfacial bond. The interfacial characteristics of fiber-reinforced ceramics can be altered by applying thin coatings to the fibers prior to composite fabrication. In a previous study, Lowden and co-workers coated Nicalon fibers (Nippon Carbon Company) with silicon and carbon prior to chemical vapor infiltration with SiC and determined the influence of interfacial frictional stress on fracture phenomena. They found that the silicon-coated Nicalon fiber-reinforced SiC had low flexure strengths and brittle fracture whereas the composites containing carbon coated fibers exhibited improved strength and fracture toughness. In this study, coatings of boron or BN were applied to Nicalon fibers via chemical vapor deposition (CVD) and the fibers were subsequently incorporated in a SiC matrix. The fiber-matrix interfaces were characterized using transmission and scanning electron microscopy (TEM and SEM). Mechanical properties were determined and compared to those obtained for uncoated Nicalon fiber-reinforced SiC.

Quantitative surface damage studies by H.R.E.M.

1989 ◽  
Vol 47 ◽  
pp. 632-633
Author(s):  
S. R. Singh ◽  
H. J. Fan ◽  
L. D. Marks
Keyword(s):  
Solar Wind ◽  
Quantitative Analysis ◽  
Surface Science ◽  
Surface Damage ◽  
Space Environment ◽  
Oxygen Desorption ◽  
The Past ◽  
Diffusion Controlled ◽  
Original Observation ◽  
Substantial Interest

Since the original observation that the surfaces of materials undergo radiation damage in the electron microscope similar to that observed by more conventional surface science techniques there has been substantial interest in understanding these phenomena in more detail; for a review see. For instance, surface damage in a microscope mimics damage in the space environment due to the solar wind and electron beam lithographic operations.However, purely qualitative experiments that have been done in the past are inadequate. In addition, many experiments performed in conventional microscopes may be inaccurate. What is needed is careful quantitative analysis including comparisons of the behavior in UHV versus that in a conventional microscope. In this paper we will present results of quantitative analysis which clearly demonstrate that the phenomena of importance are diffusion controlled; more detailed presentations of the data have been published elsewhere.As an illustration of the results, Figure 1 shows a plot of the shrinkage of a single, roughly spherical particle of WO3 versus time (dose) driven by oxygen desorption from the surface.

Study of Tip-Surface Interactions in Scanning Tunneling Microscopy (STM) by Reflection Electron Microscopy (REM)

1990 ◽  
Vol 48 (1) ◽  
pp. 320-321
Author(s):  
W. Lo ◽  
J.C.H. Spence ◽  
M. Kuwabara
Keyword(s):  
High Resolution ◽  
Elastic Strain ◽  
Tunneling Current ◽  
Surface Damage ◽  
Surface Interactions ◽  
Graphite Surface ◽  
Scanning Tunneling ◽  
Large Area ◽  
Tunneling Microscopy ◽  
High Resolution Tem

Work on the integration of STM with REM has demonstrated the usefulness of this combination. The STM has been designed to replace the side entry holder of a commercial Philips 400T TEM. It allows simultaneous REM imaging of the tip/sample region of the STM (see fig. 1). The REM technique offers nigh sensitivity to strain (<10−4) through diffraction contrast and high resolution (<lnm) along the unforeshortened direction. It is an ideal technique to use for studying tip/surface interactions in STM.The elastic strain associated with tunnelling was first imaged on cleaved, highly doped (S doped, 5 × 1018cm-3) InP(110). The tip and surface damage observed provided strong evidence that the strain was caused by tip/surface contact, most likely through an insulating adsorbate layer. This is consistent with the picture that tunnelling in air, liquid or ordinary vacuum (such as in a TEM) occurs through a layer of contamination. The tip, under servo control, must compress the insulating contamination layer in order to get close enough to the sample to tunnel. The contaminant thereby transmits the stress to the sample. Elastic strain while tunnelling from graphite has been detected by others, but never directly imaged before. Recent results using the STM/REM combination has yielded the first direct evidence of strain while tunnelling from graphite. Figure 2 shows a graphite surface elastically strained by the STM tip while tunnelling (It=3nA, Vtip=−20mV). Video images of other graphite surfaces show a reversible strain feature following the tip as it is scanned. The elastic strain field is sometimes seen to extend hundreds of nanometers from the tip. Also commonly observed while tunnelling from graphite is an increase in the RHEED intensity of the scanned region (see fig.3). Debris is seen on the tip and along the left edges of the brightened scan region of figure 4, suggesting that tip abrasion of the surface has occurred. High resolution TEM images of other tips show what appear to be attached graphite flakes. The removal of contamination, possibly along with the top few layers of graphite, seems a likely explanation for the observed increase in RHEED reflectivity. These results are not inconsistent with the “sliding planes” model of tunnelling on graphite“. Here, it was proposed that the force due to the tunnelling probe acts over a large area, causing shear of the graphite planes when the tip is scanned. The tunneling current is then modulated as the planes of graphite slide in and out of registry. The possiblity of true vacuum tunnelling from the cleaned graphite surface has not been ruled out. STM work function measurements are needed to test this.

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