Assessment of the effect of the steels structure dispersion on its magnetic and mechanical properties

2021 ◽  
Vol 23 (4) ◽  
pp. 93-110
Author(s):  
Roman Sokolov ◽  
◽  
Vitaly Novikov ◽  
Kamil Muratov ◽  
Anatolii Venediktov ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Operating Time ◽  
Testing Machine ◽  
Structural Steels ◽  
Premature Aging ◽  
Grain Structure ◽  
Internal Stresses ◽  
Size Factor ◽  
Local Areas

Introduction: The control of the mechanical properties of structural steels is one of the main processes that regulate the service life of equipment. In most technical processes (pressure treatment, welding, rolling, thermal exposure), structure changes both in local areas and in the entire volume. Changes in the steel structure entail changes in its properties and as a result in local areas, at various stages of operation, the likelihood of the occurrence and development of critical defects increases. Its presence significantly affects the performance of the equipment, and leads to premature aging of the material and its failure. Precisely because the control of the mechanical properties of steel remains one of the urgent problems, new control methods are being developed. It is known that all properties of steel depend on the structure of the substance, however, studies on the effect of the dispersion of the structure under consideration on the mechanical properties are presented in an insignificant amount. Purpose: to analyze from a mathematical point of view the influence of the factor of different grain size, as a parameter reflecting the dispersity of the system, on the mechanical properties of structural steel. The paper studies a heat-treated planar samples of steels 15KhSND, 09G2S and St3. Methods of research: scanning electron and optical microscopes are used to study the grain structure and grain boundaries; SIAMS 700 software package is used for finding the boundaries and average data of the grain structure; portable X-ray fluorescence analyzer of metals and alloys X-MET 7000 is used to determine the chemical composition of the test samples in percentage; tensile testing machine IR-50 is used for measuring the tensile strength of samples; Vickers hardness tester is used to determine the hardness of samples. Results and discussion: it is found that there is a satisfactory correlation for the mechanical properties of structural steels (hardness and ultimate strength) and the grain size factor, which can be used to predict the hazardous states of structures and the operating time. The analysis of variance and regression of the detected dependencies is carried out. It is noted that the dropout of some values from the general regression dependence can most likely be associated with a decrease in the value of internal stresses as a result of a decrease in the distortions of the crystal lattice of steel occurring during heat treatment. It should be noted that the processes occurring and the degree of its influence on the properties of the structural steels under consideration can be different due to the presence of different amounts of alloying elements in the composition of the studied steels.

Effect of Cr on Grain Refinement and Mechanical Properties of Al-Si-Mg Alloys

2015 ◽  
Vol 789-790 ◽  
pp. 95-99 ◽  
Author(s):  
Aakash Kumar ◽  
Gaurav Sharma ◽  
Chandrabalan Sasikumar ◽  
Shahrukh Shamim ◽  
Himkar Singh
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Grain Growth ◽  
Testing Machine ◽  
Weight Percent ◽  
Stir Casting ◽  
Optical Microscope ◽  
Mg Alloys ◽  
Grain Structure ◽  
Second Phase

Grain growth of Aluminium alloys at high temperature reduces their strength significantly. Therefore it is essential to control the grain growth by suitable techniques. The effect of Cr on refining the grain structure of Al alloys is investigated in the present work. Cr is added into Al-Si-Mg alloy by stir casting techniques. Subsequently the alloys were subjected to annealing at 500oC for 1 hour to study the grain growth behavior of these alloys. An optical microscope is used to analyze the grain size and microstructure. The mechanical properties of these alloys were studied using a universal testing machine. The Cr additions were varied between 0.5 to 4 weight percent. The Cr addition had shown a significant effect in refining the grain size of Al-Si-Mg alloys. The average grain diameter after annealing was found to be about 151 μm in unalloyed samples while, the 2 wt % Cr added samples showed about 92 μm. The second phase particles, Al7Cr found precipitated along the grain boundaries apart from Al2Si and Mg2Si. However Cr additions more than 2% does not show significant role in refining the grain size. Cr also improved the mechanical properties such as yield strength, ultimate tensile strength and fracture toughness moderately.

Surface Modification and its Influence on the Microstructure and Creep Resistance of Nickel Based Superalloy René 77 / Modyfikacja Powierzchniowa Oraz Jej Wpływ Na Mikrostrukture I Wytrzymałosc Na Pełzanie Odlewów Z Nadstopu Niklu Ren´E 77

2013 ◽  
Vol 58 (1) ◽  
pp. 95-98 ◽  
Author(s):  
M. Zielinska ◽  
J. Sieniawski
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Surface Modification ◽  
Turbine Blades ◽  
Processing Parameters ◽  
Grain Structure ◽  
Creep Tests ◽  
Cobalt Aluminate ◽  
Nickel Based Superalloy ◽  
Average Grain Size

Superalloy René 77 is very wide used for turbine blades, turbine disks of aircraft engines which work up to 1050°C. These elements are generally produced by the investment casting method. Turbine blades produced by conventional precision casting methods have coarse and inhomogeneous grain structure. Such a material often does not fulfil basic requirements, which concern mechanical properties for the stuff used in aeronautical engineering. The incorporation of controlled grain size improved mechanical properties. This control of grain size in the casting operation was accomplished by the control of processing parameters such as casting temperature, mould preheating temperature, and the use of grain nucleates in the face of the mould. For nickel and cobalt based superalloys, it was found that cobalt aluminate (CoAl2O4) has the best nucleating effect. The objective of this work was to determine the influence of the inoculant’s content (cobalt aluminate) in the surface layer of the ceramic mould on the microstructure and mechanical properties at high temperature of nickel based superalloy René 77. For this purpose, the ceramic moulds were made with different concentration of cobalt aluminate in the primary slurry was from 0 to 10% mass. in zirconium flour. Stepped and cylindrical samples were casted for microstructure and mechanical examinations. The average grain size of the matrix ( phase), was determined on the stepped samples. The influence of surface modification on the grain size of up to section thickness was considered. The microstructure investigations with the use of light microscopy and scanning electron microscopy (SEM) enable to examine the influence of the surface modification on the morphology of ’ phase and carbides precipitations. Verification of the influence of CoAl2O4 on the mechanical properties of castings were investigated on the basis of results obtained form creep tests.

scholarly journals Development of Al–Mg–Si alloy performance by addition of grain refiner Al–5Ti–1B alloy

2021 ◽  
Vol 104 (2) ◽  
pp. 003685042110294
Author(s):  
Khaled Abd El-Aziz ◽  
Emad M Ahmed ◽  
Abdulaziz H Alghtani ◽  
Bassem F Felemban ◽  
Hafiz T Ali ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Corrosion Resistance ◽  
Testing Machine ◽  
Dendritic Structure ◽  
Grain Refiner ◽  
Corrosion Properties ◽  
Average Grain Size ◽  
Structural Applications ◽  
Alloy Addition

Aluminum alloys are the most essential part of all shaped castings manufactured, mainly in the automotive, food industry, and structural applications. There is little consensus as to the precise relationship between grain size after grain refinement and corrosion resistance; conflicting conclusions have been published showing that reduced grain size can decrease or increase corrosion resistance. The effect of Al–5Ti–1B grain refiner (GR alloy) with different percentages on the mechanical properties and corrosion behavior of Aluminum-magnesium-silicon alloy (Al–Mg–Si) was studied. The average grain size is determined according to the E112ASTM standard. The compressive test specimens were made as per ASTM: E8/E8M-16 standard to get their compressive properties. The bulk hardness using Vickers hardness testing machine at a load of 50 g. Electrochemical corrosion tests were carried out in 3.5 % NaCl solution using Autolab Potentiostat/Galvanostat (PGSTAT 30).The grain size of the Al–Mg–Si alloy was reduced from 82 to 46 µm by the addition of GR alloy. The morphology of α-Al dendrites changes from coarse dendritic structure to fine equiaxed grains due to the addition of GR alloy and segregation of Ti, which controls the growth of primary α-Al. In addition, the mechanical properties of the Al–Mg–Si alloy were improved by GR alloy addition. GR alloy addition to Al–Mg–Si alloy produced fine-grained structure and better hardness and compressive strength. The addition of GR alloy did not reveal any marked improvements in the corrosion properties of Al–Mg–Si alloy.

Effect of Thermomechanical Processing on Grain Size, Texture and Mechanical Properties of Pure Magnesium

2020 ◽  
Vol 985 ◽  
pp. 97-108
Author(s):  
Mouhamadou Moustapha Sarr ◽  
Motohiro Yuasa ◽  
Hiroyuki Miyamoto
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Yield Stress ◽  
Thermomechanical Processing ◽  
Pure Magnesium ◽  
Grain Structure ◽  
Misorientation Distribution ◽  
Processed Material ◽  
Texture Characterization

This study aims to investigate the effect of processing routes (A and Bc) and temperature on microstructure, texture and mechanical properties of pure magnesium was studied in this research. An extruded pure magnesium (~99,9 %) was subjected to severe plastic deformation (SPD) by ECAP. Deformation was conducted at 523K and 473K and two different processing routes (A and Bc) were used to control the texture. The microstructure and texture characterization of the pressed materials were carried out. It was found that the microstructure displayed a bimodal grain structure after two passes and then became homogeneous after four passes following both routes A and Bc. The misorientation distribution was examined and the results revealed that the fraction of high angle grain boundaries (HAGB) was higher at temperature 473K. The texture was randomized following route Bc whereas it became strengthened in route A after four passes. According to the Hall-Petch (HP) relationship, the yield stress of polycrystalline metals increases with a decrease in grain size. In this study, a positive slope k was achieved in the strengthened texture while a negative one was obtained in the softened texture. The ductility of ECAP processed material was considerably improved (from 23% to 38%) without sacrificing the yield stress by route Bc at 423K.

scholarly journals Mechanical Properties and Microstructure Evolution of Mg-6 wt % Zn Alloy during Equal-Channel Angular Pressing

Metals ◽  
2018 ◽  
Vol 8 (10) ◽  
pp. 841 ◽  
Author(s):  
Jingli Yan ◽  
Zijun Qin ◽  
Kai Yan
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Grain Refinement ◽  
Equal Channel Angular Pressing ◽  
Testing Machine ◽  
Grain Structure ◽  
X Ray Diffraction ◽  
Angular Pressing ◽  
Transmission Electron ◽  
Zn Alloy

Equal-channel angular pressing (ECAP) was performed on a Mg (6 wt %) Zn alloy at temperatures from 160 to 240 °C and the microstructures and mechanical properties were studied using optical microscopy, X-ray diffraction, scanning electron microscopy, transmission electron microscopy, and an electronic universal testing machine. The results showed that ECAP was effective for grain refinement and a bi-modal grain structure formed at low temperatures, which was stable during ECAP from 160 to 200 °C. MgZn2 phase and Mg4Zn7 phase were generated during the ECAP process. The mechanical properties remarkably increased after two repetitions of ECAP. However, the strengths could not be further improved by increasing the plastic deformation, but decreased when ECAP was performed between 200 and 240 °C. The mechanical properties of the ECAP Mg-6Zn alloy was determined by a combination of grain refinement strengthening, precipitation hardening, and texture softening.

Impact of Grain Structure and Material Properties on Via Extrusion in 3-D Interconnects

2014 ◽  
Vol 2014 (1) ◽  
pp. 000008-000012
Author(s):  
Tengfei Jiang ◽  
Chenglin Wu ◽  
Jay Im ◽  
Rui Huang ◽  
Paul S. Ho
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Analytical Model ◽  
Material Properties ◽  
Grain Structure ◽  
Silicon Vias ◽  
The Relationship

In this paper, the effects of Cu microstructure on the mechanical properties and extrusion of though-silicon vias (TSVs) were studied based on two types of TSVs with different microstructure. A direct correlation was found between the grain size and the mechanical properties of the vias. Both an analytical model and FEA were used to establish the relationship between the mechanical properties and via extrusion. The effect of via/Si interface on extrusion was also studied by FEA. The results suggest small and uniform grains in the Cu vias, as well as stronger interfaces between the via and Si led to smaller via extrusion, and are thus preferable for reduced via extrusion failure and improved TSV reliability.

Impact of Grain Structure and Material Properties on Via Extrusion in 3D Interconnects

2015 ◽  
Vol 12 (3) ◽  
pp. 118-122 ◽  
Author(s):  
Tengfei Jiang ◽  
Chenglin Wu ◽  
Jay Im ◽  
Rui Huang ◽  
Paul S. Ho
Keyword(s):  
Mechanical Properties ◽  
Finite Element Analysis ◽  
Grain Size ◽  
Finite Element ◽  
Analytical Model ◽  
Material Properties ◽  
Grain Structure ◽  
Element Analysis ◽  
Silicon Vias ◽  
The Relationship

In this article, the effects of Cu microstructure on the mechanical properties and extrusion of through-silicon vias (TSVs) were studied based on two types of TSVs with different microstructure. A direct correlation was found between the grain size and the mechanical properties of the vias. Both an analytical model and finite element analysis (FEA) were used to establish the relationship between the mechanical properties and via extrusion. The effect of via/Si interface on extrusion was also studied by FEA. The results suggest small and uniform grains in the Cu vias, as well as stronger interfaces between the via and Si led to smaller via extrusion, and are thus preferable for reduced via extrusion failure and improved TSV reliability.

Novel Grain Refiner for Hypo- and Hyper-Eutectic Al-Si Alloys

2011 ◽  
Vol 690 ◽  
pp. 49-52 ◽  
Author(s):  
Magdalena Nowak ◽  
Nadendla Hari Babu
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Al Alloys ◽  
Grain Structure ◽  
Grain Refiner ◽  
Silicon Alloys ◽  
Fine Grain ◽  
Cooling Conditions ◽  
Wide Range ◽  
Master Alloys

A novel effective grain refiner for hypo and hyper-eutectic Aluminium-Silicon alloys has been developed. The composition of the grain refiner has been optimized to produce a fine grain structure and finer eutectic. Effectiveness of grain size under various cooling conditions has also been investigated to simulate various practical casting conditions. For comparative purposes, a wide range of Al alloys have been produced with the addition of commercially available Al-5Ti-B master alloys. The results show that the addition of novel grain refiner reduces the grain size significantly. As a result of fine grains, the porosity in the solidified alloys is remarkably lower. A notable improvement in mechanical properties has also been observed.

Experimental Research on Ultrasound Cast-Rolling Lead Alloy Strip

2011 ◽  
Vol 366 ◽  
pp. 181-186
Author(s):  
Jian Ping Li ◽  
Li Bang Zeng ◽  
Da Heng Mao ◽  
Hong Feng Jiang
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Acoustic Streaming ◽  
Organization Structure ◽  
Grain Structure ◽  
Alloy Strip ◽  
Lead Alloy ◽  
Test Results ◽  
Lead Alloys ◽  
Better Than

With the ultrasound was put into the experiment of cast-rolling lead alloy strip, it broke the dendrite structures and enhanced the under-cooling by the effect of cavity and acoustic streaming. The microstructure comparison of ultrasound and general cast-rolling shows that: The grain size of general cast-rolled lead strip is big; the grain boundary is coarse and the organization structure is uneven. However, the grain structure is refined, smaller grains and uniform organization structure is acquired with ultrasound treatment. Besides, the mechanical properties test results of the two kinds lead alloys shows that the ultrasound cast-rolling lead alloys are better than general cast-rolling. The tensile strength, yield strength and elongation of ultrasound cast-rolling lead strip are increased by 11.30%, 22.15% and 21.74% than that of general cast-rolling lead strip.

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