Strength of silicon containing nanoscale flaws

2004 ◽  
Vol 19 (2) ◽  
pp. 657-660 ◽  
Author(s):  
Antonia Pajares ◽  
Marina Chumakov ◽  
Brian R. Lawn

Silicon is a principal material in submicrometer-scale devices. Components in such devices are subject to intense local stress concentrations from nanoscale contacts during function. Questions arise as to the fundamental nature and extent of any strength-degrading damage incurred at such contacts on otherwise pristine surfaces. Here, a simple bilayer test procedure is adapted to probe the strengths of selected areas of silicon surfaces after nanoindentation with a Berkovich diamond. Analogous tests on silicate glass surfaces are used as a control. The strengths increase with diminishing contact penetration in both materials, even below thresholds for visible cracking at the impression corners. However, the strength levels in the subthreshold region are much lower in the silicon, indicating exceptionally high brittleness and vulnerability to small-scale damage in this material. The results have important implications in the design of devices with silicon components.

Author(s):  
Xiaozhi Wang ◽  
Joong-Kyoo Kang ◽  
Yooil Kim ◽  
Paul H. Wirsching

There are situations where a marine structure is subjected to stress cycles of such large magnitude that small, but significant, parts of the structural component in question experiences cyclic plasticity. Welded joints are particularly vulnerable because of high local stress concentrations. Fatigue caused by oscillating strain in the plastic range is called “low cycle fatigue”. Cycles to failure are typically below 104. Traditional welded joint S-N curves do not describe the fatigue strength in the low cycle region (< 104 number of cycles). Typical Class Society Rules do not directly address the low cycle fatigue problem. It is therefore the objective of this paper to present a credible fatigue damage prediction method of welded joints in the low cycle fatigue regime.


2. Adhesion of the plasma-polymerized fluorocarbon films to silicon substrates The adhesion properties of the plasma-polymerized FC coatings were determined by using a test, already employed by Yasuda and Sharma [13] (see Fig. 1 and Table 1) in which the silicon substrates coated with plasma FC-films were boiled in a0.9% sodium chloride solution. The FC thin films produced in the processes 1 and 2 were lifted after a very short time (15 minutes). Coatings generated in process 3 were lifted after the second cycle of boiling. The films produced in processes 4 and 5 withstood the complete test procedure. The results are shown in Fig. 3. The poor adhesion of the polymerized films in the first two processes is due to the fact that these processes do not involve a plasma pre-treatment process. The difference between processes 1 and 3 is only in the plasma pre-treatment (process 1 does not contain the pre-treatment step of the silicon surface). The fluorocarbon films deposited by processes 4 and 5 have shown the best adhesion. These test results indicate that the plasma pre-treatment is very important and necessary for a good adhesion of the FC coatings to the silicon surfaces. 2.3. Patterning of FC films 2.3.1. Patterning through resist mask. The patterning of the FC films through a photoresist mask (conventional All resist AR-P351) was examined after deposition for process No. 5. Different coating parameters were investigated to improve the adhesion of the resist to the FC surface. The best adhesion results were obtained using the process parameters, shown in Table 3. Differences in the thickness uniformity of so-deposited resists were in a range below 5%. The samples were etched in a pure oxygen plasma in an RIE-system after the lithography steps (pre-bake, exposure, development, post-bake). A resolution of 2 /xm was obtained. A significant increase in the surface energy was not observed after resist stripping. The sessile contact angle of water was 103°. 2.3.2. Lift-off process for patterning thin plasma polymerized FC films. A lift-off process was also examined to pattern the thin FC films. The lithography steps were used before the plasma polymerization process was carried out (Fig. 2). A standard resist AR-P351 was coated directly onto the Si substrates. After all lithography

2014 ◽  
pp. 275-278

InterConf ◽  
2021 ◽  
pp. 917-933
Author(s):  
Аkbota Serikkyzy ◽  
A. Baimakhan ◽  
A. Makhanova ◽  
Baimakhan Baimakhan ◽  
G. Baimakhanova

The results of theoretical and experimental works devoted to the determination of the physical and mechanical properties of water–saturated soil are analyzed. On the basis of a comprehensive analysis, conclusions are formulated, and a method is proposed for determining the Young’s modulus and Poisson’s ratio for water-saturated soil, depending on humidity (degree of saturation) and porosity. Tables of data on the physical and mechanical properties of water–saturated soil are proposed. The study established the places of formation of local stress concentrations along the inclined layer. The values of dangerous stress concentrations found in various areas of the mountain slope that are vulnerable to collapse are shown in the tables.


2019 ◽  
Vol 60 (79) ◽  
pp. 125-136 ◽  
Author(s):  
Tao Zhang ◽  
Yuqiao Chen ◽  
Min Ding ◽  
Zhongyan Shen ◽  
Yuande Yang ◽  
...  

ABSTRACTWe conducted a 9-d seismic experiment in October 2015 at Laohugou Glacier No. 12. We identified microseismic signals using the short-term/long-term average trigger algorithm at four stations and classified them as long and short-duration events based on waveform, frequency, duration and magnitude characteristics. Both categories show systematical diurnal trends. The long-duration events are low-frequency tremor-like events that mainly occurred during the daytime with only several events per day. These events lasted tens of seconds to tens of minutes and are likely related to resonance of daytime meltwater. The dominant short-duration events mostly occurred during the night time with a peak occurrence frequency of ~360 h−1. Their short-duration (<0.2 s), high frequency (20–100 Hz) and dominance of Rayleigh waves are typical of events for near-surface crack opening. A strong negative correlation between the hourly event number and temperature change rate suggests that the occurrence of night-time events is controlled by the rate of night-time cooling. We estimated the near-surface tensile stress due to thermal contraction at night to be tens of kilopascals, which is enough to induce opening of surface cracks with pre-existing local stress concentrations, although we cannot exclude the effect of refreezing of meltwater produced during the day.


Author(s):  
MJ Schollerer ◽  
J Kosmann ◽  
D Holzhüter ◽  
C Bello-Larroche ◽  
C Hühne

Bonding is known for its wide range of advantages over bolted joints when joining different materials together. However, the advantages e.g. of homogeneous load distribution can quickly be lost in case of overload. For this reason, the load occurring in the adhesive is reduced by constructive measures far below the yield stress of the adhesive, which leads to a conservative joint design. And to be on the safe side, a few “chicken rivets” are then placed again. This problem is particularly well known in aviation. Highly loaded components are structurally bonded by a combination of rivets and adhesive in order to underline the advantages of structural adhesive bonding with the safety of the well-known bolted joints. Known as fail-safe design, this concept is damage tolerant and more robust against manufacturing defects through a secured double load path.  Especially when joining fiber-reinforced composites, bolts weaken the adherends of the joint and only contribute to load transfer when the brittle adhesive fails. With the help of Surface Toughening, a boltless technique for reducing stress concentrations and arresting cracks in adhesive bonded joints is available. This work describes the industrial application of this technique. Starting with coupon tests and a small scale demonstrator to ensure the compatibility with industrial manufacturing processes, such as infusion and prepreg manufacturing, a large scale demonstrator of a 2 m carbon fiber reinforced plastic (CFRP) - HTP leading edge with hybrid laminar flow control is manufactured by the industrial partner AERnnova. Verifying a simple and cost-effective application of the technology, Surface Toughening enables robust bonded joints with a minimum impact on today's process of adhesive bonding.


Author(s):  
Jianghong Zhao ◽  
Xin Li

The vortex gripper is a kind of pneumatic noncontact gripper that does not produce a magnetic field and heat. It can grip a workpiece without physical contact, which avoids any unintentional damage such as mechanical scratches, local stress concentrations, frictional static electricity, and surface stains. This study focused on the two-dimensional pressure distribution field on a workpiece surface under the vortex gripper. Theoretical, experimental, and computational fluid dynamics results were combined to study the backflow phenomenon in the annular skirt, which can decrease the gripper’s suction force after the maximum value is reached. First, the pressure distribution in the annular skirt was theoretically modeled. A comparison with the experimental results showed that increasing the gap height between the gripper and workpiece generates a circumferentially asymmetrical flow field in the skirt. Based on this, it was hypothesized that an airflow in the circumferential direction may exist. The experimental data and simulation results were analyzed under large gap height conditions to observe the backflow in detail and it was found that an uneven pressure distribution with positive and negative pressure regions generated by the uneven flow is the root cause of the backflow. Finally, the effect of the backflow on the flow field in two different flow regions (in the annular skirt and inside the vortex chamber) was analyzed and the reason why the suction force of the vortex gripper has a maximum value was determined.


2008 ◽  
Vol 24 (12) ◽  
pp. 2194-2205 ◽  
Author(s):  
Romana Piat ◽  
Igor Tsukrov ◽  
Thomas Böhlke ◽  
Norbert Bronzel ◽  
Tilottama Shrinivasa ◽  
...  

2013 ◽  
Vol 592-593 ◽  
pp. 61-66
Author(s):  
Maxime Sauzay ◽  
Mohamed Ould Moussa

Slip localization is widely observed in metallic polycrystals after tensile deformation, cyclic deformation or pre-irradiation followed by tensile deformation. Such strong deformation localized in thin slip bands induces local stress concentrations in the quasi-elastic matrix around, at the intersections between slip bands (SBs) and grain boundaries (GBs) where microcrack initiation is often observed. Since the work of Stroh, such stress fields have been mostly modeled using the dislocation pile-up theory which leads to stress singularities similar to the LEFM ones. The Griffith criterion has then been widely applied, leading usually to strong underestimations of the macroscopic stress to GB crack initiation. In fact, slip band thickness is finite: 20nm-1000nm depending on material, temperature and loading conditions. Then, many slip planes are plastically activated through the thickness, and not only one single atomic plane. To evaluate more realistic stress fields, numerous crystalline finite element (FE) computations have been carried out using microstructure inputs (slip band aspect ratio, crystal and GB orientation...). A strong influence of slip band thickness close to the slip band corner has been highlighted, which is not accounted for by the pile-up theory. But far away, the thickness has a negligible effect and the predicted stress fields are close to the one predicted by the pile-up theory. Closed-form expressions are deduced from the numerous FE computation results allowing a straightforward prediction of GB stress fields. Slip band plasticity parameters, such as length and thickness, as well as crystal orientation, GB plane and remote stress are taken into account. The dependence with respect to the various parameters can be understood in the framework of matching expansions usually applied to cracks with V notches of finite thickness. As the exponent of the GB stress close-field is only about one-half of the pile-up or LEFM crack one, the Griffith criterion may not be used for GB microcrack prediction in case of finite thickness. That is why finite crack fracture mechanics is used together with both energy and stress criteria. Taking into account SB finite thickness, t>0, leads to predicted remote stresses to GB microcrack initiation three to six times lower than the ones predicted using the to pile-up theory, in agreement with experimental data.


2006 ◽  
Author(s):  
M. A. Qidwai ◽  
J. N. Baucom ◽  
A. C. Leung ◽  
J. P. Thomas

We are developing and exploring the concept of in-plane tiling of composite laminates, called MOSAIC, to mitigate or control delamination at free edges due to interlaminar stresses. Initial mechanical testing has shown that MOSAIC composites with uniaxial graphite-fiber reinforced tiles retain the stiffness levels of traditional uniaxially reinforced composites but with reduced strength. The reduction in strength is attributed to the formation of resin-rich pockets between adjacent tiles. In this study, we have performed detailed finite element analyses to identify the critical design parameters that affect the mechanical performance of uniaxially reinforced MOSAIC composites. We have found that using continuous laminae on the outer surfaces significantly increases the overall loadcarrying capacity. Increasing aspect ratio of the pocket and decreasing material property differences between resin and tiles also cause better load transfer between tiles but may not necessarily improve overall strength due to increasing stress concentration. The tiling scheme and density of pocket placement influence the interaction of local stress concentrations. Consequently, a novel composite joint is proposed and found to have superior performance.


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