Micropatterned freestanding magnetron sputtered Mg-alloy scaffolds

2015 ◽  
Vol 16 (1) ◽  
Author(s):  
David Haffner ◽  
Christiane Zamponi ◽  
Rodrigo Lima de Miranda ◽  
Eckhard Quandt

AbstractFreestanding scaffolds were fabricated of Mg5W (wt.% yttrium) alloy using magnetron sputtering technology. Appropriate method was found to produce scaffolds with high reproducibility, spatial resolution of 1 μm and good mechanical properties. Two different techniques were used for surface finishing, microblasting and chemical polishing. SEM investigation showed high surface quality after chemical polishing while microblasting influenced mechanical properties of the Mg5W alloy. Magnetron sputtering offers a high potential for the production of microstructured scaffolds.

2008 ◽  
Vol 587-588 ◽  
pp. 157-161 ◽  
Author(s):  
Teresa P. Duarte ◽  
Rui J.L. Neto ◽  
Rui Félix ◽  
F. Jorge Lino

Companies are continuously under pressure to innovate their products and processes. In Portugal, there are already several examples of enterprises that have chosen research groups, associated to universities, to straighten collaboration seeking the development of new materials and advanced technological processes, to produce components with complex shapes, high surface quality, and others, at low cost, for continuously more demanding applications. Unfortunately, these cases are still a very small number, and many efforts have to be done to enlarge the collaboration university-companies. Ti and other reactive alloys are important groups of metals that are under intense and continuous research and development. For example, the high mechanical properties, low density, osteointegration behavior, corrosion resistance to fluids and tissues of the human body, the ability to be sterilized, and the possibility to obtain complex shapes, makes Ti a very attractive material for medical applications. The investment casting process, using lost wax or lost rapid prototyping models, allows designers a great amount of freedom and capacity to quickly produce castings of high dimensional accuracy and excellent surface quality suitable for different applications. Many of the castings obtained by this process are immediately ready for use, avoiding costly machining operations and joining processes, making the process very attractive to produce precision parts in Ti and other reactive alloys. However, the high reactivity of the Ti raises several compatibility problems with the traditional materials employed on the ceramic shells for casting steels and non ferrous alloys. The fragile surface layer obtained on the interface Ti-ceramic shell, result of the Ti reaction with oxygen and nitrogen of the shell, significantly reduces the mechanical properties of the cast parts, making them useless. The aim of the present work is the study of the interface properties of the Ti-ceramic shell, in order to be able to manufacture ceramic shells of low chemical reactivity for the investment casting process of reactive alloys, namely; titanium alloys, inconel, aluminotitanates, and others. Ceramic shells manufactured with calcium and yttria stabilized zirconia and other non reactive ceramics were employed and the metallic interface characterized in terms of microscopic and microhardness properties.


2010 ◽  
Vol 667-669 ◽  
pp. 217-222 ◽  
Author(s):  
Tina Hausöl ◽  
Heinz Werner Höppel ◽  
Matthias Göken

Among the well-known methods of severe plastic deformation the accumulative roll bonding (ARB) process is most promising for producing ultrafine-grained (UFG) materials with extraordinary mechanical properties at an industrial scale. Besides, it has also been shown that the ARB process can be successfully used to produce multi-component materials with tailored properties by reinforcement or grading, respectively. In this work, laminates with alternating layers of the high strength aluminium alloy AA5754 and the AA6014 alloy, well-known for good formability and high surface quality, were produced by ARB at 230 °C. Microstructural and mechanical investigations were performed after 2, 4 and 6 ARB cycles by means of light and electron microscopy, nanoindentation experiments and tensile testing. After ARB processing an ultrafine-grained microstructure is obtained. The UFG microstructure as well as the local mechanical properties alter with the layer composition. With increasing number of ARB cycles the interfaces between the layers become more and more wavy by shear band formation. Compared to the pure accumulative roll bonded AA6014 the yield and ultimate tensile strength of the multi-component laminates are considerably higher and are only slightly reduced in comparison to the high strength AA5754. In terms of elongation to failure no reduction in ductility is found. The serrated yielding effect, clearly visible in AA5754, is shifted to higher strains or fully disappears, respectively, whereas in AA5754 the magnitude of serrations increases with increasing number of ARB cycles. Combining AA5754 and AA6014 sheets by ARB results in well bonded ultrafine-grained laminates which exhibit a combination of the beneficial properties of the single-component materials: high strength of AA5754 and good surface quality of AA6014.


Author(s):  
Lukas Seeholzer ◽  
Stefan Süssmaier ◽  
Fabian Kneubühler ◽  
Konrad Wegener

AbstractEspecially for slicing hard and brittle materials, wire sawing with electroplated diamond wires is widely used since it combines a high surface quality with a minimum kerf loss. Furthermore, it allows a high productivity by machining multiple workpieces simultaneously. During the machining operation, the wire/workpiece interaction and thus the material removal conditions with the resulting workpiece quality are determined by the material properties and the process and tool parameters. However, applied to machining of carbon fibre reinforced polymers (CFRP), the process complexity potentially increases due to the anisotropic material properties, the elastic spring back potential of the material, and the distinct mechanical wear due to the highly abrasive carbon fibres. Therefore, this experimental study analyses different combinations of influencing factors with respect to process forces, workpiece surface temperatures at the wire entrance, and the surface quality in wire sawing unidirectional CFRP material. As main influencing factors, the cutting and feed speeds, the density of diamond grains on the wire, the workpiece thickness, and the fibre orientation of the CFRP material are analysed and discussed. For the tested parameter settings, it is found that while the influence of the grain density is negligible, workpiece thickness, cutting and feed speeds affect the process substantially. In addition, higher process forces and workpiece surface temperatures do not necessarily deteriorate the surface quality.


Machines ◽  
2021 ◽  
Vol 9 (4) ◽  
pp. 75
Author(s):  
Nikolaos E. Karkalos ◽  
Panagiotis Karmiris-Obratański ◽  
Szymon Kurpiel ◽  
Krzysztof Zagórski ◽  
Angelos P. Markopoulos

Surface quality has always been an important goal in the manufacturing industry, as it is not only related to the achievement of appropriate geometrical tolerances but also plays an important role in the tribological behavior of the surface as well as its resistance to fatigue and corrosion. Usually, in order to achieve sufficiently high surface quality, process parameters, such as cutting speed and feed, are regulated or special types of cutting tools are used. In the present work, an alternative strategy for slot milling is adopted, namely, trochoidal milling, which employs a more complex trajectory for the cutting tool. Two series of experiments were initially conducted with traditional and trochoidal milling under various feed and cutting speed values in order to evaluate the capabilities of trochoidal milling. The findings showed a clear difference between the two milling strategies, and it was shown that the trochoidal milling strategy is able to provide superior surface quality when the appropriate process parameters are also chosen. Finally, the effect of the depth of cut, coolant and trochoidal stepover on surface roughness during trochoidal milling was also investigated, and it was found that lower depths of cut, the use of coolant and low values of trochoidal stepover can lead to a considerable decrease in surface roughness.


2017 ◽  
Vol 36 (3) ◽  
pp. 151-166 ◽  
Author(s):  
Christian Hopmann ◽  
Nicolai Lammert ◽  
Yuxiao Zhang

Thermoplastic foam injection moulding offers various advantages for both processing and product design. Despite its many benefits, the moderate surface quality still constitutes a major disadvantage of this process. The mould temperature can be controlled dynamically to improve the surface quality. Different dynamic temperature control strategies are employed and analysed regarding their effectiveness and scope of application. Mould temperatures above the specific material transition temperatures allow the surface defects to be cured and enable the production of foamed thermoplastic parts with surface qualities comparable to those of the compact reference samples. The high mould temperatures during the injection phase alter the foam structure and the skin layer thicknesses, which impacts the mechanical properties.


Machines ◽  
2021 ◽  
Vol 9 (12) ◽  
pp. 325
Author(s):  
Muslim Mahardika ◽  
Martin Andre Setyawan ◽  
Tutik Sriani ◽  
Norihisa Miki ◽  
Gunawan Setia Prihandana

Titanium is widely used in biomedical components. As a promising advanced manufacturing process, electropolishing (EP) has advantages in polishing the machined surfaces of material that is hard and difficult to cut. This paper presents the fabrication of a titanium microchannel using the EP process. The Taguchi method was adopted to determine the optimal process parameters by which to obtain high surface quality using an L9 orthogonal array. The Pareto analysis of variance was utilized to analyze the three machining process parameters: applied voltage, concentration of ethanol in an electrolyte solution, and machining gap. In vitro experiments were conducted to investigate the fouling effect of blood on the microchannel. The result shows that an applied voltage of 20 V, an ethanol concentration of 20 vol.%, and a machining gap of 10 mm are the optimum machining parameters by which to enhance the surface quality of a titanium microchannel. Under the optimized machining parameters, the surface quality improved from 1.46 to 0.22 μm. Moreover, the adhesion of blood on the surface during the fouling experiment was significantly decreased, thus confirming the effectiveness of the proposed method.


2014 ◽  
Vol 1018 ◽  
pp. 269-276
Author(s):  
Andrea Reiß ◽  
Ulf Engel

With cold forging processes it is possible to produce parts characterized by high strength, high dimensional accuracy and high surface quality. In order to optimize the forming process and to be able to use the advantages of cold forging specifically and combined, it is necessary to find correlations between manufacturing parameters on the one side, strength and other properties like hardness distribution and surface quality of the component on the other side. The research work covered in this paper focuses on the correlation of the components properties influenced by its manufacturing history and their fatigue strength. The used component is a gear produced by a lateral cold forging process. For the investigations an experimental setup has been designed. The aim for the design of the setup is to reproduce the real contact condition for the contact of two gears. To obtain different component properties the production process of the gear was varied by producing the parts by a milling operation. First of all, the components’ properties, for example hardness distribution, remaining residual stresses, orientation of fibers and surface quality, were determined. The components’ fatigue behavior was determined using a high frequency pulsator and evaluated in terms of finite life fatigue strength and fatigue endurance limit. These examinations were used to produce Woehler curves for the differently manufactured components with a certain statistical data analysis method.


2013 ◽  
Vol 581 ◽  
pp. 211-216 ◽  
Author(s):  
Jiří Čop ◽  
Imrich Lukovics

This research paper focuses on grinding of materials used for tools (100Cr6 (CSN 4 14109), X210Cr12 ( CSN 4 19436) and epoxy resin) using grinding wheels from cubic boron nitride and diamond. The disadvantage of grinding of difficult-to-machine materials is higher wear of grinding wheels. The modern grinding wheels are able to achieve high accuracy of dimensions and high surface quality with a smaller wear of grinding wheels then grinding wheels from conventional materials. Correctly selected technological conditions are one of the most important matters to achieve the required surface quality. The main aim of this research is to determine the influence of technological conditions to quality of surface after planar grinding. The research determines the influence of the grain type of grinding wheels, feed rate and cutting depth on the quality of functional surfaces.


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