In situ x-ray CT under tensile loading using synchrotron radiation

1995 ◽  
Vol 10 (2) ◽  
pp. 381-386 ◽  
Author(s):  
T. Hirano ◽  
K. Usami ◽  
Y. Tanaka ◽  
C. Masuda

Internal damage in metal matrix composite (MMC) under static tensile loading was observed by in situ x-ray computed tomography based on synchrotron radiation (SR-CT). A tensile testing sample stage was developed to investigate the fracture process during the tensile test. Aluminum alloy matrix composites reinforced by long or short SiC fibers were used. The projection images obtained under tensile loading showed good performance of the sample stage, and matrix deformation and breaks of the long SiC fibers could be observed. In the CT images taken at the maximum stress just before failure, debondings of the short SiC fibers to the matrix, many pullouts of the fibers, and matrix cracking could be clearly observed. The in situ SR-CT allowed the observation of generation and growth of such defects under different tensile stress levels. The results from the nondestructive observation revealed that the MMC was broken by propagation of the matrix cracks which might be caused by stress concentration at the ends of the short fibers. A three-dimensional CT image reconstructed from many CT images provided easy understanding of the fiber arrangement, crack shape, and form of the void caused by fiber pullout. In situ SR-CT is a useful method for understanding failure mechanisms in advanced materials.

2017 ◽  
Vol 24 (2) ◽  
pp. 521-530 ◽  
Author(s):  
S. Huotari ◽  
Ch. J. Sahle ◽  
Ch. Henriquet ◽  
A. Al-Zein ◽  
K. Martel ◽  
...  

An end-station for X-ray Raman scattering spectroscopy at beamline ID20 of the European Synchrotron Radiation Facility is described. This end-station is dedicated to the study of shallow core electronic excitations using non-resonant inelastic X-ray scattering. The spectrometer has 72 spherically bent analyzer crystals arranged in six modular groups of 12 analyzer crystals each for a combined maximum flexibility and large solid angle of detection. Each of the six analyzer modules houses one pixelated area detector allowing for X-ray Raman scattering based imaging and efficient separation of the desired signal from the sample and spurious scattering from the often used complicated sample environments. This new end-station provides an unprecedented instrument for X-ray Raman scattering, which is a spectroscopic tool of great interest for the study of low-energy X-ray absorption spectra in materials under in situ conditions, such as in operando batteries and fuel cells, in situ catalytic reactions, and extreme pressure and temperature conditions.


2003 ◽  
Vol 321 (2-3) ◽  
pp. 221-232 ◽  
Author(s):  
A Yilmazbayhan ◽  
O Delaire ◽  
A.T Motta ◽  
R.C Birtcher ◽  
J.M Maser ◽  
...  

2007 ◽  
Vol 130 ◽  
pp. 7-14 ◽  
Author(s):  
Andrew N. Fitch

The highly-collimated, intense X-rays produced by a synchrotron radiation source can be harnessed to build high-resolution powder diffraction instruments with a wide variety of applications. The general advantages of using synchrotron radiation for powder diffraction are discussed and illustrated with reference to the structural characterisation of crystalline materials, atomic PDF analysis, in-situ and high-throughput studies where the structure is evolving between successive scans, and the measurement of residual strain in engineering components.


Author(s):  
Andrea Martini ◽  
Alexander A. Guda ◽  
Sergey A. Guda ◽  
Aram L. Bugaev ◽  
Olga V. Safonova ◽  
...  

Modern synchrotron radiation sources and free electron laser made X-ray absorption spectroscopy (XAS) an analytical tool for the structural analysis of materials under in situ or operando conditions. Fourier approach...


2009 ◽  
Vol 54 (5) ◽  
pp. 420-423 ◽  
Author(s):  
Tsunenori Matsunaga ◽  
Hidetaka Ishizaki ◽  
Shuji Tanabe ◽  
Yoshihiko Hayashi

2016 ◽  
Vol 83 (5) ◽  
Author(s):  
Brian Nyvang Legarth ◽  
Qingda Yang

Failure in elastic dual-phase materials under transverse tension is studied numerically. Cohesive zones represent failure along the interface and the augmented finite element method (A-FEM) is used for matrix cracking. Matrix cracks are formed at an angle of 55 deg−60 deg relative to the loading direction, which is in good agreement with experiments. Matrix cracks initiate at the tip of the debond, and for equi-biaxial loading cracks are formed at both tips. For elliptical reinforcement the matrix cracks initiate at the narrow end of the ellipse. The load carrying capacity is highest for ligaments in the loading direction greater than that of the transverse direction.


2015 ◽  
Vol 127 (47) ◽  
pp. 14129-14133 ◽  
Author(s):  
Letizia Monico ◽  
Koen Janssens ◽  
Ella Hendriks ◽  
Frederik Vanmeert ◽  
Geert Van der Snickt ◽  
...  

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