scholarly journals Thermal Stability of Nanocrystalline Structure In X37CrMoV5-l Steel

2015 ◽  
Vol 60 (1) ◽  
pp. 511-516 ◽  
Author(s):  
E. Skołek ◽  
S. Marciniak ◽  
W.A. Świątnicki
Keyword(s):  
Thermal Stability ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Bainitic Ferrite ◽  
Nanocrystalline Structure ◽  
Thin Layers ◽  
Isothermal Quenching ◽  
Initial Stage ◽  
Increasing Temperature ◽  
Thermal Stability Of

AbstractThe aim of the study was to investigate the thermal stability of the nanostructure produced in X37CrMoV5-1 tool steel by austempering heat treatment consisted of austenitization and isothermal quenching at the range of the bainitic transformation. The nanostructure was composed of bainitic ferrite plates of nanometric thickness separated by thin layers of retained austenite. It was revealed, that the annealing at the temperature higher than temperature of austempering led to formation of cementite precipitations. At the initial stage of annealing cementite precipitations occurred in the interfaces between ferritic bainite and austenite. With increasing temperature of annealing, the volume fraction and size of cementite precipitations also increased. Simultaneously fine spherical Fe7C3carbides appeared. At the highest annealing temperature the large, spherical Fe7C3carbides as well as cementite precipitates inside the ferrite grains were observed. Moreover the volume fraction of bainitic ferrite and of freshly formed martensite increased in steel as a result of retained austenite transformation during cooling down to room temperature.

scholarly journals The Effect of Stepped Austempering on Phase Composition and Mechanical Properties of Nanostructured X37CrMoV5-1 Steel

2015 ◽  
Vol 60 (1) ◽  
pp. 517-521
Author(s):  
S. Marciniak ◽  
E. Skołek ◽  
W. Świątnicki
Keyword(s):  
Mechanical Properties ◽  
Retained Austenite ◽  
Isothermal Annealing ◽  
Volume Fraction ◽  
Bainitic Ferrite ◽  
High Volume ◽  
Thin Layers ◽  
Strength Parameters ◽  
One Step ◽  
Step Heat Treatment

AbstractThis paper presents the results of studies of X37CrMoV5-1 steel subjected to quenching processes with a one-step and a two-step isothermal annealing. The TEM observation revealed that steel after one-step treatment led is composed of carbide-free bainite with nanometric thickness of ferrite plates and of high volume fraction of retained austenite in form of thin layers or large blocks. In order to improve the strength parameters an attempt was made to reduce the austenite content by use of quenching with the two-step isothermal annealing. The temperature and time of each step were designed on the basis of dilatometric measurements. It was shown, that the two-step heat treatment led to increase of the bainitic ferrite content and resulted in improvement of steel's strength with no loss of steel ductility.

Thermal Stability of Retained Austenite in Advanced TRIP Steel with Bainitic Ferrite Matrix for Automotive Industries

2021 ◽  
Vol 1016 ◽  
pp. 429-434
Author(s):  
Eman El-Shenawy ◽  
Hoda Refaiy ◽  
Hoda Nasr El-Din
Keyword(s):  
Mechanical Properties ◽  
Thermal Stability ◽  
Retained Austenite ◽  
Bainitic Ferrite ◽  
Residual Austenite ◽  
Ferrite Matrix ◽  
Sheet Steels ◽  
Coiling Process ◽  
Hot Rolled ◽  
Thermal Stability Of

Multiphase steels consisting of retained austenite and martensite/bainite microstructures such as TRIP, low-temperature-bainite, and Q&P steels are attractive candidates for the new-generation of AHSS. These steels exhibit a remarkable combination of strength and toughness which is essential to meet the objective of weight reduction of engineering-components, while maintaining the compromise of tough-safety requirements. Such good mechanical properties are due to the enhanced work hardening rate caused by austenite-to-martensite transformation during deformation and the strengthening contribution of martensite/bainite. The retained austenite can thermally decompose into more thermodynamically stable phases as a consequence of temperature changes, which is referred to as the thermal stability of retained austenite. TRIP-aided steel is an effective candidate for automotive parts because of safety and weight reduction requirements. The strength–ductility balance of high strength steel sheets can be remarkably improved by using transformation induced plasticity behavior of retained austenite. In manufacturing hot rolled TRIP-aided sheet steels, austenite transforms into bainite during the coiling process. Because black hot coils cool slowly after the coiling process, they are exposed at about 350–450°C for a few hours or days. Therefore, the metastable residual austenite can be decomposed into other phases. This decomposition of residual austenite can produce serious deteriorate of mechanical properties in hot rolled TRIP-aided sheet steels. The present work identified the decomposition behavior and study the thermal stability of retained austenite in the TRIP-aided steel with bainitic/ferrite matrix depending on coiling temperatures and holding times by means of DSC and XRD analysis.

scholarly journals Thermal Stability of Retained Austenite and Properties of A Multi-Phase Low Alloy Steel

Metals ◽  
2018 ◽  
Vol 8 (10) ◽  
pp. 807 ◽  
Author(s):  
Zhenjia Xie ◽  
Lin Xiong ◽  
Gang Han ◽  
Xuelin Wang ◽  
Chengjia Shang
Keyword(s):  
Thermal Stability ◽  
High Temperature ◽  
Alloy Steel ◽  
Retained Austenite ◽  
Mechanical Stability ◽  
Volume Fraction ◽  
Low Carbon ◽  
Low Alloy Steel ◽  
Multi Phase ◽  
Thermal Stability Of

In this work, we elucidate the effects of tempering on the microstructure and properties in a low carbon low alloy steel, with particular emphasis on the thermal stability of retained austenite during high-temperature tempering at 500–700 °C for 1 h. Volume fraction of ~14% of retained austenite was obtained in the studied steel by two-step intercritical heat treatment. Results from transmission electron microscopy (TEM) and X-ray diffraction (XRD) indicated that retained austenite had high thermal stability when tempering at 500 and 600 °C for 1 h. The volume fraction was ~11–12%, the length and width remained ~0.77 and 0.21 μm, and concentration of Mn and Ni in retained austenite remained ~6.2–6.6 and ~1.6 wt %, respectively. However, when tempering at 700 °C for 1 h, the volume fraction of retained austenite was decreased largely to ~8%. The underlying reason could be attributed to the growth of austenite during high-temperature holding, leading to a depletion of alloy contents and a decrease in stability. Moreover, for samples tempered at 700 °C for 1 h, retained austenite rapidly transformed into martensite at a strain of 2–10%, and a dramatic increase in work hardening was observed. This indicated that the mechanical stability of retained austenite decreased.

scholarly journals Mechanical and thermal stability of retained austenite in plastically deformed bainite-based TRIP-aided medium-Mn steels

2021 ◽  
Vol 21 (3) ◽  
Author(s):  
Aleksandra Kozłowska ◽  
Adam Grajcar ◽  
Aleksandra Janik ◽  
Krzysztof Radwański ◽  
Ulrich Krupp ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Thermal Stability ◽  
Retained Austenite ◽  
Elevated Temperatures ◽  
Mechanical Performance ◽  
Mechanical Stability ◽  
Electron Backscatter Diffraction ◽  
Cost Effective ◽  
Tensile Tests ◽  
Thermal Stability Of

AbstractAdvanced medium-Mn sheet steels show an opportunity for the development of cost-effective and light-weight automotive parts with improved safety and optimized environmental performance. These steels utilize the strain-induced martensitic transformation of metastable retained austenite to improve the strength–ductility balance. The improvement of mechanical performance is related to the tailored thermal and mechanical stabilities of retained austenite. The mechanical stability of retained austenite was estimated in static tensile tests over a wide temperature range from 20 °C to 200 °C. The thermal stability of retained austenite during heating at elevated temperatures was assessed by means of dilatometry. The phase composition and microstructure evolution were investigated by means of scanning electron microscopy, electron backscatter diffraction, X-ray diffraction and transmission electron microscopy techniques. It was shown that the retained austenite stability shows a pronounced temperature dependence and is also stimulated by the manganese addition in a 3–5% range.

Isothermal Transformation, Microstructure and Mechanical Properties of Ausformed Low-Carbon Carbide-Free Bainitic Steel

2018 ◽  
Vol 941 ◽  
pp. 329-333 ◽  
Author(s):  
Jiang Ying Meng ◽  
Lei Jie Zhao ◽  
Fan Huang ◽  
Fu Cheng Zhang ◽  
Li He Qian
Keyword(s):  
Mechanical Properties ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Bainitic Ferrite ◽  
Isothermal Transformation ◽  
Bainitic Transformation ◽  
Isothermal Treatment ◽  
Bainitic Steel ◽  
Low Carbon ◽  
Microstructure And Mechanical Properties

In the present study, the effects of ausforming on the bainitic transformation, microstructure and mechanical properties of a low-carbon rich-silicon carbide-free bainitic steel have been investigated. Results show that prior ausforming shortens both the incubation period and finishing time of bainitic transformation during isothermal treatment at a temperature slightly above the Mspoint. The thicknesses of bainitic ferrite laths are reduced appreciably by ausforming; however, ausforming increases the amount of large blocks of retained austenite/martenisite and decreases the volume fraction of retained austenite. And accordingly, ausforming gives rise to significant increases in both yield and tensile strengths, but causes noticeable decreases in ductility and impact toughness.

Structure and Thermal Stability of Cu after Severe Plastic Deformation

2010 ◽  
Vol 297-301 ◽  
pp. 1312-1321 ◽  
Author(s):  
Vladimir V. Popov ◽  
A.V. Stolbovkiy ◽  
E.N. Popova ◽  
V.P. Pilyugin
Keyword(s):  
Thermal Stability ◽  
Plastic Deformation ◽  
Severe Plastic Deformation ◽  
High Pressure Torsion ◽  
Pure Copper ◽  
Nanocrystalline Structure ◽  
Transmission Electron ◽  
Evolution Of Structure ◽  
Stability Of Structure ◽  
Thermal Stability Of

Evolution of structure of high-purity and commercially pure copper at severe plastic deformation (SPD) by high pressure torsion (HPT) at room temperature and in liquid nitrogen has been studied by transmission electron microscopy (TEM) and measurements of microhardness. Thermal stability of structure obtained by HPT has been investigated. Factors preventing from obtaining nanocrystalline structure in Cu are analyzed and possible ways of their overcoming are discussed.

Effect of Chemistry Modification, Hot Forging and Partitioning on Low Alloy Grade Tool Steel

2018 ◽  
Vol 786 ◽  
pp. 75-83
Author(s):  
Ahmed Ismail Zaky Farahat ◽  
Mohamed Kamal El Fawkhry ◽  
Ayman M. Fathy ◽  
Taha M. Mattar
Keyword(s):  
Thermal Stability ◽  
Tool Steel ◽  
Retained Austenite ◽  
Treatment Process ◽  
Hot Forging ◽  
Optical Microscope ◽  
Isothermal Treatment ◽  
The Novel ◽  
Slow Cooling ◽  
Thermal Stability Of

Development of S6 tool steel has been discussed in this research by conducting a bit modification in the chemical composition using aluminum instead of molybdenum, and micro addition of boron to enhance the marteniste structure. Then, the hardenability and thermal stability have been detected in regarding to S6 tool steel. A novel isothermal treatment process has been suggested to enrich the retained austenite, and thereby, it has been tracked by using XRD, optical microscope, and SEM in conjugation with EDS. The effect of retained on the mechanical properties has been determined. The results ensure that aluminum has inhibited the graphite formation through the slow cooling regime. No change of hardenability or thermal stability of S6 tool steel triggered from adding of aluminum and microaddition of boron. In addition, the novel isothermal process leads to enrichment of retained austenite that has significantly affected on the combination of ductility with strength of the newly designed steel.

scholarly journals Microstructure and Mechanical Properties of Tempered Ausrolled Nanobainite Steel

Crystals ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 573
Author(s):  
Jing Zhao ◽  
Dezheng Liu ◽  
Yan Li ◽  
Yongsheng Yang ◽  
Tiansheng Wang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Ultimate Tensile Strength ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Bainitic Ferrite ◽  
Energy Yield ◽  
Partial Recovery ◽  
Fracture Appearance ◽  
The Impact

The microstructures and mechanical properties of ausrolled nanobainite steel, after being tempered at temperatures in the range of 200−400 °C, were investigated in this study. After being tempered, bainitic ferrite is coarsened and the volume fraction of retained austenite is reduced. The hardness and ultimate tensile strength decrease sharply. The impact energy, yield strength, and elongation increase with elevated tempered temperature at 200–300 °C but decrease with elevated tempered temperature when the samples are tempered at 350 °C and 400 °C. The fracture appearance of all the samples after impact tests is a brittle fracture. The variation of the mechanical properties may be due to partial recovery and recrystallization.

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