scholarly journals Microstructure and mechanical properties of A357/SiC nanocomposites fabricated by ultrasonic cavitation-based dispersion of ball-milled nanoparticles

2016 ◽  
Vol 51 (3) ◽  
pp. 395-404 ◽  
Author(s):  
Sinan Kandemir

In this work, A357/0.5 wt.% SiC nanocomposites were fabricated with a combination of ultrasonic processing and a nanoparticle feeding mechanism that involves the introduction of a closed end aluminium tube filled with the ball-milled SiC nanoparticles (20–30 nm) and aluminium powders (<75 µm) into the melt for complete deagglomeration and uniform dispersion of nanoparticles through the matrix. The microstructural and mechanical properties of the fabricated nanocomposites were investigated. The microstructural studies conducted with optical and advanced electron microscopes indicate that relatively effective deagglomeration and uniform dispersion of SiC nanoparticles into the molten alloy were achieved. The hardness and tensile properties of the nanocomposites were notably improved compared to those of the ultrasonically processed A357 alloy without reinforcement, showing the strengthening potency of nanoparticles and the good bonding obtained at the particle-reinforcement interface.

2021 ◽  
Vol 1023 ◽  
pp. 45-52
Author(s):  
Xiao Yan Wang ◽  
Meng Li ◽  
Zhi Xun Wen

After solid solution treatment at 1335°C for 4 hours and cooling to room temperature at different rate, the nickel-based single crystal superalloy were made into three kinds of nickel-based single crystal superalloy materials containing different size γ′ phases, respectively. The tensile test of I-shaped specimens was carried out at 980°C, and their effect of γ′ phase microstructure on the tensile properties was studied. The results show that the yielding strength of the material air-cooled to room temperature was lower than that with cooling rate at 0.15°C/s, but both of them were lower than the yielding strength of original material. Little difference was found on the elastic modulus of I-shaped specimens made of three kinds of materials. When the cubic degree of the γ′ phase is higher and the size is larger, the tensile properties of the material is better, which can be attributed to the larger size and narrower channel of the matrix phase that lead to higher dislocation resistance.


Polymers ◽  
2019 ◽  
Vol 11 (5) ◽  
pp. 842 ◽  
Author(s):  
Weiwei Zhang ◽  
Jin Gu ◽  
Dengyun Tu ◽  
Litao Guan ◽  
Chuanshuang Hu

Paper fibers have gained broad attention in natural fiber reinforced composites in recent years. The specific problem in preparing paper fiber reinforced composites is that paper fibers easily become flocculent after pulverization, which increases difficulties during melt-compounding with polymer matrix and results in non-uniform dispersion of paper fibers in the matrix. In this study, old newspaper (ONP) was treated with a low dosage of gaseous methyltrichlorosilane (MTCS) to solve the flocculation. The modified ONP fibers were characterized by Scanning Electron Microscope (SEM), Fourier Transform Infrared Spectroscopy (FTIR), and Thermogravimetric Analysis (TG). Then the modified ONP fibers and high-density polyethylene (HDPE) were extruded and pelletized to prepare ONP/HDPE composites via injection molding. Maleic anhydride-grafted polyethylene (MAPE) was added to enhance the interfacial bonding performance with the ultimate purpose of improving the mechanical strength of the composites. The mechanical properties such as tensile, flexural, and impact strength and the water absorption properties of the composite were tested. The results showed that the formation of hydrogen bonding between ONP fibers was effectively prevented after MTCS treatment due to the reduction of exposed –OH groups at the fiber surface. Excessive dosage of MTCS led to severe fiber degradation and dramatically reduced the aspect ratio of ONP fibers. Composites prepared with ONP fibers modified with 4% (v/w) MTCS showed the best mechanical properties due to reduced polarity between the fibers and the matrix, and the relatively long aspect ratio of treated ONP fibers. The composite with or without MAPE showed satisfactory water resistance properties. MTCS was proven to be a cheap and efficient way to pretreat old newspaper for preparing paper fiber reinforced composites.


2005 ◽  
Vol 13 (2) ◽  
pp. 139-150 ◽  
Author(s):  
Zhanpai Su ◽  
Pingkai Jiang ◽  
Qiang Li ◽  
Ping Wei ◽  
Yong Zhang

The flame retardant and mechanical properties of polypropylene (PP), highly filled with aluminum hydroxide (Al(OH)3) and toughened with ethylene propylene diene monomer (EPDM) and zinc neutralized sulfated EPDM ionomer (Zn-S-EPDM), were studied along with their morphology. The PP matrix when highly filled with Al(OH)3 particles can achieve an adequate level of flame retardancy, but there is a decrease in the mechanical properties because of inadequate adhesion between the Al(OH)3 particles and the PP matrix and the strong tendency of the filler to agglomerate. The rubber incorporated in the PP/Al(OH)3 composites has two roles: as compatibilizer and toughening agent. Although ordinary EPDM significantly improves the Izod impact strength of the composites, the tensile properties are much worse because of the weak interfacial adhesion between the modifier and the matrix. Using Zn-S-EPDM instead EPDM, the tensile properties are much improved with only a slight decrease in toughness, because of improvements in the interfacial adhesion between modifier and matrix. SEM micrographs show that the rubber phase is dispersed in the continuous PP matrix and that most Al(OH)3 particles are uniformly distributed in the rubbery phase. Larger, obviously rubbery, domains can be seen in the PP/EPDM/Al(OH)3 ternary composites. Much finer rubbery domains were found in the PP/Zn-S-EPDM/Al(OH)3 composites.


2017 ◽  
Vol 36 (4) ◽  
pp. 381-387 ◽  
Author(s):  
Yang Xuan ◽  
Shian Jia ◽  
Laurentiu Nastac

AbstractRecent studies have showed that the microstructure and mechanical properties of A356 alloy can be significantly improved when ultrasonic cavitation and solidification processing is used. This is because during the fabrication of A356 castings, ultrasonic cavitation processing plays an important role in degassing and refining the as-cast microstructure. In the present study, A356 alloy and Al2O3/SiC nanoparticles are used as the matrix alloy and the reinforcements, respectively. Nanoparticles are injected into the molten alloy and dispersed by ultrasonic cavitation. Ultrasonic cavitation was also applied during solidification of these nanocomposites. The microstructure and nanoparticle distribution of the cast samples have been investigated in detail. The current experimental results indicated that ultrasonic cavitation during solidification will greatly improve the microstructure of the samples. Al2O3 and SiC nanoparticle reinforced nanocomposites have different nanoparticle distributions in the matrix.


2019 ◽  
Vol 130 ◽  
pp. 01040 ◽  
Author(s):  
Yuniar Ratna Pratiwi ◽  
Indah Widiastuti ◽  
Budi Harjanto

The aim of this article is to evaluate water absorption in bamboo fiber composites. Bamboo is hydrophilic, means that it easily absorbs water. In this study the bamboo fiber-based composites were developed using hand lay up method, with epoxy resin as the matrix constituent. Water absorption characteristics of specimens of bamboo composite and epoxy were determined from water immersion tests at several temperatures. Gravimetric analysis was performed to determine the moisure absorbed as a function of time at two different temperatures: 25 ºC and 50 C. The diffusivity of water in an epoxy bamboo composite was determined after reaching saturation point. During room temperature soaking, epoxy specimen showed the characteristic of Fickian behavior. Similar immersion tests on bamboo-epoxy composites followed nonfickian behavior. Changes in the mechanical properties of material due to water absorption were evaluated from tensile testing on materials with varied water content. It was found that the waterabsorption in all samples reduced the tensile properties. The degradation of tensile properties was greater with an increasing temperature of immersion. The results of this study emphasize the importance ofconsidering deterioration of mechanical properties in the bamboo epoxy composites during their application in water and possibly in humid environment.


2010 ◽  
Vol 150-151 ◽  
pp. 792-795 ◽  
Author(s):  
Hong Yan ◽  
Zhi Hu

SiC nanoparticles reinforced AZ61 magnesium composites were fabricated by Ultrasonic method. The distribution of nanoparticles in the matrix and the fracture morphology of the composites were observed by SEM, and the mechanical properties of the composites were tested at room temperature. Experimental shows that SiC nanoparticles were dispersed well in the matrix with the pretreatment method. Compared with the matrix, the tensile strength and hardness of the composites were improved respectively. Meanwhile, the ductility of the composites didn’t be obviously decreased. The enhancement function of nano composites was predicted with the dislocation strengthening and Orowan dispersion strengthening mechanisms. The predicted results coincided well with experimental ones.


2007 ◽  
Vol 546-549 ◽  
pp. 499-502
Author(s):  
X. Qiu ◽  
Xiao Jun Wang ◽  
Ming Yi Zheng ◽  
Kun Wu

The fabrication processing, mechanical properties and fracture characters of SiCp/AZ91 magnesium matrix composites fabricated by squeeze casting were investigated. The SiC particles with different diameters (5μm, 20μm and 50μm) were employed as the reinforcement in the composites, the volume fraction of them was 50% in all cases. Experimental results showed that when the size of SiC particle decreased, the tensile properties of the composite increased. The tensile properties of SiCp/AZ91 composite with small particles are controlled by the properties of matrix alloy and the strength of the interface between the matrix and reinforcements, but the composites reinforced by large particles are controlled by the fracture of the particles.


2012 ◽  
Vol 585 ◽  
pp. 297-300 ◽  
Author(s):  
Prakriti Kumar Ghosh ◽  
Manjeet Singh Goyat ◽  
Deepak Mishra ◽  
Rishabh Nagori

The effect of type of nanoparticles on morphology, thermal and mechanical properties of epoxy-nanoparticulate composite adhesive produced via ultrasonic vibration process has been investigated. The morphology, thermal and mechanical properties of epoxy-nanoparticulate composite adhesive was measured with FESEM/AFM, DTA/TGA, and Hounsfield respectively. The FESEM/AFM images of the epoxy-nanoparticulate composite adhesive reveals significantly fine dispersion of nanoparticles. The incorporation TiO2 nanoparticles in epoxy adhesive results in improved glass transition temperature (Tg), thermal stability and tensile properties of the nanocomposite. But, the incorporation of comparatively finer size Al2O3 nanoparticles leads to decrease in the Tg, thermal stability and tensile properties of the nanocomposite.


2008 ◽  
Vol 569 ◽  
pp. 89-92
Author(s):  
Xi Hai Jin ◽  
Lian Gao ◽  
Jing Sun

SiC/ZTM nanocomposites were prepared, and the influence of nanosized SiC addition on the microstructure and mechanical properties were investigated. It was found that the addition of nanosized SiC significantly retarded the matrix grain growth, making the microstructure much finer and more uniform. This led to a significant improvement in the mechanical properties. And further enhancement in the mechanical property can be achieved through the addition of mullite seeds in the starting powder and improving the distribution homogeneity of SiC nanoparticles in the matrix.


2009 ◽  
Vol 618-619 ◽  
pp. 449-452 ◽  
Author(s):  
Shi Ying Liu ◽  
Fei Peng Gao ◽  
Qiong Yuan Zhang ◽  
Wen Zhen Li

A high intensity ultrasonic assisted casting method was used to fabricate SiC nanoparticles reinforced magnesium matrix nanocomposites (n-SiCp/AZ91D). The microstructures and mechanical properties of the nanocomposites were investigated. The results show that n-SiCp are well dispersed in the matrix and the grain size was refined. A HRTEM study of the interface between n-SiCp and the matrix suggests that SiC bonds well with matrix without forming an intermediate phase. With the lower addition of n-SiCp, the mechanical properties of nanocomposites are greatly improved. As compared to an unreinforced magnesium alloy matrix, the tensile and yield strength were improved by 43.6% and 117% respectively.


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