scholarly journals First Approach to Measure Interfacial Rheology at High-Pressure Conditions by the Oscillating Drop Technique

2021 ◽  
Vol 5 (2) ◽  
pp. 23
Author(s):  
Albert Barrabino ◽  
Torleif Holt ◽  
Bård Bjørkvik ◽  
Erik Lindeberg

An oscillating drop rheometer capable of operating under conditions of high pressure and high temperature has been built. The oscillating drop mechanism was able to support pressures as high as 1300 bar and successfully performed oscillations at constant pressure. Apparent elastic and viscous complex moduli were measured for a system of CO2 and synthetic seawater containing 100 ppm of a linear alkyl ethoxylate surfactant for different pressures and temperatures. The moduli had strong dependencies on both pressure and temperature. At temperatures of 40 and 80 °C, the apparent elastic modulus passed through a maximum for pressures between 100 and 300 bar. The harmonic distortion of the oscillations was calculated for all measurements, and it was found that drop oscillations below ca. 2.6 µL caused distortions above 10% due to a mechanical backlash of the motor.

2013 ◽  
Vol 457-458 ◽  
pp. 423-427
Author(s):  
Xiao Qing Li ◽  
Xiao Yan Liu

With the development of oilfield exploration, the performance of electric submersible pump (ESP) has been enhanced very fast. It requires testing techniques develop at the same time. The most outstanding question is the testing of high temperature and pressure ESP. A testing well was drilled in Daqing in 1992. It keeps the water liquid state on 150 centigrade by high pressure. This system can simulate operational mode 3000 meters under the ground. But many new ESPs have been produced these years. The quondam testing system couldnt meet the testing requirement. A new testing system is desiderated eagerly. This paper developed a high temperature and pressure ESP testing experimentation system. Hydraulic/thermodynamic analysis calculation has been carried on. Friction resistance from constant pressure point to the suction inlet of hot water pump and the ESP in heating-forced cycle and experimentation primary cycle are calculated respectively. Keeping the water liquid state on 180 centigrade, constant pressure value was fixed on 2.5 MPa. The heat load is calculated including the heat that the water in the system and the equipment need and the heat loss. In order to protect ESP from emanating too much heat to keep the temperature and pressure of the system steady, heat exchange system has been designed. Cold load and heat exchange square have been calculated. Friction resistance and the size of the cold water cistern have been calculated. These provide necessary academic foundation for the testing experimentation of high temperature and pressure ESP.


2014 ◽  
Vol 07 (04) ◽  
pp. 1450040 ◽  
Author(s):  
Yanan Xue ◽  
Jiaqian Qin ◽  
Xinyu Zhang ◽  
Mingzhen Ma ◽  
Duanwei He ◽  
...  

Vickers hardness, phase combination, elastic modulus and cutting performance of the cubic boron nitride (cBN) based composites with different cBN weight ratios sintered at high pressure and high temperature were investigated. During high-pressure sintering, reactions occurred between cBN and Ti 3 SiC 2, then new compounds, TiB 2, C 0.7 N 0.3 Ti , SiC and SiB 4 were formed, and no hBN phase was observed. Bulk modulus and hardness of the cBN composites decreased with increasing Ti 3 SiC 2 contents in raw mixture, and the highest hardness of 35.9 GPa was achieved for 95 wt.% cBN–5 wt.% Ti 3 SiC 2 composition specimen sintered at 1600°C. In addition, the present cBN-based composites exhibited good cutting performance.


2010 ◽  
Vol 24 (26) ◽  
pp. 2647-2657 ◽  
Author(s):  
R. KUMAR ◽  
UMA D. SHARMA ◽  
MUNISH KUMAR

Two different approaches to study thermal expansion and compression of nanosystems are unified, which have been treated quite independently by earlier workers. We provide the simple theoretical analysis, which demonstrates that these two approaches may be unified into a single theory, viz. one can be derived from other. It is concluded that there is a single theory in the place of two different approaches. To show the real connection with the nanomaterials, we study the effect of temperature (at constant pressure), the effect of pressure (at constant temperature) as well as the combined effect of pressure and temperature. We have considered different nanomaterials viz. carbon nanotube, AlN , Ni , 80 Ni –20 Fe , Fe – Cu , MgO , CeO 2, CuO and TiO 2. The results obtained are compared with the available experimental data. A good agreement between theory and experiment demonstrates the validity of the present approach.


Geofluids ◽  
2021 ◽  
Vol 2021 ◽  
pp. 1-14
Author(s):  
Mingwei Kong ◽  
Zhaopeng Zhang ◽  
Chunyan Zhao ◽  
Huasheng Chen ◽  
Xinfang Ma ◽  
...  

The mechanical properties of the high-temperature and high-pressure reservoirs in the southern margin of Junggar Basin have not been clearly understood, which correspondingly results in uncertainties when predicting the breakdown pressure. To address this issue, firstly, rock mechanical experiments under high temperature, high confining pressure, and high pore pressure were carried out. Secondly, empirical formulas related to the transformation of dynamic and static mechanical parameters in the regional strata were proposed. Finally, the existing prediction model for the formation breakdown pressure was improved by taking the wellbore seepage and thermal stress into consideration. Results show that under the reservoir condition of high temperature and high pressure, the rock sample tends to form closed shear cracks. High temperature causes thermal damages and the reduction of the compressive strength and elastic modulus, while the combined effects of high confining pressure and pore pressure enhance the compressive strength and plasticity of the rock sample simultaneously. Based on the correlation analysis, it is found that the static elastic modulus is linearly related to the dynamic value, while static Poisson’s ratio is a quadratic function of the dynamic value. These fitting functions can be used to obtain the profiles of static elastic modulus and Poisson’s ratio based on their dynamic values from the logging interpretation. Besides, the improved prediction model for the rock breakdown pressure can yield more accurate results indicated by the error less than 2%. Therefore, the proposed breakdown pressure prediction model in this study can provide theoretical guidance in the selection of fracturing truck groups and the design of the pumping schedule for high-temperature and high-pressure reservoirs.


Author(s):  
E. F. Koch

Because of the extremely rigid lattice structure of diamond, generating new dislocations or moving existing dislocations in diamond by applying mechanical stress at ambient temperature is very difficult. Analysis of portions of diamonds deformed under bending stress at elevated temperature has shown that diamond deforms plastically under suitable conditions and that its primary slip systems are on the ﹛111﹜ planes. Plastic deformation in diamond is more commonly observed during the high temperature - high pressure sintering process used to make diamond compacts. The pressure and temperature conditions in the sintering presses are sufficiently high that many diamond grains in the sintered compact show deformed microtructures.In this report commercially available polycrystalline diamond discs for rock cutting applications were analyzed to study the deformation substructures in the diamond grains using transmission electron microscopy. An individual diamond particle can be plastically deformed in a high pressure apparatus at high temperature, but it is nearly impossible to prepare such a particle for TEM observation, since any medium in which the diamond is mounted wears away faster than the diamond during ion milling and the diamond is lost.


Alloy Digest ◽  
2019 ◽  
Vol 68 (11) ◽  

Abstract YSS YXM4 is a cobalt-alloyed molybdenum high-speed tool steel with resistance to abrasion, seizure, and deformation under high pressure. This datasheet provides information on composition, physical properties, and hardness. It also includes information on high temperature performance. Filing Code: TS-780. Producer or source: Hitachi Metals America, Ltd.


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