Effects of Sr and B addition on microstructure and mechanical properties of AZ91 magnesium alloy

2007 ◽  
Vol 22 (9) ◽  
pp. 2423-2428 ◽  
Author(s):  
H.L. Zhao ◽  
S.K. Guan ◽  
F.Y. Zheng

The effects of Sr and B addition on the microstructure and mechanical properties of AZ91 alloy were studied. The results of this work show that a small amount of Sr addition to AZ91 refined the grain size. The highest tensile strength was obtained from the alloy with the optimal composition of 0.5% Sr and 0.09% B added, in which the average grain size was 42 μm. The tensile strength and elongation of the AZ91–0.5%Sr–0.09%B alloy were 151 MPa and 1.62%, respectively. Some needle-shaped Al4Sr particles distributed mainly at grain boundaries have been observed in the alloys with Sr and B additions. The fluidity is improved significantly, and the solidification range decreased by adding Sr and B. The liquidus of AZ91 alloy decreased markedly with the addition of Sr and B, but the solidus hardly changed. Therefore, the solidification range can be decreased, which will improve the die-casting properties.

2007 ◽  
Vol 546-549 ◽  
pp. 155-158
Author(s):  
Qu Dong Wang ◽  
Yang Zhao ◽  
Qing Hua Li

Effects of CaCO3 modificator on microstructure and mechanical properties of cast AZ91 Magnesium alloy have been investigated. Tensile fracture behavior of AZ91 alloys modified by CaCO3 has also been studied. Results show that CaCO3 modificator can obviously refine the grain of AZ91 magnesium alloy and Mg17Al12. Mg17Al12 in grain boundary of AZ91 alloy after modified by CaCO3 changes from continuous reticular structure to discontinuous reticular structure, even so much as granular structure and rod structure. After modified by 0.5wt% CaCO3 modificator, ultimate tensile strength, yield strength, impact toughness and elongation of AZ91 alloy increase from 186MPa to 200MPa, from 147MPa to 160MPa, from 4J to 9J and from 2.6% to 5%, respectively. And 0.5wt% CaCO3 modificator brings about an optimal refining effect. The study also shows that the fracture mechanism of modified AZ91 alloy is between cleavage fracture and quasi-cleavage fracture, which is as same as that of unmodified AZ91 alloy.


2018 ◽  
Vol 37 (1) ◽  
pp. 97-103 ◽  
Author(s):  
Hansong Xue ◽  
Xinyu Li ◽  
Weina Zhang ◽  
Zhihui Xing ◽  
Jinsong Rao ◽  
...  

AbstractThe effects of Bi on the microstructure and mechanical properties of AZ80-2Sn alloy were investigated. The results show that the addition of Bi within the as-cast AZ80-2Sn alloy promotes the formation of Mg3Bi2 phase, which can refine the grains and make the eutectic phases discontinuous. The addition of 0.5 % Bi within the as-extruded AZ80-2Sn alloy, the average grain size decreases to 12 μm and the fine granular Mg17Al12 and Mg3Bi2 phases are dispersed in the α-Mg matrix. With an increase in Bi content, the Mg17Al12 and Mg3Bi2 phases become coarsened and the grain size increases. The as-extruded AZ80-2Sn-0.5 %Bi alloy has the optimal properties, and the ultimate tensile strength, yield strength and elongation are 379.6 MPa, 247.1 MPa and 14.8 %, respectively.


2011 ◽  
Vol 328-330 ◽  
pp. 1650-1653 ◽  
Author(s):  
Jin Ling Zhang ◽  
She Bin Wang ◽  
Xiao Ye Qi ◽  
Bing She Xu

Microstructure changes brought by the addition of La element to AZ91 magnesium alloy are studied, also, the precipitating phases were identified and their influence on the mechanical properties of alloys was investigated. Results show La makes refinement of microstructure of the AZ91 alloy, and decrease the size of Mg17Al12 phase. La element takes a priority to react with Al element over Mg, forming binary phase Al11La3 with high melting point. Certain amount of La increases tensile strength, yield strength and elongation. With more addition, La would combine more Al in matrix and decrease strengthening effect, because Al11La3 phase would become coarsening. The mechanical poroerties tests indicate that AZ91+0.16%La alloy has the best properties. Maximum tensile strength, maximum yield strength and elongation are 245MPa, 178MPa and 14.5% respective, increased by 21%, 19% and 48% respectively. The mechanism of La strenthing mechanical properties is proposed that Al11La3 phase enriched on solid-liquid interface, increased the degree of supercooling, refined the grain size and changed the crystal style.


2011 ◽  
Vol 704-705 ◽  
pp. 892-896
Author(s):  
Bao Hong Zhang ◽  
Zhi Min Zhang

In order to study the effect of plastic deformation on microstructure and mechanical properties of as-cast AZ91 magnesium alloy, experiments of hot direct extrusion were performed at different extrusion temperatures and different extrusion ratios. The microstructure and mechanical properties of extruded billets and extrudate were measured. Experimental results show that the grain size of as-cast AZ91 magnesium alloy can be dramatically refined by extrusion. Hot extrusion can obviously improve the mechanical properties of as-cast AZ91 magnesium Alloy, comparing with the pre-extruded billet, the tensile strength, yield strength and elongation of extrudate can be improved by at least 69%, 117% and 150% respectively. As the extrusion temperature increases, the tensile strength and yield strength of extrudate will increase. As the extrusion ratio increases, the tensile strength and yield strength of extrudate will increase at first and then fall. At the time of extrusion temperature of 420°C and extrusion ratio of 45, the highest tensile strength of 381Mpa and yield strength of 303MPa can be achieved for the extrudate.


2012 ◽  
Vol 562-564 ◽  
pp. 242-245 ◽  
Author(s):  
Ming Tan ◽  
Zhao Ming Liu ◽  
Gao Feng Quan

The effects of heat treatment on the microstructure, tensile property and fracture behavior of as-extruded AZ91 magnesium alloy were studied by OM and SEM. The results show that the grain of as-cast AZ91 alloy is refined by extruding and dynamic recrystallization, and the mechanical properties increase obviously. The ductility is significantly enhanced after solution treatment of the as-extruded AZ91 alloy, tensile strength is almost the same before and hardness is significantly reduced after solution treatment and artificial aging treatment. The tensile strength reduced and the ductility is significantly enhanced of as-extruded AZ91 magnesium alloy after annealing processes. The fracture surface of as-extruded AZ91 magnesium alloy has the mixture of ductile and brittle characteristic. But after T6 or annealing treatment, its dimple number increases evidently.


2012 ◽  
Vol 706-709 ◽  
pp. 1261-1266 ◽  
Author(s):  
Wei Guo ◽  
Qu Dong Wang ◽  
Man Ping Liu ◽  
Xin Tao Liu ◽  
Hao Zhou

Repetitive upsetting (RU) was applied to a commercial AZ31 Mg alloy. The samples were processed at temperatures of 230 °C, 250 °C and 300 °C up to 3 passes. Effects of processing temperature on the microstructure and mechanical properties were investigated. The results indicate that the microstructure was effectively refined by RU and an average grain size of ~1.9 μm was obtained at 250 °C. Increasing the temperature resulted in larger mean grain size and higher microstructural homogeneity. Both the strength and hardness were significantly improved. It was also found that increasing the processing temperature led to increase in the strength but decrease in the ductility. The sample after RU 3 passes at 230 °C had tensile strength of 330 MPa compared with 173 MPa prior to the processing.


2013 ◽  
Vol 747-748 ◽  
pp. 276-281 ◽  
Author(s):  
Fang Chai ◽  
Da Tong Zhang ◽  
Wen Zhang ◽  
Cheng Qiu

Normal and submerged friction stir processing (SFSP) were conducted to AZ91 magnesium alloy plates with 6mm in thickness, and influence of processing speed (ν) on microstructures and mechanical properties of the experimental materials was investigated. The results revealed that fine and equiaxed grains were observed in the stirred zone (SZ). As the processing speed increased from 60mm/min to 150mm/min, the average grain size in the SZ of normal FSP material decreased. However, the grain size of the SFSP specimens first increased with the processing rate increasing from 60mm/min to 120mm/min, and then decreased when the processing rate increased to 150mm/min. Microstructure of the SFSP specimen was much finer compared with the normal FSP one, and the grain size of α-Mg was about 1.2µm when the processing speed was 60mm/min during SFSP. Because of much finer microstructure of SFSP, the microhardness, tensile strength and elongation were all improved. SEM fracture observation showed that fine dimples and tearing edges could be observed on SFSP specimen which showing good ductility. In addition, high temperature tensile tests showed that SFSP AZ91 alloys exhibited excellent superplasticity at high strain rate, with an elongation of 1202% at 623 K with a strain rate of 3x10-3s-1. The present study demonstrated that SFSP possesses great potential in preparing fine-grained materials.


2020 ◽  
Vol 17 (6) ◽  
pp. 831-836
Author(s):  
M. Vykunta Rao ◽  
Srinivasa Rao P. ◽  
B. Surendra Babu

Purpose Vibratory weld conditioning parameters have a great influence on the improvement of mechanical properties of weld connections. The purpose of this paper is to understand the influence of vibratory weld conditioning on the mechanical and microstructural characterization of aluminum 5052 alloy weldments. An attempt is made to understand the effect of the vibratory tungsten inert gas (TIG) welding process parameters on the hardness, ultimate tensile strength and microstructure of Al 5052-H32 alloy weldments. Design/methodology/approach Aluminum 5052 H32 specimens are welded at different combinations of vibromotor voltage inputs and time of vibrations. Voltage input is varied from 50 to 230 V at an interval of 10 V. At each voltage input to the vibromotor, there are three levels of time of vibration, i.e. 80, 90 and 100 s. The vibratory TIG-welded specimens are tested for their mechanical and microstructural properties. Findings The results indicate that the mechanical properties of aluminum alloy weld connections improved by increasing voltage input up to 160 V. Also, it has been observed that by increasing vibromotor voltage input beyond 160 V, mechanical properties were reduced significantly. It is also found that vibration time has less influence on the mechanical properties of weld connections. Improvement in hardness and ultimate tensile strength of vibratory welded joints is 16 and 14%, respectively, when compared without vibration, i.e. normal weld conditions. Average grain size is measured as per ASTM E 112–96. Average grain size is in the case of 0, 120, 160 and 230 is 20.709, 17.99, 16.57 and 20.8086 µm, respectively. Originality/value Novel vibratory TIG welded joints are prepared. Mechanical and micro-structural properties are tested.


2021 ◽  
Vol 21 (9) ◽  
pp. 4897-4901
Author(s):  
Hyo-Sang Yoo ◽  
Yong-Ho Kim ◽  
Hyeon-Taek Son

In this study, changes in the microstructure, mechanical properties, and electrical conductivity of cast and extruded Al–Zn–Cu–Mg based alloys with the addition of Li (0, 0.5 and 1.0 wt.%) were investigated. The Al–Zn–Cu–Mg–xLi alloys were cast and homogenized at 570 °C for 4 hours. The billets were hot extruded into rod that were 12 mm in diameter with a reduction ratio of 38:1 at 550 °C. As the amount of Li added increased from 0 to 1.0 wt.%, the average grain size of the extruded Al alloy increased from 259.2 to 383.0 µm, and the high-angle grain boundaries (HGBs) fraction decreased from 64.0 to 52.1%. As the Li content increased from 0 to 1.0 wt.%, the elongation was not significantly different from 27.8 to 27.4% and the ultimate tensile strength (UTS) was improved from 146.7 to 160.6 MPa. As Li was added, spherical particles bonded to each other, forming an irregular particles. It is thought that these irregular particles contribute to the strength improvement.


2010 ◽  
Vol 667-669 ◽  
pp. 457-461
Author(s):  
Wei Guo ◽  
Qu Dong Wang ◽  
Man Ping Liu ◽  
Tao Peng ◽  
Xin Tao Liu ◽  
...  

Cyclic channel die compression (CCDC) of AZ31-1.7 wt.% Si alloy was performed up to 5 passes at 623 K in order to investigate the microstructure and mechanical properties of compressed alloys. The results show that multi-pass CCDC is very effective to refine the matrix grain and Mg2Si phases. After the alloy is processed for 5 passes, the mean grain size decreases from 300 μm of as-cast to 8 μm. Both dendritic and Chinese script type Mg2Si phases break into small polygonal pieces and distribute uniformly in the matrix. The tensile strength increases prominently from 118 MPa to 216 MPa, whereas the hardness of alloy deformed 5 passes only increase by 8.4% compared with as-cast state.


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