scholarly journals Pemodelan Kondisi Optimum Ekstraksi dan Identifikasi Senyawa Penyusun Minyak Atsiri Lada Hitam

2021 ◽  
pp. 99-108
Author(s):  
Shintawati Shintawati ◽  
Analianasari Analianasari ◽  
Zukryandry Zukryandry
Keyword(s):  
Essential Oil ◽  
Respiratory Infections ◽  
Antimicrobial Properties ◽  
Black Pepper ◽  
Operating Conditions ◽  
Solvent Ratio ◽  
Test Results ◽  
Optimum Conditions ◽  
Muscle Disorders ◽  
Surface Method

Black pepper is a spice with a spicy taste and a distinctive aroma that has become known as the King of Spices. The distinctive aroma of black pepper comes from the volatile compounds that make up the essential oil of pepper. Black pepper essential oil has antimicrobial properties that can relieve respiratory infections and relieve muscle disorders. The acquisition of pepper essential oil from the distillation process is influenced by operating conditions. The aim of this study was to identify the composition of black pepper essential oil compounds using GCMS and to optimize the operating conditions (material size, solvent ratio, and distillation time). The method used to determine the optimum condition is using the Response Surface Method (RSM). The results showed that the highest yield of black pepper essential oil from this experiment is 5.14%. The empirical model was also suitable for the experiment and the optimum conditions for producing the maximum pepper oil yield 5,81% were 40 mesh of material size, 0.12 (g.ml-1) of solvent ratio and 162 minutes of distillation time. GCMS test results showed that the main constituents of pepper essential oil are caryophyllene, ocimene, limonene, carene, and a-pinene.

scholarly journals Optimization of Anthocyanin Extraction from Cockspur Coral (Erythrina Crista-Galli L.) Petals with Microwave-Assisted Extraction (MAE) using Response Surface Methodology

2021 ◽  
Vol 21 (2) ◽  
pp. 143
Author(s):  
Astrilia Damayanti ◽  
Bayu Triwibowo ◽  
Megawati Megawati ◽  
Miftahuddin Azhari ◽  
Sandra Anggita Fadriana
Keyword(s):  
Response Surface ◽  
Extraction Process ◽  
Operating Conditions ◽  
Solvent Ratio ◽  
Microwave Assisted Extraction ◽  
Microwave Assisted ◽  
Surface Method ◽  
Assisted Extraction ◽  
Order Polynomial ◽  
Independent Variable

Cockspur coral (Erythrina crista-galli L) petals are flowers that contain anthocyanins and active compounds of flavonoids and tannins. This study aims to determine the optimum conditions for the anthocyanin extraction process of cockspur coral petals using Microwave-Assisted Extraction (MAE), analyzed through the Response Surface Method (RSM). This process uses ethanol-hydrochloric acid solvents and a Box-Behnken experimental design involving three factors, namely the solvent ratios (w/v) (1:5, 1:15, and 1:25), microwave powers (300, 450, and 600 watts), and extraction times (3, 9, and 15 minutes). As a result, the second-order polynomial model was enhanced and sufficient to explain the variation of the data that denoted the significant correlation with the independent variables and the response. Derringer's desired function methodology was used for optimizing studies and generated ideal conditions for each or combined an independent variable.  The optimum anthocyanin extract of 5.82 mg/L was obtained at a power condition of 325,5 Watts, an extraction time of 3.05 minutes, and a solvent ratio of 20.5. Meanwhile, the operating conditions at a power of 310.8 Watts, a time of 14.94 minutes, and a solvent ratio of 24.96 resulted in the optimum color intensity (IC) of 1040.26. In the meantime, the optimum antioxidant activity was obtained at a power of 585.97 Watts, a time of 4.93 minutes, and a solvent ratio of 5.43 with IC50 of 0.115.

scholarly journals Ekstraksi Oleoresin Lada Hitam Secara Maserasi Menggunakan Metode Permukaan Respon

2018 ◽  
Vol 3 (1) ◽  
Author(s):  
Liya Fitriyana ◽  
Irmayanti Irmayanti ◽  
Putri Meutia Sari ◽  
Virna Muhardina
Keyword(s):  
Response Surface ◽  
Response Surface Method ◽  
Black Pepper ◽  
Extraction Time ◽  
Optimum Conditions ◽  
Iso Standards ◽  
Ultrasonic Methods ◽  
Surface Method ◽  
Ft Ir ◽  
Extraction Solvents

Purpose of this study is to determine the optimum conditions of extraction using conventional methods (maceration) and ultrasonic methods by using response surface method (RSM). The variables used in this study is the ratio of solvent with black pepper, temperature and time of extraction. Solvents used in this study is 99% ethanol. The bigest yield of oleoresin using maceration method was  4.42% with a ratio of solvent and black pepper for 1: 4 g / ml and extraction time of 4.68 hours. GC-MS test showed that the piperine contained in oleoresin extracted by using maceration are respectively<br />69.92% FT-IR test showed that oleoresin extracted using maceration have the same bound that same as piperine bound. Organoleptic test showed that oleoresin produced by using maceration meet the requirement of ISO standards 06-2388-1998 (dark brown color, pepper smell and thick paste form).<br /><br />

scholarly journals The Study on Extraction Process and Analysis of Components in Essential Oils of Black Pepper (Piper nigrum L.) Seeds Harvested in Gia Lai Province, Vietnam

Processes ◽  
2019 ◽  
Vol 7 (2) ◽  
pp. 56 ◽  
Author(s):  
Thien Hien Tran ◽  
Le Ke Ha ◽  
Duy Chinh Nguyen ◽  
Tan Phat Dao ◽  
Le Thi Hong Nhan ◽  
...  
Keyword(s):  
Essential Oil ◽  
Respiratory Infections ◽  
Mesh Size ◽  
Extraction Process ◽  
Black Pepper ◽  
Raw Material ◽  
Gas Chromatography Mass Spectrometry ◽  
Piper Nigrum ◽  
Efficient Technology ◽  
Preservation Method

Black pepper (Piper nigrum L.) is a tropical crop with extensive medicinal potential in ethnomedicine and nutraceutical applications. The essential oil of black pepper finds wide applications in inhabitation of respiratory infections and soothing of muscular pains due to its warming and energizing property. The pungent bioactive piperine is responsible for this function, and therefore, efficient technology is required for an optimal extraction process of this compound. In the present article, we have developed a procedure for extracting black pepper essential oil from Vietnam, optimizing conditions that affect the extraction process. The effect of process parameters, namely material size, preservation method, the concentration of sodium chloride, the concentration of soak time, the ratio of material to water, temperature extraction, time extraction on the extraction yield, and relative efficiency were investigated. Results demonstrated that 20 g of black pepper milled with a mesh size of 160 obtained 0.48 g of essential oil (2.4%) at a raw material to water ratio of 1/21 (g/mL) at 150 °C in a time of 5.2 h. GC-MS (Gas chromatography–mass spectrometry) spectra showed that 3-carene (29.21%), D-limonene (20.94%), caryophyllene (15.05%), and β-pinene (9.77%) were present as major components. These results suggested that the essential oil extracted from Vietnamese black pepper is applicable in the manufacturing processes of insecticides and air deodorizers.

Effect of Ethanol Treatment on Lycopene Extraction yield

2018 ◽  
Author(s):  
Nam Kyong-il ◽  
KIM rak-chon ◽  
Kang chang-hyok ◽  
Lee song-nam ◽  
Ryom sok-hun
Keyword(s):  
Antioxidant Activity ◽  
Treatment Time ◽  
Extraction Yield ◽  
Extraction Rate ◽  
Test Results ◽  
Ethanol Treatment ◽  
Optimum Conditions ◽  
Liquid Ratio ◽  
Pretreatment Method ◽  
Ethanol Pretreatment

In order to extract lycopene more effectively, this experiment focused on the optimization of ethanol pretreatment method to study the effects of ethanol treatment on the extraction rate of lycopene and its antioxidant activity. The test results show that 2 times ethanol treatment is very effective for improving lycopene yield. The optimum conditions of ethanol treatment are temperature 50 ℃, treatment time 1 time 2h, 2 times 2h, solid to liquid ratio is 1:12. The lycopene yield can be reached 20mg / 100g above.

Hysteresis loss of ultra-large off-the-road tire rubber compounds based on operating conditions at mine sites

2021 ◽  
pp. 095440702110155
Author(s):  
Shaosen Ma ◽  
Guangping Huang ◽  
Khaled Obaia ◽  
Soon Won Moon ◽  
Wei Victor Liu
Keyword(s):  
Large Strain ◽  
Tensile Tests ◽  
Operating Conditions ◽  
Hysteresis Loss ◽  
Strain Rates ◽  
Test Results ◽  
Tire Rubber ◽  
The Road ◽  
Rubber Compounds ◽  
Mine Sites

The objective of this study is to investigate the hysteresis loss of ultra-large off-the-road (OTR) tire rubber compounds based on typical operating conditions at mine sites. Cyclic tensile tests were conducted on tread and sidewall compounds at six strain levels ranging from 10% to 100%, eight strain rates from 10% to 500% s−1 and 14 rubber temperatures from −30°C to 100°C. The test results showed that a large strain level (e.g. 100%) increased the hysteresis loss of tire rubber compounds considerably. Hysteresis loss of tire rubber compounds increased with a rise of strain rates, and the increasing rates became greater at large strain levels (e.g. 100%). Moreover, a rise of rubber temperatures caused a decrease in hysteresis loss; however, the decrease became less significant when the rubber temperatures were above 10°C. Compared with tread compounds, sidewall compounds showed greater hysteresis loss values and more rapid increases in hysteresis loss with the rising strain rate.

scholarly journals Methodology for Selecting the Operating Conditions of a Vibration Generator Used in the Hot-Dip Galvanizing Process

Materials ◽  
2021 ◽  
Vol 14 (8) ◽  
pp. 2042
Author(s):  
Wojciech Kacalak ◽  
Igor Maciejewski ◽  
Dariusz Lipiński ◽  
Błażej Bałasz
Keyword(s):  
Simulation Model ◽  
Asynchronous Motor ◽  
Experimental Tests ◽  
Suspension System ◽  
Operating Conditions ◽  
Test Results ◽  
Forced Simulation

A simulation model and the results of experimental tests of a vibration generator in applications for the hot-dip galvanizing process are presented. The parameters of the work of the asynchronous motor forcing the system vibrations were determined, as well as the degree of unbalance enabling the vibrations of galvanized elements weighing up to 500 kg to be forced. Simulation and experimental tests of the designed and then constructed vibration generator were carried out at different intensities of the unbalanced rotating mass of the motor. Based on the obtained test results, the generator operating conditions were determined at which the highest values of the amplitude of vibrations transmitted through the suspension system to the galvanized elements were obtained.

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